Amphetamine and Related Drugs

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Procedure for Test B Measure 20 ml of urine into a 50 ml glass- glass stoppered centrifuhe tube. Add 1 g of potassium carbonate to adjust the pH to 10. Add 4 g of sodium chloride. Add the salts using a powder funnel and measuring spoons. Shake to dissolve the salts. Add 20 ml of chloroform and shake for 5 minutes and centrifuge. 4/27/2009 ٧٢
Aspirate off the lower chloroform layer and filter into another tube. Add 20 ml of chloroform for a second extraction. Shake for 5 minutes and centrifuge. Aspirate off the lower chloroform layer and filter into the second tube. Wash the filtered pooled chloroform with 10 ml of pH 9 aqueous ammonium hydroxide solution as follows: shake for 5 minutes and centrifuge and aspirate off and discard the upper wash phase. phase 4/27/2009 ٧٣
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Amphetamine and Related Drugs 4/27/
Page 3 and 4:
Cocaine Amphetamines Methcathinone
Page 5 and 6:
Marijuana Hashish Hashish Oil Canna
Page 7 and 8:
Other Categories Inhalants like amy
Page 9 and 10:
Schedule I amphetamine derivatives
Page 11 and 12:
Schedule III • The drug or other
Page 13 and 14:
Schedule V • The drug or other su
Page 15 and 16:
4/27/2009 ١٥
Page 17 and 18:
As use of amphetamines spread, so d
Page 19 and 20:
To meet the ever-increasing ever in
Page 21 and 22: The effects of amphetamines, especi
Page 23 and 24: A colourless, mobile, slowly volati
Page 25 and 26: Amfetamine Sulfate Synonyms. Amphet
Page 27 and 28: 4/27/2009 ٢٧
Page 29 and 30: Therapeutic concentration After no
Page 31 and 32: Toxicity The estimated minimum leth
Page 33 and 34: Methylenedioxymethamfetamine Stimul
Page 35 and 36: N,α-Dimethyl Dimethyl-1,3,benzodio
Page 37 and 38: Colour Test. Marquis Reagent—bla
Page 39 and 40: Therapeutic concentration 8 healthy
Page 41 and 42: Toxicity Fatalities with doses of 3
Page 43 and 44: Metamfetamine Central Stimulant Syn
Page 45 and 46: Metamfetamine Hydrochloride Propri
Page 47 and 48: Disposition in the Body Readily abs
Page 49 and 50: Half-life Half life Plasma half-li
Page 51 and 52: A viscous, colourless oil. B.p. is
Page 53 and 54: Disposition in the Body. It is abs
Page 55 and 56: Methylenedioxyamfetamine Hallucinog
Page 57 and 58: Why are adulterants and diluants ad
Page 59 and 60: Sampling and Physical Description o
Page 61 and 62: Recording the ballistic features of
Page 63 and 64: Having carried out the control proc
Page 65 and 66: For tableted materials, homogenizat
Page 67 and 68: The sample should be dissolved as f
Page 69 and 70: The pooled sulfuric acid extracts a
Page 71: Urine analyzed by Test B shows an i
Page 75 and 76: Add 20 ml chloroform and shake for
Page 77 and 78: Transfer the residue to a 3 ml micr
Page 79 and 80: Dissolve the residues in 20 µl l o
Page 81 and 82: Remove the developed plate and allo
Page 83 and 84: Methamphetamine (Methedrine ( Methe
Page 85 and 86: In addition, MDA, MDMA and MDEA giv
Page 87 and 88: Thin-layer Thin layer Chromatograph
Page 89 and 90: Colour test The Marquis test gives
Page 91 and 92: System TC Plates: Plates: Silica ge
Page 93 and 94: System TAE Plates: Plates: Silica g
Page 95 and 96: Location reagents for systems TA, T
Page 97 and 98: Dragendorff spray Yellow, orange, r
Page 99 and 100: Mandelin’s Mandelin s reagent Thi
Page 101 and 102: Acidified potassium permanganate so
Page 103 and 104: Column: DB-5 DB 5 fused silica (30
Page 105 and 106: Column: Chiralcel OD-RH OD RH (150
Page 107 and 108: Definitive De nitive Identification
Page 109 and 110: 4/27/2009 ١٠٩
Page 111 and 112: In order to alleviate this problem,
Page 113 and 114: The reaction (see equation (2.1)) i
Page 115 and 116: Quantification Quanti cation of Amp
Page 117 and 118: The amphetamines (standards and sam
Page 119 and 120: Derivatization 4/27/2009 ١١٩
Page 121: Mass Spectra 44 91 40 42 65 45 39 4
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