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EPA Method 1600 Series1600Method 1658 Phenoxy-Acid HerbicidesMethod 1658 consolidates several EPA wastewater methods used to determine Phenoxy-Acid Herbicides & Herbicide esters associated with theCWA, RCRA, & CERCLA; & other compounds amenable to extraction & analysis by wide-bore capillary column GC/ECD.M-1658-CAL-SET$ 75 / 3 x 1 mLAll solutions in Isooctane12 comps.Components Low Medium High(units in ng/mL) ( 1X ) ( 10X ) ( 100X )2,4-D 100 1,000 10,000Dalapon 50 500 5,0002,4-DB 200 2,000 20,0002,4-Dichlorphenylacetic acid 10 100 1,000(Surrogate)Dicamba 20 200 2,000Dichlorprop 100 1,000 10,000Dinoseb 50 500 5,000MCPA 5,000 50,000 500,000MCPP 5,000 50,000 500,000Picloram 50 500 5,0002,4,5-T 20 200 2,0002,4,5-TP 20 200 2,000Method 1658-1665Method 1659 Dazomet in Municipal & Industrial Wastewater by NPDMethod 1659 is used to determine Dazomet by base hydrolysis to Methyl Isothiocyanate (MITC) and subsequent determination of MITC by wide-borefused-silica capillary column gas chromatography with a Nitrogen Phophorus Detector (NPD).Recovery & Precision SolutionM-1659-RPS$ 10 / 1 x 1 mL25 µg/mL in AcetoneMethyl isothiocyanate (MITC)Matrix Spiking SolutionM-1659-MS$ 10 / 1 x 1 mL25 µg/mL in AcetoneDazometCalibration SolutionsM-1659-CAL-SET$ 25 / 3 x 1 mLM-1659-CAL-1X 0.2 mg/mL in Acetone 1 mLM-1659-CAL-5X 1.0 mg/mL in Acetone 1 mLM-1659-CAL-25X 5.0 mg/mL in Acetone 1 mLMethyl isothiocyanate (MITC)Method 1664 See Petrochemical or Inorganic SectionsMethod 1665 Semi-Volatile Organic Compounds Specific to the PMI by Isotope Dilution GC/MSThe following method series is designed to meet PMI (Pharmaceutical Manufacturing Industry) methods promulgated in 40 CFR part 136. It is usedto monitor the discharge of pollutants into surface waters. It can also be used to identify and measure purgeable and non-purgeable volatiles, semivolatiles,and certain organic pollutants specific to PMI discharge in water, soils, and municipal sludges.PMI Semi-Volatile SetM-1665-SETGPC Calibration SolutionM-1618-GP-5MLAt stated conc. in Acetone$ 35 / 1 x 5 mL5 comps.$ 320 / 5 x 1 mL(M-1618-GP-5ML, M-1653-TS, M-625-07-10X, M-1665, M-1665-LAB)PMI Stock StandardM-1665 $ 60 / 1 x 1 mL2000 µg/mL each in CH 2 Cl 2 6 comps.Corn oilbis(2-Ethylhexyl)phthalatePentachlorophenol(300.0 mg/mL)(15.0 mg/mL)(1.4 mg/mL)PeryleneSulfur(0.1 mg/mL)(0.5 mg/mL)AnilineN,N-DimethylacetamideN,N-DimethylanilineDimethylformamide2-PicolinePyridineInstrument Performance Check SolutionM-1653-TS$ 20 / 1 x 1 mL50 µg/mL in AcetonePMI Labeled Stock Standard (Not for individual sale)M-1665-LAB1 x 1 mL500 µg/mL each in CH 2 Cl 2 5 comps.DFTPPPMI Internal StandardM-625-07-10X2.0 mg/mL in CH 2 Cl 22,2'-Difluorobiphenyl$ 20 / 1 x 1 mLAniline-d 72-Picoline-d 7N,N-Dimethylaniline-d 11Pyridine-d 5Dimethylformamide-d 7Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 205

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