NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...
NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...
NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...
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the range ±1 V are digitised to a7 bit resolution and summed in<br />
a 16 bit register. The time interval per point is variable bet-<br />
ween 2 Ps and 50 ms and the averaged signal may be displayed on<br />
an oscilloscope to 7 bit accuracy. In the particular experimental<br />
set-up used the full 16 bit output of each register was read out<br />
through a Data Laboratories 1002/100c interface coupled to a Data<br />
Dynamics teletype.<br />
The M12 electromagnet used in this work had originally been<br />
part of an RS 2 high resolution CWNMR<br />
spectrometer manufactured by<br />
AEI. The maximum period of time over which the signal could be<br />
accumulated<br />
in the signal averager was in some cases limited by<br />
the slight drift in the magnetic field.<br />
5.2 MODIFICATION OF THE SPECTROMETER<br />
PULSE PROGRAMMER<br />
The four pulse units of the spectrometer are located in inter-<br />
changeable plug-in units. Each unit consists of two monostable<br />
flip-flops; one for determining the pulse length and one for deter-<br />
mining the delay time with respect to the previous pulse. However,<br />
because the delay times are set via decade counters, they are<br />
correct only when the pulse delay time is less or equal to that<br />
of the preceeding pulse. Such a condition means that some simple<br />
pulse sequences cannot be performed using the standard spectrometer.<br />
To overcome this problem a Mullard FJK 101 integrated<br />
mono-<br />
stable circuit was set-up to provide a positive DC pulse of contin-<br />
uously variable duration between 0.5 us and 120 ms compatible with<br />
the internal logic of the spectrometer. The complete circuit was<br />
mounted in an aluminium box with a plug connector so as to be inter-<br />
changeable with any of the plug-in pulse units. The monostable