Chapter 4 - Jacobs University

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<strong>Chapter</strong> 9 Unpublished Results Figure 9.31 Solution 13 C NMR spectrum of freshly prepared 16a mixture dissolved in H 2 2O/D 2 O. Figure 9.32 Solution 89 Y NMR spectrum of freshly prepared 16a mixture dissolved in H 2 O/D 2 O. 181
<strong>Chapter</strong> 9 Unpublished Results 9.2.2.4 Conclusion We have synthesized a novel trimeric yttrium containing polyoxometalate, which may contain tetrahedral tungsten, linked through three yttrium ions. We have characterized it by single crystal XRD, NMR, IR and TGA. The final compound was synthesized in one-pot procedure in a simple aqueous conditions and it crystallizes in orthorhombic crystal system (space group Pnma). The given structure shows us that used precursor ligand Na 9 [a-SbW 9 O 33 ]∙27H 2 O is quite an interesting species which supports a yttrium cluster as well as and may have a tetrahedral central tungsten atom stabilizing the whole complex. 182
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Synthesis, Structure and Properties
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"The greatest book of philosophy, w
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system, space group I4/m, unit cell
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Acknowledgements The accomplishment
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teaching, and Professor Maravanji S
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2.1.2 Single crystal X-ray diffract
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5.5 Conclusion…………………
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9.1.6.1 Results and discussion…
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9.3.5 Synthesis of K 12 [Hf 4 (µ 2
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Crespo………………………
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Figure 5.4 ORTEP view of the asymme
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Figure 9.6 31 P NMR of 7a in H 2 O/
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Figure 9.34 TGA spectrum of 17a…
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Figure 9.62 FTIR spectrum of 23a…
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Table 9.6 Crystal data and structur
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Chapter 1 Introduction heteropolyan
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Chapter 1 Introduction 1.3 Structur
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Chapter 1 Introduction C) Keggin a-
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Chapter 1 Introduction shows no suc
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Chapter 1 Introduction α-[P 2 W 18
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Chapter 1 Introduction Figure 1.7 B
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Chapter 1 Introduction [P 2 W 18 O
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Chapter 1 Introduction 1.5.3 Medici
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Chapter 1 Introduction (17) Evans,
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Chapter 1 Introduction (48) Mizuno,
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Chapter 1 Introduction (84) Isabell
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Chapter 2 were block-diagonal least
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Chapter 2 Experimental 2.2.3 Synthe
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Chapter 2 Experimental 2.2.7 Synthe
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Chapter 2 Experimental 2.2.11 Synth
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Chapter 2 Experimental 2.3Reference
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Chapter 3 The Wheel-Shaped Cu 20 in
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Chapter 3 The Wheel-Shaped Cu 20 3.
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Chapter 3 The Wheel-Shaped Cu 20 Fi
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Chapter 3 The Wheel-Shaped Cu 20 Cu
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Chapter 3 The Wheel-Shaped Cu 20 20
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Chapter 4 16-Iron Metal Center Nano
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Chapter 5 Organoruthenium POM Chapt
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Chapter 5 Organoruthenium POM 5.2 S
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Chapter 5 Organoruthenium POM 5.3 X
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Chapter 5 Organoruthenium POM 5.4 R
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Chapter 5 Organoruthenium POM The f
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Chapter 5 Organoruthenium POM On th
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Chapter 5 Organoruthenium POM Figur
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Chapter 5 Organoruthenium POM (11)
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Chapter 6 U-peroxo-Polyoxometalate
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Chapter 7 Pt-containing Polyoxometa
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Chapter 9 Unpublished Results Table
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Curriculum Vitae SIB SANKAR MAL Dep
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EDUCATION PhD Jacobs University (20
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POSTER, ORAL PRESENTATION 1. Poster
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6. “Two Iron-Containing Tungstoge
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Appendix
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Appendix
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Chapter 4 - Jacobs University

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