Amphetamine and Related Drugs

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Gas Chromatography. System GA—amfetamine GA amfetamine RI 1125, amfetamine-TFA amfetamine TFA RI 1095, amfetamine-PFP amfetamine PFP RI 1330, amfetamine-TMS amfetamine TMS RI 1190, amfetamine-AC amfetamine AC RI 1501, art (formyl) RI 1100, M (3-OH (3 OH-)- PFP2 RI 1520, M (3-OH (3 OH-)-TMS2 TMS2 RI 1850, M (3-OH (3 OH-)-AC2 AC2 RI 1930, M (4-OH (4 OH-) ) RI 1480, M (4-OH (4 OH-)-AC2 AC2 RI 1900, M (3,4–di (3,4 di-OH OH-)-AC3 AC3 RI 2150, M (OH-methoxy (OH methoxy-) ) RI 1465, M (OH-methoxy (OH methoxy-)-AC2 AC2 RI 2065, M (desamino–oxo (desamino oxo-OH OH-)-AC AC RI 1520, M (desamino–oxo (desamino oxo-OH OH-methoxy methoxy-) ) RI 1510, M (desamino–oxo (desamino oxo-OH OH-methoxy methoxy-)-AC AC RI 1600, M (desamino– (desamino oxo–di oxo di-OH OH-)-AC2 AC2 RI 1735; system GB—amfetamine GB amfetamine RI 1150; art (formyl) RI 1142; system GC—RI GC RI 1536; system GF—RI GF RI 1315; system GAK—retention GAK retention time 4.9 min. 4/27/2009 ١٠٢
Column: DB-5 DB 5 fused silica (30 m × 0.25 mm i.d., 0.25 μm m film thickness). Column temperature: 70° 70 for 1 min, ramp to 100° 100 at 30°/min, 30 /min, <strong>and</strong> to 270° 270 at 10°/min. 10 /min. Injector temperature: 280°. 280 . Carrier gas: helium, flow rate 0.8 mL/min. MS detection. Retention time: 6.5 min. 4/27/2009 ١٠٣
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Amphetamine and Related Drugs 4/27/
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Cocaine Amphetamines Methcathinone
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Marijuana Hashish Hashish Oil Canna
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Other Categories Inhalants like amy
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Schedule I amphetamine derivatives
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Schedule III • The drug or other
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Schedule V • The drug or other su
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4/27/2009 ١٥
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As use of amphetamines spread, so d
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To meet the ever-increasing ever in
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The effects of amphetamines, especi
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A colourless, mobile, slowly volati
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Amfetamine Sulfate Synonyms. Amphet
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4/27/2009 ٢٧
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Therapeutic concentration After no
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Toxicity The estimated minimum leth
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Methylenedioxymethamfetamine Stimul
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N,α-Dimethyl Dimethyl-1,3,benzodio
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Colour Test. Marquis Reagent—bla
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Therapeutic concentration 8 healthy
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Toxicity Fatalities with doses of 3
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Metamfetamine Central Stimulant Syn
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Metamfetamine Hydrochloride Propri
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Disposition in the Body Readily abs
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Half-life Half life Plasma half-li
Page 51 and 52: A viscous, colourless oil. B.p. is
Page 53 and 54: Disposition in the Body. It is abs
Page 55 and 56: Methylenedioxyamfetamine Hallucinog
Page 57 and 58: Why are adulterants and diluants ad
Page 59 and 60: Sampling and Physical Description o
Page 61 and 62: Recording the ballistic features of
Page 63 and 64: Having carried out the control proc
Page 65 and 66: For tableted materials, homogenizat
Page 67 and 68: The sample should be dissolved as f
Page 69 and 70: The pooled sulfuric acid extracts a
Page 71 and 72: Urine analyzed by Test B shows an i
Page 73 and 74: Aspirate off the lower chloroform l
Page 75 and 76: Add 20 ml chloroform and shake for
Page 77 and 78: Transfer the residue to a 3 ml micr
Page 79 and 80: Dissolve the residues in 20 µl l o
Page 81 and 82: Remove the developed plate and allo
Page 83 and 84: Methamphetamine (Methedrine ( Methe
Page 85 and 86: In addition, MDA, MDMA and MDEA giv
Page 87 and 88: Thin-layer Thin layer Chromatograph
Page 89 and 90: Colour test The Marquis test gives
Page 91 and 92: System TC Plates: Plates: Silica ge
Page 93 and 94: System TAE Plates: Plates: Silica g
Page 95 and 96: Location reagents for systems TA, T
Page 97 and 98: Dragendorff spray Yellow, orange, r
Page 99 and 100: Mandelin’s Mandelin s reagent Thi
Page 101: Acidified potassium permanganate so
Page 105 and 106: Column: Chiralcel OD-RH OD RH (150
Page 107 and 108: Definitive De nitive Identification
Page 109 and 110: 4/27/2009 ١٠٩
Page 111 and 112: In order to alleviate this problem,
Page 113 and 114: The reaction (see equation (2.1)) i
Page 115 and 116: Quantification Quanti cation of Amp
Page 117 and 118: The amphetamines (standards and sam
Page 119 and 120: Derivatization 4/27/2009 ١١٩
Page 121: Mass Spectra 44 91 40 42 65 45 39 4
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Amphetamine and Related Drugs

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