Chapter 4 - Jacobs University

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<strong>Chapter</strong> 9 Unpublished Results Figure 9.49 Polyhedral/ball and stick type structural representation of 19. Color scheme: Y, Si and WO 6 units are shown by yellow, green and red respectively. 9.2.5.3 Solution NMR To complement our solid state XRD results on 18 with solution studies, we performed 89 Y NMR at room temperature on 18a redissolved in H 2 O/D 2 O. 89 Y NMR (Figure 9.50) spectrum exhibits one signal at 43.11 ppm which is fully consistent with the solid state structure. 205
<strong>Chapter</strong> 9 Unpublished Results Figure 9.50 89 YNMR study of freshly prepared 19a mixture dissolved in H 2 O/D 2 O. 9.2.5.4 Conclusion We have isolated a sandwich yttrium-containing polyoxometalate and we analyzed the compound by single crystal XRD, IR, NMR and TGA. The final compound was derived in single pot and with simple aqueous conditions, which crystallizes in orthorhombic crystal system with Pnma space group. 206
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Synthesis, Structure and Properties
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"The greatest book of philosophy, w
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system, space group I4/m, unit cell
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Acknowledgements The accomplishment
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teaching, and Professor Maravanji S
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2.1.2 Single crystal X-ray diffract
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5.5 Conclusion…………………
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9.1.6.1 Results and discussion…
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9.3.5 Synthesis of K 12 [Hf 4 (µ 2
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Crespo………………………
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Figure 5.4 ORTEP view of the asymme
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Figure 9.6 31 P NMR of 7a in H 2 O/
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Figure 9.34 TGA spectrum of 17a…
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Figure 9.62 FTIR spectrum of 23a…
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Table 9.6 Crystal data and structur
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Chapter 1 Introduction heteropolyan
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Chapter 1 Introduction 1.3 Structur
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Chapter 1 Introduction C) Keggin a-
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Chapter 1 Introduction shows no suc
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Chapter 1 Introduction α-[P 2 W 18
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Chapter 1 Introduction Figure 1.7 B
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Chapter 1 Introduction [P 2 W 18 O
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Chapter 1 Introduction 1.5.3 Medici
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Chapter 1 Introduction (17) Evans,
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Chapter 1 Introduction (48) Mizuno,
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Chapter 1 Introduction (84) Isabell
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Chapter 2 were block-diagonal least
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Chapter 2 Experimental 2.2.3 Synthe
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Chapter 2 Experimental 2.2.7 Synthe
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Chapter 2 Experimental 2.2.11 Synth
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Chapter 2 Experimental 2.3Reference
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Chapter 3 The Wheel-Shaped Cu 20 in
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Chapter 3 The Wheel-Shaped Cu 20 3.
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Chapter 3 The Wheel-Shaped Cu 20 Fi
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Chapter 3 The Wheel-Shaped Cu 20 Cu
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Chapter 3 The Wheel-Shaped Cu 20 20
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Chapter 5 Organoruthenium POM (11)
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Chapter 6 U-peroxo-Polyoxometalate
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Chapter 8 Collaborative Work Chapte
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Chapter 8 Collaborative Work 8.2.1
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Chapter 9 Unpublished Results Figur
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Chapter 9 Unpublished Results solid
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Chapter 9 Unpublished Results Figur
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Chapter 9 Unpublished Results 9.1.3
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Chapter 4 - Jacobs University

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