Chapter 4 - Jacobs University

Figure 9.6 31 P NMR of 7a in H 2 O/D 2 O at room temperature……………………….………...147
Figure 9.7 FT-IR spectrum of 8a………………………………………………………………148
Figure 9.8 Polyhedral/ball and stick type structural representation of 8. Color scheme: Cu, P and
WO 6 units are shown by turquoise, blue and red respectively……………………149
Figure 9.9 FT-IR spectrum of 9a………………………………………………………………150
Figure 9.10 Thermogravimetric analysis of 9a………………………………………………...151
Figure 9.11 Polyhedral/ball and stick type structural representation of 9. Color scheme: Co, P
and WO 6 units are shown by pink, blue and red respectively……….……………154
Figure 9.12 FT-IR spectrum of 10a……………………………………………………………155
Figure 9.13 TGA analysis of 10a………………………………………………………………156
Figure 9.14 Polyhedral/ball and stick type structural representation of 10. Color scheme: Ni, P
and WO 6 units are shown by green, blue and red respectively………………..…157
Figure 9.15 FT-IR spectrum of 11a……………………………………………………………158
Figure 9.16 Thermogravimetric analysis of 11a……………………………………………….159
Figure 9.17 Polyhedral/ball and stick type structural representation of 11. Color scheme: Mn, P
and WO 6 units are shown by yellow, blue and red respectively………….………160
Figure 9.18 FT-IR spectrum of 12a……………………………………………………………161
Figure 9.19 Polyhedral/ball and stick type structural representation of 12. Color scheme: V, P
and WO 6 units are shown by yellow, blue and red respectively………......………162
Figure 9.20 FT-IR spectrum of 13a……………………………………………………………163
Figure 9.23 Polyhedral/ball and representation of 13. Color scheme: U, P and WO 6 units are
shown by green, blue and red respectively………………………………...……...164
Figure 9.22 FT-IR spectrum of 14a……………………………………………………………165
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