AccuStandard®

EPA Method 8000 SeriesReady-to-Inject Working Level Semi-Volatile StandardsMethod 8270C/D (Continued)Matrix Spike (SW 846)CLP-007-WL-50MLAt stated conc. in MeOH4-Chloro-3-methyl phenol2-Chlorophenol4-NitrophenolPentachlorophenolPhenolAcenaphtheneInternal Standard(200 µg/mL)(200 µg/mL)(200 µg/mL)(200 µg/mL)(200 µg/mL)(100 µg/mL)Prep Note$ 115 / 1 x 50 mL11 comps.1,4-Dichlorobenzene (100 µg/mL)2,4-Dinitrotoluene (100 µg/mL)N-Nitrosodi-n-propylamine (100 µg/mL)Pyrene(100 µg/mL)1,2,4-Trichlorobenzene (100 µg/mL)To help maximize instrument performance, add 10 µL of internal standard toa 1 mL sample extract.Z-014J$ 80 / 1 x 1 mLZ-014J-PAKSAVE 37% $ 250 / 5 x 1 mL4.0 mg/mL each in CH 2 Cl 2 6 comps.Method 8270 Surrogate Spiking SolutionM-8270-SS-R-WL-PAK$ 190 / 5 x 10 mLM-8270-SS-R-WL-VAP$ 300 / 10 x 10 mLAt stated conc. in CH 2 Cl 2 : MeOH (4:1)6 comps.2-Fluorobiphenyl (100 µg/mL) Phenol-d 5(200 µg/mL)2-Fluorophenol (200 µg/mL) Terphenyl-d 14 (100 µg/mL)Nitrobenzene-d 5 (100 µg/mL) 2,4,6-Tribromophenol (200 µg/mL)M-8270-SS-R$ 75 / 1 x 1 mLM-8270-SS-R-PAKSAVE 20% $ 300 / 5 x 1 mLAt stated conc. in CH 2 Cl 2 : MeOH (4:1)6 comps.2-Fluorobiphenyl (1000 µg/mL) Phenol-d 5(2000 µg/mL)2-Fluorophenol (2000 µg/mL) Terphenyl-d 14 (1000 µg/mL)Nitrobenzene-d 5 (1000 µg/mL) 2,4,6-Tribromophenol (2000 µg/mL)Prep NoteTo ensure extraction efficiency add, 1 mL of Surrogate to the sample.Method 8270-8275Naphthalene-d Acenaphthene-d 101,4-Dichlorobenzene-d 4 Phenanthrene-d 10Chrysene-d 128Perylene-d 12Benzidine SolutionM-625C-1-40X2.0 mg/mL in CH 2 Cl 2Benzidine$ 20 / 1 x 1 mLCLP Surrogate Spiking SolutionCLP-031-R-WL-25ML$ 110 / 1 x 25 mLCLP-031-R-WL-50ML$ 190 / 1 x 50 mLAt stated conc. in MeOH8 comps.2-Chlorophenol-d 4 (150 µg/mL) Nitrobenzene-d 5 (100 µg/mL)1,2-Dichlorobenzene-d 4 (100 µg/mL) Phenol-d 6(150 µg/mL)2-Fluorobiphenyl (100 µg/mL) p-Terphenyl-d 14 (100 µg/mL)2-Fluorophenol (150 µg/mL) 2,4,6-Tribromophenol (150 µg/mL)GC/MS Tuning SolutionM-625-TS$ 40 / 1 x 1 mLM-625-TS-PAKSAVE 20% $ 160 / 5 x 1 mL50 µg/mL each in CH 2 Cl 2 4 comps.Benzidinep,p'-DDTDFTPP GC/MS Tuning SolutionM-625C-3M-625C-3-PAK25 µg/mL in CH 2 Cl 2Decafluorotriphenylphosphine (DFTPP)Matrix Spike (3/90 SOW)CLP-007R-WL-50MLAt stated conc. in MeOH4-Chloro-3-methyl phenol2-Chlorophenol4-NitrophenolPentachlorophenolPhenolAcenaphthene(150 µg/mL)(150 µg/mL)(150 µg/mL)(150 µg/mL)(150 µg/mL)(100 µg/mL)Technical NoteDFTPPPentachlorophenol$ 20 / 1 x 1 mLSAVE 20% $ 80 / 5 x 1 mL$ 115 / 1 x 50 mL11 comps.1,4-Dichlorobenzene (100 µg/mL)2,4-Dinitrotoluene (100 µg/mL)N-Nitrosodi-n-propylamine (100 µg/mL)Pyrene(100 µg/mL)1,2,4-Trichlorobenzene (100 µg/mL)AccuStandard has found that benzidine degrades in multi-component semivolatilesolutions. For this reason, the benzidine in any calibration curveshould be used as a qualitative retention time marker. Reported hits forbenzidine should be quantitatively determined by analyzing a single benzidinesolution or by using the benzidine response observed in the Daily GC/MStuning solution.Method 8275A (Thermal Extraction/GC/FID/MS)Semi-Volatiles by Thermal ChromatographySemi-VolatilesM-8275 $ 60 / 1 x 1 mL1.0 mg/mL each in Acetone 17 comps.AldrinBenzo[k]fluorantheneBenzo[a]pyreneCarbazole4-Chloro-3-methylphenol1-Chloronaphthalene2-ChlorophenolDibenzothiophene2,4-DichlorophenolInternal Standard2,4-DinitrotolueneDiphenylamineFluoreneHexachlorobenzene4-MethylphenolNaphthalenePhenanthrenePyreneZ-014J$ 80 / 1 x 1 mLZ-014J-PAKSAVE 37% $ 250 / 5 x 1 mL4.0 mg/mL each in CH 2 Cl 2 6 comps.Naphthalene-d Acenaphthene-d 101,4-Dichlorobenzene-d 4 Phenanthrene-d 10Chrysene-d 128Perylene-d 12Alternate Source LineFor complete listing ofcompetitive 8270 see the QC SectionTel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 247