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Thesis - Oztek_Muzaffer_T_200508_MA

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After dehydriding by the sample, the same procedure was repeated by using 50% (v/v)<br />

H 2 :He.<br />

For the reaction of the samples with H 2 , the pressure profiles were plotted (Figure<br />

33). The reactions were complete within 10 minutes; much like the reaction of LaNi 5<br />

with H 2 analyzed using the DSC. The hydrogen capacities of the samples given in Table<br />

6 indicate the percent hydrogen absorbed by the LaNi 5 was also in accordance with the<br />

results obtained from DSC analysis, which were given in Table 1.<br />

8<br />

7<br />

P (atm)<br />

6<br />

5<br />

0.74 %Al<br />

1.35 %Al<br />

3.38 %Al<br />

4<br />

3<br />

0 100 200 300 400 500 600 700 800<br />

time (s)<br />

Figure 33. Pressure profiles under H 2 atmosphere.<br />

71

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