Chapter 4 - Jacobs University

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<strong>Chapter</strong> 9 Unpublished Results Figure 9.68 TGA spectrum of 24a. 9.3.5.1 Results and discussion The polyanion [Hf 4 (OH) 6 (H 2 O) 4 (β-SiW 10 O 37 ) 2 ] 10- (24) (Figure 9.69) consists of two β - [SiW 10 O 37 ] 8- units sandwiching a [Hf 4 (OH) 6 (H 2 O) 4 ] 10+ cluster. All hafnium ions have a coordination number of seven. The Hf cluster has an inversion center, thus polyanion 24 has an idealized C i symmetry. 223
<strong>Chapter</strong> 9 Unpublished Results Figure 9.69 Polyhedral/ball and stick type structural representation of 24. Color scheme: Hf, Si and WO 6 units are shown by light green, green and red respectively. 224
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Synthesis, Structure and Properties
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"The greatest book of philosophy, w
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system, space group I4/m, unit cell
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Acknowledgements The accomplishment
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teaching, and Professor Maravanji S
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2.1.2 Single crystal X-ray diffract
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5.5 Conclusion…………………
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9.1.6.1 Results and discussion…
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9.3.5 Synthesis of K 12 [Hf 4 (µ 2
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Crespo………………………
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Figure 5.4 ORTEP view of the asymme
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Figure 9.6 31 P NMR of 7a in H 2 O/
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Figure 9.34 TGA spectrum of 17a…
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Figure 9.62 FTIR spectrum of 23a…
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Table 9.6 Crystal data and structur
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Chapter 1 Introduction heteropolyan
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Chapter 1 Introduction 1.3 Structur
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Chapter 1 Introduction C) Keggin a-
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Chapter 1 Introduction α-[P 2 W 18
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Chapter 1 Introduction [P 2 W 18 O
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Chapter 9 Unpublished Results Table
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