Chapter 4 - Jacobs University

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Chapter 9 Unpublished Results 9.3.7.2 Results and discussion The polyanion [Hf(BW 11 O 39 ) 2 ] 14- (26) (Figure 9.74) is composed of one hafnium and two units of [α-BW 11 O 39 ] 9- . The compound 26a was characterized in the solid state by single-crystal XRD, and IR. The hafnium atom is bridged between two lacunary Keggin species and the coordination number of Hf 4+ is eight. Figure 9.74 Polyhedral/ball and stick type structural representation of 26. Color scheme Hf, B and WO 6 units are shown by light green, green and red respectively. 233
Curriculum Vitae SIB SANKAR MAL Department of Chemistry Jacobs University Bremen, Campus Ring 8, D-28759, Bremen, Germany Email: s.mal@jacobs-university.de phone: +4917621910330 Personal Information: Citizenship Languages Known Gender Indian English, Hindi, Bengali (native) Male Date of Birth 10 th May, 1980 Qualifications Dedicated researcher, educated and worked in Indian Institute of Technology Bombay, India’s top- most institute. Strong background in synthesis of inorganic metal cluster, in particular Polyoxometalates. Have hands-on experience with various analytical instruments. Articulate in communicating complex ideas to others, including teaching (tutorials and labs) in general chemistry courses at Jacobs University Bremen, Germany. Professional activities include publishing research results in mainstream journals. Have sound computer knowledge. 234
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Synthesis, Structure and Properties
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"The greatest book of philosophy, w
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system, space group I4/m, unit cell
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Acknowledgements The accomplishment
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teaching, and Professor Maravanji S
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2.1.2 Single crystal X-ray diffract
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5.5 Conclusion…………………
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9.1.6.1 Results and discussion…
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9.3.5 Synthesis of K 12 [Hf 4 (µ 2
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Crespo………………………
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Figure 5.4 ORTEP view of the asymme
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Figure 9.6 31 P NMR of 7a in H 2 O/
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Figure 9.34 TGA spectrum of 17a…
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Figure 9.62 FTIR spectrum of 23a…
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Table 9.6 Crystal data and structur
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