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450<br />
400<br />
coating thickness (Å)<br />
350<br />
300<br />
250<br />
200<br />
150<br />
100<br />
0 1 2 3 4 5<br />
duration of coating (min)<br />
Figure 8. Coating thickness dependence on coating duration.<br />
2.4. Sample characterization and Analysis<br />
A Rigaku Multiflex X-ray diffractometer using Cu Kα radiation, was employed to<br />
characterize LaNi 5 +Al samples. Analysis was done over a 2θ range of 20º to 80º. The slit<br />
width and scanning speed were 0.020 mm and 2.400 degrees per minute, respectively.<br />
The X-ray generator voltage and current were set to 40 kV and 30 mA, respectively.<br />
Samples were supported on a metal sample holder whose bottom was closed by scotch<br />
tape and the sample was filled above it. Data were analyzed by Jade analysis software.<br />
Elemental analysis of LaNi 5 and Al doped LaNi 5 was done by flame emission<br />
spectroscopy using a Varian Inc. SpectrAA10 spectrometer. Lanthanum, nickel, and<br />
33