1600 EPA Method 1600 SeriesBromodiphenyl EthersMethod 1614 Bromodiphenyl Ether MixturesResponding to the need for the analysis of polybrominated diphenyl ether (PBDE) congeners, the EPA has developed Method 1614. Method 1614 isrecommended for analysis of aqueous, solid, tissue, and multi-phase environmental samples. AccuStandard has the largest offering of synthesizedPBDEs, see Flame Retardant section for complete listing.Method 1614PBDEs Standard Solution for Accuracy & PrecisionAt stated conc. in Isooctane39 comps.BDE-AAP-A BDE-AAP-A-15XComponent $ 195 / 1 mL $ 750 / 1 mLng/mLµg/mL2-Bromodiphenyl ether (#1) 100 1.53-Bromodiphenyl ether (#2) 100 1.54-Bromodiphenyl ether (#3) 100 1.52,4-Dibromodiphenyl ether (#7) 100 1.52,4'-Dibromodiphenyl ether (#8) 100 1.52,6-Dibromodiphenyl ether (#10) 100 1.53,3'-Dibromodiphenyl ether (#11) 100 1.53,4-Dibromodiphenyl ether (#12) 100 1.53,4'-Dibromodiphenyl ether (#13) 100 1.54,4'-Dibromodiphenyl ether (#15) 100 1.52,2',4-Tribromodiphenyl ether (#17) 100 1.52,3',4-Tribromodiphenyl ether (#25) 100 1.52,4,4'-Tribromodiphenyl ether (#28) 100 1.52,4,6-Tribromodiphenyl ether (#30) 100 1.52,4',6-Tribromodiphenyl ether (#32) 100 1.52',3,4-Tribromodiphenyl ether (#33) 100 1.53,3',4-Tribromodiphenyl ether (#35) 100 1.53,4,4'-Tribromodiphenyl ether (#37) 100 1.52,2',4,4’-Tetrabromodiphenyl ether (#47) 100 1.52,2',4,5'-Tetrabromodiphenyl ether (#49) 100 1.52,3',4,4'-Tetrabromodiphenyl ether (#66) 100 1.52,3',4',6-Tetrabromodiphenyl ether (#71) 100 1.52,4,4',6-Tetrabromodiphenyl ether (#75) 100 1.53,3',4,4'-Tetrabromodiphenyl ether (#77) 100 1.52,2',3,4,4'-Pentabromodiphenyl ether (#85) 150 2.252,2',4,4',5-Pentabromodiphenyl ether (#99) 150 2.252,2',4,4',6-Pentabromodiphenyl ether (#100) 150 2.252,3,4,5,6-Pentabromodiphenyl ether (#116) 150 2.252,3',4,4',5-Pentabromodiphenyl ether (#118) 150 2.252,3',4,4',6-Pentabromodiphenyl ether (#119) 150 2.253,3',4,4',5-Pentabromodiphenyl ether (#126) 150 2.252,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 200 3.02,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 200 3.02,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 200 3.02,2',4,4',6,6'-Hexabromodiphenyl ether (#155) 200 3.02,3,4,4',5,6-Hexabromodiphenyl ether (#166) 200 3.02,2',3,4,4',5,6-Heptabromodiphenyl ether (#181) 250 3.752,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 250 3.752,3,3',4,4',5,6-Heptabromodiphenyl ether (#190) 250 3.75BrBrCommonly Occurring PBDE Congeners forPrecision and RecoveryBDE-COC$ 600 / 1 x 1 mLAt stated conc. in Isooctane14 comps.µg/mL2,2',4-Tribromodiphenyl ether (#17) 52,4,4'-Tribromodiphenyl ether (#28) 52,2',4,4'-Tetrabromodiphenyl ether (#47) 52,3',4,4'-Tetrabromodiphenyl ether (#66) 52,3',4',6-Tetrabromodiphenyl ether (#71) 52,2',3,4,4’-Pentabromodiphenyl ether (#85) 52,2',4,4',5-Pentabromodiphenyl ether (#99) 52,2',4,4',6-Pentabromodiphenyl ether (#100) 52,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 52,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 52,2',4,4’,5,6'-Hexabromodiphenyl ether (#154) 52,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 52,3,3',4,4’,5,6-Heptabromodiphenyl ether (#190) 5Decabromodiphenyl ether (#209) 25PBDE Congeners of Primary InterestBDE-CSM$ 225 / 1 x 1 mLAt stated conc. in Isooctane:Toluene8 comps.µg/mL2,4,4'-Tribromodiphenyl ether (#28) 202,2',4,4'-Tetrabromodiphenyl ether (#47) 202,2',4,4',5-Pentabromodiphenyl ether (#99) 202,2',4,4',6-Pentabromodiphenyl ether (#100) 202,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 202,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 202,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 20Decabromodiphenyl ether (#209) 200Calibration MixBDE-CMAt stated conc. in IsooctaneMatrix Spiking SolutionBDE-MSAt stated conc. in Isooctane$ 65 / 1 x 1 mL8 comps.$ 40 / 1 x 1 mL8 comps.BDE-CM BDE-MSµg/mL ng/mL2,4,4'-Tribromodiphenyl ether (#28) 2.5 12,2',4,4'-Tetrabromodiphenyl ether (#47) 2.5 12,2',4,4',5-Pentabromodiphenyl ether (#99) 2.5 12,2',4,4',6-Pentabromodiphenyl ether (#100) 2.5 12,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 2.5 12,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 2.5 12,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 2.5 1Decabromodiphenyl ether (#209) 25 10BrOBr200 AccuStandard is accredited to ISO/IEC 17025 and certified to ISO 9001
EPA Method 1600 SeriesPesticides and Herbicides1600Method 1618 Organo-halide, Organo-phosphorus Pesticides and Phenoxyacid Herbicides by Wide Bore Capillary Column GCMethod 1618 was developed by the Industrial Technology Division (ITD) within the United States Environmental Protection Agency’s (US EPA) Officeof Water Regulations and Standards (OWRS) to provide improved precision and accuracy of analysis of pollutants in aqueous and solid matrices inorder to determine the level of these pollutants in industrial discharges. Method 1618 is used with wide bore GC columns to analyze for organohalideand organo-phosphorus pesticides, phenoxy-acid herbicides and herbicide esters, polychlorinated biphenyls (PCBs) and other compoundsamenable to extraction and analysis by wide bore capillary column gas chromatography with halogen-specific and organo-phosphorus detectors.The chemical compounds in the AccuStandard mixtures that follow may be determined in waters, soils, sediments and sludges by this method. Themethod is a consolidation of EPA Methods 608, 608.1, 614, 615, 617, 622 and 701.Organochlorine PesticidesM-1618-1M-1618-1-PAKAt stated conc. in IsooctaneAldrin (100 ng/mL)Captan (200 ng/mL)Chlorobenzilate (500 ng/mL)Diallate (250 ng/mL)p,p’-DDE (200 ng/mL)p,p’-DDT (200 ng/mL)Endosulfan I (200 ng/mL)M-1618-2At stated conc. in Isooctaneα-BHC(100 ng/mL)β-BHC(100 ng/mL)δ-BHC(100 ng/mL)α-Chlordane (100 ng/mL)γ-Chlordane (100 ng/mL)Carbophenothion (1000 ng/mL)Captafol(200 ng/mL)p,p'-DDD (100 ng/mL)$ 75 / 1 x 1 mLSAVE 20% $ 300 / 5 x 1 mL14 comps.Endosulfan II (200 ng/mL)Endrin aldehyde (100 ng/mL)Heptachlor(100 ng/mL)Heptachlor epoxide (100 ng/mL)Lindane(100 ng/mL)Methoxychlor (200 ng/mL)Isodrin(100 ng/mL)$ 75 / 1 x 1 mL16 comps.Dichlone (100 ng/mL)Dieldrin(100 ng/mL)Endrin(100 ng/mL)Endosulfan sulfate (100 ng/mL)Endrin ketone (100 ng/mL)Mirex(100 ng/mL)PCNB(100 ng/mL)Trifluralin (200 ng/mL)Phenoxyacid HerbicidesM-8150M$ 40 / 1 x 1 mLM-8150M-PAKSAVE 20% $ 160 / 5 x 1 mL20 µg/mL each in Hexane 8 comps.2,4-D2,4-DB2,4,5-T2,4,5-TPM-8150M-2$ 15 / 1 x 1 mLM-8150M-2-PAKSAVE 20% $ 60 / 5 x 1 mL2.0 mg/mL in Hexane 2 comps.MCPASurrogate StandardsOrganochlorine PesticideM-1618-SSM-1618-SS-PAK2 µg/mL in AcetoneDibutylchlorendateDalaponDicambaDichlorpropDinosebMCPP$ 15 / 1 x 1 mLSAVE 20% $ 60 / 5 x 1 mLMethod 1618Organophosphate PesticidesM-1618-3At stated conc. in IsooctaneAzinphos methyl (100 ng/mL) MerphosCoumaphos (50 ng/mL) Methyl parathionDiazinon (100 ng/mL) MalathionDichlorvos (50 ng/mL) PhorateDimethoate (100 ng/mL) RonnelEPN(100 ng/mL) SulprofosEthyl parathion (100 ng/mL) TerbufosEthoprop (100 ng/mL) TetrachlorvinphosEthyl azinphos (100 ng/mL) TrichlorofonFensulfothion (200 ng/mL)M-1618-4At stated conc. in IsooctaneChlorfenvinphos (50 ng/mL) EthionChlorpyrifos (50 ng/mL) FamphurChlorpyrifos methyl (100 ng/mL) FenthionCrotoxyphos (200 ng/mL) LeptophosDichlorofenthion (100 ng/mL) MevinphosDemeton (400 ng/mL) NaledDioxathion (600 ng/mL) PhosmetDisulfoton (100 ng/mL) Sulfotep$ 90 / 1 x 1 mL19 comps.(200 ng/mL)(100 ng/mL)(100 ng/mL)(100 ng/mL)(100 ng/mL)(50 ng/mL)(100 ng/mL)(100 ng/mL)(100 ng/mL)$ 90 / 1 x 1 mL16 comps.(100 ng/mL)(200 ng/mL)(100 ng/mL)(100 ng/mL)(100 ng/mL)(100 ng/mL)(200 ng/mL)(50 ng/mL)Organophosphate PesticideM-1618-SP$ 20 / 1 x 1 mL2 µg/mL each in Acetone 2 comps.Tributyl phosphateTriphenyl phosphatePhenoxyacid HerbicideM-1618-SA$ 10 / 1 x 1 mL2 µg/mL in Acetone2,4-Dichlorophenyl acetic acidDecomposition SolutionM-1618D$ 15 / 1 x 1 mLM-1618D-PAKSAVE 20% $ 60 / 5 x 1 mLAt stated conc. in Acetone2 comps.p,p’-DDT (2.0 µg/mL)Endrin (1.0 µg/mL)GPC Calibration SolutionM-1618-GP-5ML$ 35 / 1 x 5 mLAt stated conc. in Acetone5 comps.Corn oil(300.0 mg/mL) Perylene (0.1 mg/mL)bis(2-Ethylhexyl)phthalate (15.0 mg/mL) Sulfur (0.5 mg/mL)Pentachlorophenol(1.4 mg/mL)SPE Cartridge Calibration SolutionM-1618-SE$ 10 / 1 x 1 mLM-1618-SE-PAKSAVE 20% $ 40 / 5 x 1 mL0.1 µg/mL in Acetone2,4,6-TrichlorophenolTel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 201
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