Chemistry 155 Introduction to Instrumental Analytical Chemistry

More documents

Recommendations

Info

Chem 155 Unit 1 Page 2 of 3131 Overview and Review ........................................................................................ 72 Propagation of Error ......................................................................................... 563 Introduction to Spectrometric Methods ............................................................ 654 Photometric Methods and Spectroscopic Instrumentation ............................... 865 Radiation Transducers (Light Detectors): ...................................................... 1006 Monochromators for Atomic Spectroscopy: ................................................... 1147 Photometric Issues in Atomic Spectroscopy .................................................. 1348 Practical aspects of atomic spectroscopy: ..................................................... 1489 Atomic Emission Spectroscopy ...................................................................... 15910 Ultraviolet-Visible and Near Infrared Absorption .......................................... 17411 UV-Visible Spectroscopy of Molecules ........................................................ 19212 Intro to Fourier Transform Infrared Spectroscopy ........................................ 20813 Infrared Spectrometry: ................................................................................. 23114 Infrared Spectrometry - Applications ............................................................ 24415 Raman Spectroscopy: .................................................................................. 25616 Mass Spectrometry (MS) overview: ............................................................. 27617 Chromatography .......................................................................................... 291Page 2 of 313
Chem 155 Unit 1 Page 3 of 3131 Overview and Review ........................................................................................ 71.1 Tools of Instrumental Analytical Chem. ................................................ 81.2 Instrumental vs. Classical Methods. ................................................... 121.3 Vocabulary: Basic Instrumental .......................................................... 131.4 Vocabulary: Basic Statistics Review .................................................. 141.5 Statistics Review ................................................................................ 151.6 Calibration Curves and Sensitivity ...................................................... 231.7 Vocabulary: Properties of Measurements .......................................... 241.8 Detection Limit ................................................................................... 251.9 Linear Regression .............................................................................. 311.10 Experimental Design: ....................................................................... 351.11 Validation – Assurance of Accuracy: ................................................ 431.12 Spike Recovery Validates Sample Prep. .......................................... 451.13 Reagent Blanks for High Accuracy: .................................................. 461.14 Standard additions fix matrix effects:................................................ 471.15 Internal Standards ............................................................................ 522 Propagation of Error ......................................................................................... 563 Introduction to Spectrometric Methods ............................................................ 653.1 Electromagnetic Radiation: ................................................................ 663.2 Energy Nomogram ............................................................................. 673.3 Diffraction ........................................................................................... 683.4 Properties of Electromagnetic Radiation: ........................................... 714 Photometric Methods and Spectroscopic Instrumentation ............................... 864.1 General Photometric Designs for the Quantitation of Chemical Species................................................................................................................. 874.2 Block Diagrams .................................................................................. 884.3 Optical Materials ................................................................................ 894.4 Optical Sources .................................................................................. 904.5 Continuum Sources of Light: .............................................................. 914.6 Line Sources of Light: ........................................................................ 924.7 Laser Sources of Light: ...................................................................... 935 Radiation Transducers (Light Detectors): ...................................................... 1005.1 Desired Properties of a Detector: ..................................................... 1005.2 Photoelectric effect photometers ...................................................... 1015.3 Limitations to photoelectric detectors: .............................................. 1035.4 Operation of the PMT detector: ........................................................ 1045.5 PMT Gain Equation: ......................................................................... 1056 Monochromators for Atomic Spectroscopy: ................................................... 1146.1 Adjustable Wavelength Selectors ..................................................... 1156.2 Monochromator Designs: ................................................................. 1166.3 The Grating Equation: ...................................................................... 1176.4 Dispersion ........................................................................................ 1206.5 Angular dispersion: .......................................................................... 1216.6 Effective bandwidth .......................................................................... 1236.7 Bandwith and Atomic Spectroscopy ................................................. 124Page 3 of 313
Page 1: Chem 155 Unit 1 Page 1 of 313Chemis
Page 5 and 6: Chem 155 Unit 1 Page 5 of 31312 Int
Page 7 and 8: Chem 155 Unit 1 Page 7 of 3131 Over
Page 9 and 10: Chem 155 Unit 1 Page 9 of 3131.1.2
Page 13 and 14: Chem 155 Unit 1 Page 13 of 3131.3 V
Page 15 and 16: Chem 155 Unit 1 Page 15 of 3131.5 S
Page 17 and 18: Chem 155 Unit 1 Page 17 of 313Confi
Page 19: Chem 155 Unit 1 Page 19 of 3131.5.4
Page 24 and 25: Chem 155 Unit 1 Page 24 of 3131.7 V
Page 34 and 35: Chem 155 Unit 1 Page 34 of 313See a
Page 36 and 37: Chem 155 Unit 1 Page 36 of 3136. Yo
Page 38 and 39: Chem 155 Unit 1 Page 38 of 3131.10.
Page 40 and 41: Chem 155 Unit 1 Page 40 of 3134. Wh
Page 42 and 43: Chem 155 Unit 1 Page 42 of 3137. Ho
Page 44 and 45: Chem 155 Unit 1 Page 44 of 313In ge
Page 46 and 47: Chem 155 Unit 1 Page 46 of 3131.13
Page 52 and 53:
Chem 155 Unit 1 Page 52 of 3131.15
Page 54 and 55:
Chem 155 Unit 1 Page 54 of 3131.15.
Page 56 and 57:
Chem 155 Unit 2 Page 56 of 3132 Pro
Page 58 and 59:
Chem 155 Unit 2 Page 58 of 313error
Page 60 and 61:
Chem 155 Unit 2 Page 60 of 313For a
Page 62 and 63:
Chem 155 Unit 2 Page 62 of 313Obvio
Page 64:
Chem 155 Unit 2 Page 64 of 313The p
show all

Chemistry 155 Introduction to Instrumental Analytical Chemistry

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?