SPME Applications Guide - Labicom

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(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 824 Aroma volatiles Classification of wine samples according to origin and 85µm polyacrylate GC-MS in wine grape varieties on the basis of inorganic and organic 60 min trace analysis headspace American Lab, Oct. 1999, Vol. 31(20) 26-33 stirring Danzier, K., De La Calle Garcia, D., Thiel, G., Reichbacher, M., salt added 94 Trichloroanisole Analysis of Cork Taint in Wine and Cork Material at 100µm PDMS SIM-GC-MS in wine Olfactory Sub-Threshold Levels by SPME 20°C, 30 min J. Agric. Food Chem. 45: 1995-1997 (1997) Fisher, C., Fischer, U. salt added 385 Trichloroanisole Detection of Cork Taint in Wine Using Automated SPME in 100µm PDMS, GC-MS-SIM in wine Combination with GC-MS-SIM 85µm polyacrylate Book chapter 15: ACS Symposium Series 1999, Oxford 45°C, 25 min University Press, "Flavor Analysis Development in Isolation and Characterization" Butzke, C., Evans, T., Ebeler, S. headspace 377 Sulfides, disulfides Headspace SPME Analysis of Volatile Sulfides and 100µm PDMS, GC-FPD in wine Disulfides in Wine Aroma 85µm polyacrylate J. Chromatogr. A 808 (1998) 211-218 30°C, 15 min, salt Mestres, M., Busto, O., Guasch, J. headspace 406 Sulfides, disulfides Headspace SPME of Sulfides and Disulfides Using 75µm Carboxen/PDMS GC-FPD in wine Carboxen/PDMS Fibers in the Analysis of Wine Aroma 25°C, 30 min J. Chromatogr. A, 835 (1999) 137-144 headspace Mestres, M., Sala, C., Marit, M., Busto, O., Guasch, J. stirring, salt added 614 Benzothiazoles Analysis of benzothiazole in Italian wines using 65µm Carbowax/DVB GC-MS in wine SPME-GC-MS 15min @ 50°C J. Agric. Food Chem. (2000), 48(4), 1239-1242 headspace Bellavia, V., Natangelo, M., Fanelli, R., Rotilio, D. 363 Aroma volatiles Similarities in the Aroma Chemistry of Gewurztraminer 100µm PDMS GC-MS in wine Variety of Wines and Lychee (Litchi chinesis Sonn.) Fruit 15 min J. Agri. Food Chem. 1999, 47, 665-670 Ong, P., Acrees, T. headspace 427 Volatiles Fast Screening Method for Wine Headspace Compounds headspace in wine Using SPME and Capillary GC Technique Am. J. Enol. Vitic. (1998), 49(1), 100-104 Vas, G., Koteleky, K., Farkas, M., Ddobo, A., Vekey, K. 397 Aroma volatiles Determination of Volatile Aroma Compounds of 100µm PDMS GC-MS in wine Blaufrankisch Wines Extracted by SPME 10 min (headspace) J. Chromatographic Sci., Vol. 36, Oct. 1998, 505-510 Vas, G., Gal, L., Harangi, J., Dobo, A., Vekey, K. 1 hr (immersion) 457 Flavor volatiles Classification of wine samples according to origin 85µm polyacrylate GC-FID in wine and grape varieties on the basis of inorganic and 60-90 min organic trace analysis headspace Am. Laboratory, Oct. 1999, Vol. 31, No. 20, 26-34 Satr.salt Danzier, K, DeLaCalle Garcia, D, Thiel, G., Reichenbacher, M 458 Aroma volatiles Examination of aroma production kinetics of 100µm PDMS GC-FID in wine different commercial wine yeast in fermenting 10 min muscat ottonel wines with the help of SPME headspace sampling and fast GC analysis Acta Aliment, (1999), 28(2), 133-140 Vaes, W., Blechschmidt, I., Kovacs, T., Vekey, K. headspace Ambient temperature, unless otherwise indicated. 12
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 582 Aroma volatiles Improvement of the chemometric variety characterization of 85µm polyacrylate GC-EMIS in wine wines by improving the detection limit for aroma compound 3 hr. , headspace J-High-Resolut-Chromatogr. Jun 1999; 22(6): 322-326 Weber,-J; Beeg,-M; Bartzsch,-C; Feller,-K-H; De-la-Calle-Garcia,-D; Reichenbaecher,-M; Danzer,-M NaCl added 459 Aroma volatiles Determination of volatiles from red wines made 100µm PDMS GC-EIMS in wine by carbonic maceration using SPME technique Acta Aliment, 1999, 28(1), 95-101 Vas, G., Loerincz, G. 10 min headspace 559 Aroma volatiles Monitoring Toasting Intensity of Barrels by 100µm PDMS GC-FID from toasted oak Chromatographic Analysis of Volatile 30 min @ 22°C compounds from Toasted Oak Wood J. Agric. Food Chem, 1999, 47, 4310-4318 headspace Chatonnet, P., Cutzach, I., Pons, M., Dubourdieu, D. 460 Polyphenolics Assembly tests of "Nero d'Avola" with wines GC-MS in red wine derived from an allocthonous cultivar: headspace study of polyphenolic and aromatic profiles. Italian Ind. Bevande (1999), 28(160), 119-126 Papucci, A, Monte, L., D'Agostino, S, Aozzino, P., Avellone, G 775 Esters Monitoring ester formation in grape juice fermentations 100µm PDMS GC-MS in grape juice using SPME coupled with GC-MS 1 hr. J. Agric. Food Chem (2001) 49(2), 589-595 headspace Vianna, E; Ebeler, S. 315 Styrene Determination of Styrene in Wine by SPME and GC-MS GC-MS in wine Mitt. Klosterneuburg 47 (4): 117-123 (1997) Flak, W., Tscheik, G. 311 Methylisocyanate SPME Analysis of Methyl Isothiocyanate in Wine 65µm Carbowax/DVB GC-FID, NPD in wine J. Agric. Food Chem. 45 (8): 3092-3094 (1997) 30 min Gandini, N., Riguzzi, R. headspace salt added 366 Diacetyl Analysis of Diacetyl in Wine Using SPME -GC-MS 60µm Carbowax/DVB GC-MS in wine J. Agric Food Chem. 1999, 47, 612-617 24°C, 5 min Hayasaka, Y., Bartowsky, E. headspace salt added 316 Pesticides Determination of Pesticide Residues in Wine by SPME and GC-MS in Wine GC/MS for Consumer Risk Assessment Food Addit. Contam. 15 (3): 280-287 (1998) Vitali, M., Guidotti, M., Giovinazao, R., Cendrone, O. 615 Pesticide residue Applications of SPME to the Analysis of 100µm PDMS, GC-ECD on vegetables Pesticide Residues in Vegetables 60µm Carbowax/DVB GC-NPD Pest. Manag Sci 56: 618-636 (2000) Volante, M.,Pontello, M., Volante, L. Cattaneo, M., Bianchi, M., Bianchi, M., Colzani, L. 50 min 774 Pesticide residue Study on the method of SPME coupled to GC for on vegetables determination of organophosphorus pesticide residue in vegetables. Ziran Kexueban (2000) 39(4), 509-515 Chen, W; Hou, X; Zhang, L; Lin, H; Pan, Ji (in Chinese) 432 Pesticides in Some Applications of SPME in the Analysis of food Pesticide Residues in Food J. Environ. Sci. Health, Part B (1998), B33 (3), 279-292 Volante, M.,Cattaneo, M., Bianchi, M., Zoccola, G. Ambient temperature, unless otherwise indicated. 13
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