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Thesis - Oztek_Muzaffer_T_200508_MA

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1.2<br />

1.0<br />

(a)<br />

(b)<br />

Wt. % H absorbed<br />

0.8<br />

0.6<br />

0.4<br />

0.2<br />

(c)<br />

0.0<br />

0 2000 4000 6000 8000 10000 12000<br />

time (s)<br />

(a) non-coated, under H 2<br />

(b) Pt coated, under 50% (v/v) H 2 -He<br />

(c) non-coated, under 50% (v/v) H 2 -He<br />

Figure 32. Percent hydrogen curves for rate comparison of Pt coated and non-coated<br />

samples.<br />

3.3. Parr Reactor<br />

Samples of LaNi 5 with 0.74, 1.35 and 3.38% Al were tested in the Parr reactor.<br />

After the activation procedure, the reactor was pressurized with H 2 sealed. Pressure drop<br />

was monitored and the percent hydrogen absorbed was calculated using the ideal gas law.<br />

70

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