Chapter 4 - Jacobs University

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· Nuclear Magnetic Resonance (NMR): 1 H, 13 C, 29 Si, 11 B, 31 P, 51 V, 195 Pt, 183 W etc. · UV-vis, IR · TGA-DSC · Cyclic Voltagram · Dynamic Light Sacttaring(DLS) · Gas Chromatography Masters Student, Indian Institute of Technology, Bombay, India (2001-2003) · Synthesis of new phosphorus based hybrid ligands and the metal complexes using air/moisture sensitive chemicals under Argon atmosphere in schlenk-line. Characterization of these ligands and metal complexes 1 H and 31 P Nuclear Magnetic Resonance (NMR), UV-vis spectroscopy, cyclic voltamgram and X-ray crystallography. AWARDS AND FELLOWSHIPS 1. Recipient of DFG Fellowship for the PhD programme. 2. Recipient of Madhav Pandya Scholarship from IIT Bombay. 3. Qualified in Graduate Apptitude Test for Engineering (GATE) 2003 conducted by Indian Institute of Technology (IIT) (Reputed Technology based institutes of India). 4. Secured First Class in B.Sc. (Honors in Chemistry). 5. Obtained Gorg Bahadur Scholarship from Mahishadal Raj College for being topper in the B.Sc. final examination. 6. Recipient of GDCh Scholarship for ‘2nd EuCheMS Chemistry Congress’ Program 237
POSTER, ORAL PRESENTATION 1. Poster in the DFG conference on Magnetism of the transition metal complexes. Title “Synthesis and Magnetism of Multi-Transition Metal Containing Polyoxometalates ” May 2005 2. Poster in the DFG conference on Magnetism of the transition metal complexes. Title “Synthesis and Structural Characterization of Transition Metal Substituted Polyoxoanions and Investigation of Their Unique Magnetic Properties” January 2006 3. Poster and Oral presentation in the 9 th Northen-German Doctoral Student Colloquium of Inorganic Chemistry. Title “Synthesis and Structure of Multi- Transition Metal- Substituted Wheel Shaped Polyoxotungstates” October 2006 4. Poster in the DFG conference on Magnetism of the transition metal complexes. Title “Recent Developments on Magnetic Polyanions ” June 2007 5. Poster in 10 th Northen-German Doctoral Student Colloquium of Inorganic Chemistry. Title “16-Iron Ring Grafted Inside the 48-Tungsten-8-Phosphate Template Wheel ” Spetember 2007 6. Poster in DFG conference on Oxidation catalysis. Title “Transition Metal Substituted Polyanions and Their Oxidation Catalysis properties” Spetember 2007 7. Poster and Oral presentation in ‘2 nd Euchems Chemistry Congress’ in Torino, Italy. Title : Nucleation Process in the Cavity of a 48-Tungstophosphate Wheel resulting in a 16-Metal-Center Iron Oxide September 2008 238
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Synthesis, Structure and Properties
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"The greatest book of philosophy, w
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system, space group I4/m, unit cell
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Acknowledgements The accomplishment
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teaching, and Professor Maravanji S
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2.1.2 Single crystal X-ray diffract
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5.5 Conclusion…………………
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9.1.6.1 Results and discussion…
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9.3.5 Synthesis of K 12 [Hf 4 (µ 2
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Crespo………………………
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Figure 5.4 ORTEP view of the asymme
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Figure 9.6 31 P NMR of 7a in H 2 O/
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Figure 9.34 TGA spectrum of 17a…
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Figure 9.62 FTIR spectrum of 23a…
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Table 9.6 Crystal data and structur
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Chapter 1 Introduction heteropolyan
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Chapter 1 Introduction 1.3 Structur
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Chapter 1 Introduction C) Keggin a-
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Chapter 1 Introduction shows no suc
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Chapter 1 Introduction α-[P 2 W 18
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Chapter 1 Introduction Figure 1.7 B
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Chapter 1 Introduction [P 2 W 18 O
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Chapter 1 Introduction 1.5.3 Medici
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Chapter 1 Introduction (17) Evans,
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Chapter 1 Introduction (48) Mizuno,
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Chapter 1 Introduction (84) Isabell
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Chapter 2 were block-diagonal least
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Chapter 2 Experimental 2.2.3 Synthe
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Chapter 2 Experimental 2.2.7 Synthe
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Chapter 2 Experimental 2.2.11 Synth
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Chapter 2 Experimental 2.3Reference
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Chapter 3 The Wheel-Shaped Cu 20 in
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Chapter 3 The Wheel-Shaped Cu 20 3.
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Chapter 3 The Wheel-Shaped Cu 20 Fi
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Chapter 3 The Wheel-Shaped Cu 20 Cu
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Chapter 3 The Wheel-Shaped Cu 20 20
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Chapter 4 16-Iron Metal Center Nano
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Chapter 8 Collaborative Work Chapte
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Chapter 8 Collaborative Work 8.2.1
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Chapter 9 Unpublished Results Figur
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Chapter 9 Unpublished Results 9.1.3
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Chapter 9 Unpublished Results Table
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