Amphetamine and Related Drugs

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Infra–red Infra red Spectrum Principal peaks at wavenumbers 700, 740, 1495, 1090, 1605, 825 cm−1 cm 4/27/2009 ١٠٦
Definitive De nitive Identification Identi cation of <strong>Amphetamine</strong>s GC–MS GC MS is the preferred method for the identification identi cation of amphetamines. The discussion below centres on the analysis of amphetamine itself, although the same principles can also be applied to other members of this class of drug. However, there are a number of problems associated with the gas chromatographic analysis of amphetamine. Being highly polar in nature, this compound is liable to poor chromatographic behaviour <strong>and</strong> tailing if the analytical instrument is not scrupulously clean 4/27/2009 ١٠٧
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Amphetamine and Related Drugs 4/27/
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Cocaine Amphetamines Methcathinone
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Marijuana Hashish Hashish Oil Canna
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Other Categories Inhalants like amy
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Schedule I amphetamine derivatives
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Schedule III • The drug or other
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Schedule V • The drug or other su
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4/27/2009 ١٥
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As use of amphetamines spread, so d
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To meet the ever-increasing ever in
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The effects of amphetamines, especi
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A colourless, mobile, slowly volati
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Amfetamine Sulfate Synonyms. Amphet
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4/27/2009 ٢٧
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Therapeutic concentration After no
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Toxicity The estimated minimum leth
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Methylenedioxymethamfetamine Stimul
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N,α-Dimethyl Dimethyl-1,3,benzodio
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Colour Test. Marquis Reagent—bla
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Therapeutic concentration 8 healthy
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Toxicity Fatalities with doses of 3
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Metamfetamine Central Stimulant Syn
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Metamfetamine Hydrochloride Propri
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Disposition in the Body Readily abs
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Half-life Half life Plasma half-li
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A viscous, colourless oil. B.p. is
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Disposition in the Body. It is abs
Page 55 and 56: Methylenedioxyamfetamine Hallucinog
Page 57 and 58: Why are adulterants and diluants ad
Page 59 and 60: Sampling and Physical Description o
Page 61 and 62: Recording the ballistic features of
Page 63 and 64: Having carried out the control proc
Page 65 and 66: For tableted materials, homogenizat
Page 67 and 68: The sample should be dissolved as f
Page 69 and 70: The pooled sulfuric acid extracts a
Page 71 and 72: Urine analyzed by Test B shows an i
Page 73 and 74: Aspirate off the lower chloroform l
Page 75 and 76: Add 20 ml chloroform and shake for
Page 77 and 78: Transfer the residue to a 3 ml micr
Page 79 and 80: Dissolve the residues in 20 µl l o
Page 81 and 82: Remove the developed plate and allo
Page 83 and 84: Methamphetamine (Methedrine ( Methe
Page 85 and 86: In addition, MDA, MDMA and MDEA giv
Page 87 and 88: Thin-layer Thin layer Chromatograph
Page 89 and 90: Colour test The Marquis test gives
Page 91 and 92: System TC Plates: Plates: Silica ge
Page 93 and 94: System TAE Plates: Plates: Silica g
Page 95 and 96: Location reagents for systems TA, T
Page 97 and 98: Dragendorff spray Yellow, orange, r
Page 99 and 100: Mandelin’s Mandelin s reagent Thi
Page 101 and 102: Acidified potassium permanganate so
Page 103 and 104: Column: DB-5 DB 5 fused silica (30
Page 105: Column: Chiralcel OD-RH OD RH (150
Page 109 and 110: 4/27/2009 ١٠٩
Page 111 and 112: In order to alleviate this problem,
Page 113 and 114: The reaction (see equation (2.1)) i
Page 115 and 116: Quantification Quanti cation of Amp
Page 117 and 118: The amphetamines (standards and sam
Page 119 and 120: Derivatization 4/27/2009 ١١٩
Page 121: Mass Spectra 44 91 40 42 65 45 39 4
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