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NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...

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- 59 -<br />

the range ±1 V are digitised to a7 bit resolution and summed in<br />

a 16 bit register. The time interval per point is variable bet-<br />

ween 2 Ps and 50 ms and the averaged signal may be displayed on<br />

an oscilloscope to 7 bit accuracy. In the particular experimental<br />

set-up used the full 16 bit output of each register was read out<br />

through a Data Laboratories 1002/100c interface coupled to a Data<br />

Dynamics teletype.<br />

The M12 electromagnet used in this work had originally been<br />

part of an RS 2 high resolution CWNMR<br />

spectrometer manufactured by<br />

AEI. The maximum period of time over which the signal could be<br />

accumulated<br />

in the signal averager was in some cases limited by<br />

the slight drift in the magnetic field.<br />

5.2 MODIFICATION OF THE SPECTROMETER<br />

PULSE PROGRAMMER<br />

The four pulse units of the spectrometer are located in inter-<br />

changeable plug-in units. Each unit consists of two monostable<br />

flip-flops; one for determining the pulse length and one for deter-<br />

mining the delay time with respect to the previous pulse. However,<br />

because the delay times are set via decade counters, they are<br />

correct only when the pulse delay time is less or equal to that<br />

of the preceeding pulse. Such a condition means that some simple<br />

pulse sequences cannot be performed using the standard spectrometer.<br />

To overcome this problem a Mullard FJK 101 integrated<br />

mono-<br />

stable circuit was set-up to provide a positive DC pulse of contin-<br />

uously variable duration between 0.5 us and 120 ms compatible with<br />

the internal logic of the spectrometer. The complete circuit was<br />

mounted in an aluminium box with a plug connector so as to be inter-<br />

changeable with any of the plug-in pulse units. The monostable

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