Chapter 4 - Jacobs University

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PUBLICATIONS 1. “The Wheel-Shaped Cu20-Tungstophosphate [Cu 20 Cl(OH) 24 (H 2 O) 12 (P 8 W 48 O 184 )] 25- Ion” Sib Sankar Mal; Ulrich Kortz, Angew. Chem. Int. Ed. 2005, 44, 3777-3780. 2. “The Wheel-Shaped Cu20-Tungstophosphate [Cu 20 Cl(OH) 24 (H 2 O) 12 (P 8 W 48 O 184 )] 25- , Redox and Electrocatalytic Properties.” Darine Jabbour; Bineta Keita; Louis Nadjo; Ulrich Kortz; Sib Sankar Mal Electrochem. Comm. 2005, 7, 841-847 3. “STM/STS Observation of Polyoxoanions on HOPG Surfaces: The Wheel-shaped [Cu 20 Cl(OH) 24 (H 2 O) 12 (P 8 W 48 O 184 )] 25- and the Ball-shaped [{Sn(CH 3 ) 2 (H 2 O)} 24 {Sn(CH 3 ) 2 } 12 (A-PW 9 O 34 ) 12 ] 36-” Mohammad S. Alam; V. Dremov; Paul Müller; A. V. Postnikov; Sib Sankar Mal; Firasat Hussain; Ulrich Kortz, Inorg. Chem., 2006, 45, 2866-2872 4. “Wheel-Shaped Polyoxotungstate [Cu 20 Cl(OH) 24 (H 2 O) 12 (P 8 W 48 O 184 )] 25- Macroanion Forms Supramolecular "Blackberry" Structure in Aqueous Solution” Guang Liu; Tianbo Liu; Sib Sankar Mal.; Ulrich Kortz, J. Am. Chem. Soc., 2006 128, 10103-10110 (Addition/Correction), 2007, 129, 2408-2408). 5. “Organoruthenium derivative of the cyclic [H 7 P 8 W 48 O 184 ] 33- anion: [{K(H 2 O)} 3 {Ru(p-cymene)(H 2 O)} 4 P 8 W 49 O 186 (H 2 O) 2 ] 27-” Sib Sankar Mal; Nadeen H. Nsouli,; Michael H. Dickman,; Ulrich Kortz, Dalton Trans., 2007,2627-2630. ( With Inside Cover Picture)
6. “Two Iron-Containing Tungstogermanates: [K(H 2 O)(β-Fe 2 GeW 10 O 37 (OH))(γ- GeW 10 O 36 )] 12- and [{β-Fe 2 GeW 10 O 37 (OH) 2 } 2 ] 12-” Nadeen H. Nsouli,; Sib Sankar Mal; Michael H. Dickman,; Ulrich Kortz; Bineta Keita; Louis Nadjo; Clemente-Juan, J. M. Inorg. Chem., 2007, 46, 8763-8770. 7. “Facile Incorporation of Platinum(IV) into Polyoxometalate Frameworks: Preparation of [H 2 Pt IV V 9 O 28 ] 5- and First Evidence of 195 Pt NMR” Uk Lee, Hea-Chung Joo, Ki-Min Park, Sib Sankar Mal, Ulrich Kortz, Bineta Keita, and Louis Nadjo. Angew. Chem. Int. Ed. 2008, 47, 793-796. 8. “Nucleation process in the cavity of a 48-tungstophosphate wheel resulting in a 16 metal center iron-oxide nanocluster” Sib Sankar Mal, Michael H. Dickman, Ulrich Kortz, Ana Maria Todea, Alice Merca, Hartmut Bögge, Thorsten Glaser, Achim Müller, Saritha Nellutla,Narpinder Kaur, Johan van Tol, Naresh S. Dalal, Bineta Keita, and Louis Nadjo Chem. Eur. J., 2008, 14, 1186- 1195. 9. “Pulsed field magnetization, electron spin resonance, and nuclear spin-lattice relaxation in the {Cu 3 } spin triangle” Kwang-Yong Choi, Naresh S. Dalal, Arneil P. Reyes, Philip L. Kuhns, Sib Sankar Mal, and Ulrich Kortz . Physical Review B, 2008, 77, 024406 10. “Mixed-Valence 24-Vanadophosphate Decorated with Six Ru II (dmso) 3 Groups: [{Ru II 3(dmso) 9 PV V 11V IV Ru III O 37 (OH) 3 } 2 ] 8-” Li-Hua Bi, Sib Sankar Mal, Nadeen H. Nsouli, Michael H. Dickman, Ulrich Kortz, Saritha Nellutla, Naresh S. Dalal, Manuel Prinz, George Hofmann, and Manfred Neumann. J. Clust. Sci. 2008, 19, 259-273.
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Synthesis, Structure and Properties
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"The greatest book of philosophy, w
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system, space group I4/m, unit cell
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Acknowledgements The accomplishment
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teaching, and Professor Maravanji S
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2.1.2 Single crystal X-ray diffract
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5.5 Conclusion…………………
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9.1.6.1 Results and discussion…
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9.3.5 Synthesis of K 12 [Hf 4 (µ 2
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Crespo………………………
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Figure 5.4 ORTEP view of the asymme
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Figure 9.6 31 P NMR of 7a in H 2 O/
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Figure 9.34 TGA spectrum of 17a…
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Figure 9.62 FTIR spectrum of 23a…
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Table 9.6 Crystal data and structur
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Chapter 1 Introduction heteropolyan
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Chapter 1 Introduction 1.3 Structur
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Chapter 1 Introduction C) Keggin a-
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Chapter 1 Introduction shows no suc
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Chapter 1 Introduction α-[P 2 W 18
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Chapter 1 Introduction Figure 1.7 B
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Chapter 1 Introduction [P 2 W 18 O
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Chapter 1 Introduction 1.5.3 Medici
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Chapter 1 Introduction (17) Evans,
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Chapter 1 Introduction (48) Mizuno,
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Chapter 1 Introduction (84) Isabell
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Chapter 2 were block-diagonal least
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Chapter 2 Experimental 2.2.3 Synthe
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Chapter 2 Experimental 2.2.7 Synthe
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Chapter 2 Experimental 2.2.11 Synth
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Chapter 2 Experimental 2.3Reference
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Chapter 3 The Wheel-Shaped Cu 20 in
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Chapter 3 The Wheel-Shaped Cu 20 3.
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Chapter 3 The Wheel-Shaped Cu 20 Fi
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Chapter 3 The Wheel-Shaped Cu 20 Cu
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Chapter 3 The Wheel-Shaped Cu 20 20
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Chapter 4 16-Iron Metal Center Nano
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Chapter 5 Organoruthenium POM Chapt
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Chapter 5 Organoruthenium POM 5.2 S
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Chapter 5 Organoruthenium POM 5.3 X
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Chapter 5 Organoruthenium POM 5.4 R
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Chapter 5 Organoruthenium POM The f
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Chapter 5 Organoruthenium POM On th
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Chapter 5 Organoruthenium POM Figur
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Chapter 5 Organoruthenium POM (11)
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Chapter 6 U-peroxo-Polyoxometalate
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Chapter 8 Collaborative Work Chapte
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Chapter 8 Collaborative Work 8.2.1
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Chapter 9 Unpublished Results Figur
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Chapter 9 Unpublished Results solid
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Chapter 9 Unpublished Results 9.1.3
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Chapter 9 Unpublished Results Table
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