Chapter 4 - Jacobs University

More documents

Recommendations

Info

<strong>Chapter</strong> 9 Unpublished Results Figure 9.42 Combination of polyhedral/ball-stick representation of 18. Color scheme: Ge, Y, C, H are represented by turquoise, yellow, blue and black respectively. Red polyhedra represent WO 6 units. 9.2.4.3 Solution NMR To complement our solid state XRD results on 18 with solution studies, we performed 1 H, 13 C, 89 Y and 183 W NMR at room temperature on 18a redissolved in H 2 O/D 2 O. 1 H NMR (Figure 9.43) spectrum exhibits the one signal at 1.82 ppm, and 13 C NMR (Figure 9.44) spectrum exhibit two signals 23.29 and 181.5 ppm and 89 Y NMR (Figure 9.46) spectrum 197
<strong>Chapter</strong> 9 Unpublished Results exhibits one signal at 50.63 ppm, and 183 W NMR (Figure 9.45) exhibit six signal at -83.67, - 87.77, -102.15, -118.89,-146.58 and -152.57 ppm which are fully consistent with the solid state structure. Figure 9.43 Solution 1 H NMR study of freshly prepared 18a mixture dissolved in H 2 O/D 2 O. 198
Page 1 and 2:
Synthesis, Structure and Properties
Page 3 and 4:
"The greatest book of philosophy, w
Page 5 and 6:
system, space group I4/m, unit cell
Page 7 and 8:
Acknowledgements The accomplishment
Page 9 and 10:
teaching, and Professor Maravanji S
Page 11 and 12:
2.1.2 Single crystal X-ray diffract
Page 13 and 14:
5.5 Conclusion…………………
Page 15 and 16:
9.1.6.1 Results and discussion…
Page 17 and 18:
9.3.5 Synthesis of K 12 [Hf 4 (µ 2
Page 19 and 20:
Crespo………………………
Page 21 and 22:
Figure 5.4 ORTEP view of the asymme
Page 23 and 24:
Figure 9.6 31 P NMR of 7a in H 2 O/
Page 25 and 26:
Figure 9.34 TGA spectrum of 17a…
Page 27 and 28:
Figure 9.62 FTIR spectrum of 23a…
Page 29 and 30:
Table 9.6 Crystal data and structur
Page 31 and 32:
Chapter 1 Introduction heteropolyan
Page 33 and 34:
Chapter 1 Introduction 1.3 Structur
Page 35 and 36:
Chapter 1 Introduction C) Keggin a-
Page 37 and 38:
Chapter 1 Introduction shows no suc
Page 39 and 40:
Chapter 1 Introduction α-[P 2 W 18
Page 41 and 42:
Chapter 1 Introduction Figure 1.7 B
Page 43 and 44:
Chapter 1 Introduction [P 2 W 18 O
Page 45 and 46:
Chapter 1 Introduction 1.5.3 Medici
Page 47 and 48:
Chapter 1 Introduction (17) Evans,
Page 49 and 50:
Chapter 1 Introduction (48) Mizuno,
Page 51 and 52:
Chapter 1 Introduction (84) Isabell
Page 53 and 54:
Chapter 2 were block-diagonal least
Page 55 and 56:
Chapter 2 Experimental 2.2.3 Synthe
Page 57 and 58:
Chapter 2 Experimental 2.2.7 Synthe
Page 59 and 60:
Chapter 2 Experimental 2.2.11 Synth
Page 61 and 62:
Chapter 2 Experimental 2.3Reference
Page 63 and 64:
Chapter 3 The Wheel-Shaped Cu 20 in
Page 65 and 66:
Chapter 3 The Wheel-Shaped Cu 20 3.
Page 67 and 68:
Page 69 and 70:
Chapter 3 The Wheel-Shaped Cu 20 Fi
Page 71 and 72:
Chapter 3 The Wheel-Shaped Cu 20 Cu
Page 73 and 74:
Page 75 and 76:
Chapter 3 The Wheel-Shaped Cu 20 20
Page 77 and 78:
Chapter 4 16-Iron Metal Center Nano
Page 79 and 80:
Page 81 and 82:
Page 83 and 84:
Page 85 and 86:
Page 87 and 88:
Page 89 and 90:
Page 91 and 92:
Page 93 and 94:
Chapter 5 Organoruthenium POM Chapt
Page 95 and 96:
Chapter 5 Organoruthenium POM 5.2 S
Page 97 and 98:
Chapter 5 Organoruthenium POM 5.3 X
Page 99 and 100:
Chapter 5 Organoruthenium POM 5.4 R
Page 101 and 102:
Chapter 5 Organoruthenium POM The f
Page 103 and 104:
Chapter 5 Organoruthenium POM On th
Page 105 and 106:
Chapter 5 Organoruthenium POM Figur
Page 107 and 108:
Chapter 5 Organoruthenium POM (11)
Page 109 and 110:
Chapter 6 U-peroxo-Polyoxometalate
Page 111 and 112:
Page 113 and 114:
Page 115 and 116:
Page 117 and 118:
Page 119 and 120:
Page 121 and 122:
Page 123 and 124:
Page 125 and 126:
Page 127 and 128:
Chapter 7 Pt-containing Polyoxometa
Page 129 and 130:
Page 131 and 132:
Page 133 and 134:
Page 135 and 136:
Page 137 and 138:
Page 139 and 140:
Page 141 and 142:
Chapter 8 Collaborative Work Chapte
Page 143 and 144:
Chapter 8 Collaborative Work 8.2.1
Page 145 and 146:
Chapter 9 Unpublished Results Figur
Page 147 and 148:
Chapter 9 Unpublished Results solid
Page 149 and 150: Chapter 9 Unpublished Results Figur
Page 151 and 152: Chapter 9 Unpublished Results 9.1.3
Page 163 and 164: Chapter 9 Unpublished Results There
Page 173 and 174: Chapter 9 Unpublished Results Table
Page 199: Chapter 9 Unpublished Results 9.2.4
Page 219 and 220: Chapter 9 Unpublished Results The d
Page 223 and 224: Chapter 9 Unpublished Results 23a (
Page 237 and 238: Curriculum Vitae SIB SANKAR MAL Dep
Page 239 and 240: EDUCATION PhD Jacobs University (20
Page 241 and 242: POSTER, ORAL PRESENTATION 1. Poster
Page 243 and 244: 6. “Two Iron-Containing Tungstoge
Page 245 and 246: Appendix
Page 247 and 248: 6. “Two Iron-Containing Tungstoge
Page 249 and 250: Appendix
Page 251 and 252:
6. “Two Iron-Containing Tungstoge
show all

Chapter 4 - Jacobs University

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?