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NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...

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4.4.4 COMMENTS<br />

- 55 -<br />

For completeness we include at this point a few general<br />

comments about the foil bearing rotor system.<br />

It was found that at speeds up to 7 kHz the foil bearing<br />

rotors were extremely reliable. Every rotor constructed as<br />

described in Section 4.4.2 rotated stably even with full-sized<br />

liquid samples. Not all the conical rotors would rotates even<br />

on air. Although it is not a normal requirement of any NMR<br />

rotation system, it is worth noting that the Bernoulli rotors<br />

would not spin with liquid samples of any reasonable volume.<br />

Because of the heating effect upon rotation, use of the foil<br />

bearing system appears to be limited to those cases where the<br />

temperature of the sample is relatively unimportant. As the<br />

attainment of rotation rates above 7 kHz was limited only by the<br />

failure of the alumina axles, silicon nitride might well prove<br />

a more suitable axle material. Its tensile strength is typically<br />

the same as alumina, but its density is only about 2.6 gm/cm3<br />

compared to 3.8 gm/cm 3.<br />

The coefficient of thermal expansion in<br />

silicon nitride is half that of alumina(64) so upon rotation both<br />

the induced thermal and mechanical stresses should be less. If<br />

the use of this or any other material does result in a consider-<br />

able improvement in performance it might prove possible to use a<br />

much simpler rotor design in a foil bearing, such as a single<br />

hollow tube.

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