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manual of methods of analysis of foods - Ministry of Health and ...

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METALS<br />

(ii)<br />

Diaphragm pump: Neptune Dyna Pump or equivalent. Coat diaphragm<br />

<strong>and</strong> internal parts <strong>of</strong> pump with acrylic type plastic spray. Use 16<br />

gauge teflon tubing for all connections.<br />

(iii)<br />

Water condenser: 12 to 18 (id) × 400 mm borosilicate, 24/40 st<strong>and</strong>ard<br />

taper joint, modified to hold 6 mm Raschig rings. Fill condenser with<br />

Raschig rings to a height <strong>of</strong> 100 mm, then place 20 mm layer <strong>of</strong> 4 mm<br />

diameter glass beads on top <strong>of</strong> rings.<br />

(iv)<br />

Digestion flask: 250 ml fat bottom boiling flask with 24/40 st<strong>and</strong>ard<br />

taper joint.<br />

(v) Gas inlet adapter: 24/40 st<strong>and</strong>ard taper (Kontes Glass Co., No. K-<br />

181000 or equivalent.<br />

14

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