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Chapter 4 - Jacobs University

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<strong>Chapter</strong> 9<br />

Unpublished Results<br />

Figure 9.46 89 YNMR study of freshly prepared 18a mixture dissolved in H 2 O/D 2 O.<br />

9.2.4.4 Conclusion<br />

We have isolated a dimeric yttrium containing polyoxometalate and we analyzed the compound<br />

by single crystal XRD, IR, NMR and TGA. The final compound was synthesized in a one-pot<br />

procedure in simple aqueous conditions and it crystallizes in the monoclinic crystal system<br />

(space group P2 1 /c).<br />

200

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