SPME Applications Guide - Labicom

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(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 461 Pesticides SPME of pesticide residues from strawberries 100µm PDMS on strawberries Food Addit. Contam. (1999), 16(3), 111-117 45 min @ 25°C Hut, R., Henniont, B., Urrutyt, L., Monturyt, M. 783 Pesticides SPME coupled with HPLC: a complementry technique to SPME 60µm PDMS/DVB LC-UV on strawberries GC for the analysis of pesticide residues in strawberries 45 min @ 25°C Food Addit. Contam. (2000), 17(11), 915-923 headspace Wang, Z.; Hennion, B.; Urruty, L.; Montury, M. 462 Organophosphorus Validation of a SPME method for the 100µm PDMS GC-FPD pesticides in determination of organophosphorus pesticides 3 min fruit/fruit juices in fruits and fruit juice immersed J. Chromatogr. A (1999), 843(1), 35-42 Simplicio, A, Vilas Boas, L. 929 Organophosphorus Determination of organophosphorus pesticides in honeybees 85µm Polyacrylate GC-NPD pesticides in after solid phase microextraction 45min @ 25°C honeybees J. Chromatogr. A (2001), 922(1-2) 257-265 immersed Fernandez, M., Padron, C., Marconi, L., Colombo, R. Ghinie, S. stirred Sabatini, A, Girotti, S. 463 Organochlorine & A Systematic Approach to Optimize SPME organophosphorus determination of Pesticides in Ethanol/Water in water/ethanol mixtures used as Food Simulates Anal. Chem. (1999), 71(13), 2417-2422 Batlle, R, Sanchez, C., Nerin, C. 616 Volatiles Evidence for selectivity of absorption of volatile organics 30µm PDMS GC-MS in water compounds by PDMS SPME fiber 60min J. Chromatogr. A,(2000) 885, 457-464 Niedziella, S., Rudkin, S., Cooke, M. headspace 317 Aroma volatiles Analysis of Aroma Release During Microwave Heating 60µm Carbowax/DVB GC-FID in water traps J. Agric. Food Chem. 45 (11): 4388-4392 (1997) 10 min Roberts, D., Pollien, R. immersion, stirring 435 Aroma volatiles SPME Associated with Microwave Assisted Extraction of in food products Food Products J. High Resolut. Chromatogr. (1997), 20(4), 213-216 Wang, Y., Bonilla, M., McNari, H., Khaled, M. 318 N-nitrosamines Rapid Semi-Quantitative Estimation of N-Nitrosodibulylamine 85µm polyacrylate GC-thermal in smoked hams and N-Nitrosodibenzylamine in Smoked Hams by SPME 10 min energy or MS Followed by GC-Thermal Energy Analysis headspace J. Chromatogr. A 788(1+2): 131-140 (1997) stirring Sen, N., Seaman, S., Page, B. salt added 348 Flavor volatiles Application of SPME to the Analysis of Warmed 100µm PDMS GC-MS in beef Over Flavor in Beef 35°C, 10 min Poster Paper, IFT 1999 Gruen, I., Fernando, L., Mobley, S. headspace 890 Atrazine in Ethanol-modified subcritical water extraction combined 60µm Carbowax/DVB GC-MS beef with SPME for determining atrazine in beef kidney. J.Ag Food Chem (2001) 49(5) 2175-2180 Curren, Meredith S. S.; King, Jerry 30MIN @ 25°c 617 Aroma compounds Two-fiber SPME combined with GC-MS for the analysis of Carboxen/PDMS. GC-MS in cooked pork volatile aroma compounds in cooked pork Carboxen/DVB/PDMS J. Chromatogr. A 905(2000), 233-240 Elmore, J. Mottram, D., Hierro, E. 30 min @ 60°C 618 Hexanal, pentanal A comparison of SPME fibers for measurement of hexanal Carboxen/DVB/PDMS GC-FID in cooked turkey and pentanal in cooked turkey Food Chem Feb. 2000, 68(3), 339-345 Brunton, N., Cronin, D, Durcan, R., Monahan, F. 20 min, headspace @ 40°C Ambient temperature, unless otherwise indicated. 14
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 924 Volatiles SPME as a tool for studying volatile compounds in frog skin in frog skin Chemistry and Ecology 2000 Smith, B, Zini, C., Pawliszyn, J. Tyler, M., Hayasaka, Y, Williams, B., Caramao, E. 423 Volatiles Comparison of Volatile Analysis of Lipid-Containing and in meat Meat Matrices by SPME and SFE ACS Symp. Ser. (1998), 705 (Flavor Analysis), 107-115 Snyder, J., King, J., Zhang, Z. 786 Volaitle amines New method for the rapid determination of volatile GC-FID, NPD in fish substances: The SPME-direct method. Part II. Determination of the freshness of fish headspace Sens Actuators, B Chem (2001) 72(3), 204-207 Bene, A.; Hayman, A.; Luisier, J.L.; Reynard, E.; Villettaz, J 619 Volatiles from SPME/GC of Salmonella-Infected Beef 75µm Carboxen/PDMS GC-FID salmonellas infected J Agric Food Chem, 2000, 48, 2253-2259 10 min beef Ogihara, H., Horimoto, Y., Hai, Z., Skura, B., Nakai, S. 25% NaCl 393 Volatiles from Use of Digital Aroma Technology and SPME GC-MS to 100µm PDMS GC-MS processed poultry compare Volatile compounds Produced by Bacteria 30 min @ 37°C isolated from Processed Poultry headspace J. Sci. food Agric. 1998, 78, 343-348 Arnold, J., Senter, S. stirred 862 Allyl isothiocyanate Formation of allyl isothiocyanate from sinigrin in the GC-MS in rats digestive tract of rats monoassociated with a human colonic strain of Bacteroides thetaiotaomicron FEMS Microbiology Letters (2001) 197(1) 99-103 Rabot, S; Duguay, A; Elfoul, L; Khelifa, N; Quinsac,A; Rimbault, A headspace 253 Putrescine, An Electrodeposition Device for the Determination of carbon fibers HPLC cadaverine in Putrescine and Cadaverine by High-Resolution GC 0-60 min, immersion (C18 column) borate buffer solution J. High Resolut. Chromatogr. 19 (5): 294-297 (1996) stirring Conte, E., Miller, D. pH 8 620 Hexanal, pentanal Shelf-life prediction of processed milk by SPME -MS and 75µm Carboxen/PDMS GC-MS metabolites in milk multivariate analysis 20min. @ 50°C J. Agric Food chem (2000), 48(8), 3470-3475 Marsili, R. headspace 386 Oxidative byproducts Comparison of SPME and Dynamic Headspace Methods for 75µm Carboxen/PDMS GC-MS in milk the GC-MS Analysis of Lighted Induced Lipid Oxidation 45°C, 15 min Products in Milk headspace J. Chromatogr. Sci. 1999, 37, 17-23 Marsili, R. salt added 372 Off-flavors SPME-MS-MVA as an Electronic Nose for the Study of 75µm Carboxen/PDMS GC-MS in milk Off-Flavors in Milk 45°C, 12 min J. Agric. Food Chem. 1999, 47, 648-654 Marsili, R. headspace 621 Chlorinated organics Application of SPME for the rapid analysis of chlorinated GC-ECD in breast milk organics in breast milk Fresenius, J. Anal.Chem, Jan 2000, 366(1), 106-111 Rohrig, L., Meisch, H. 749 Acetaldehyde Flavor threshold for acetaldehyde in milk, chocolate milk, and 75µm Carboxen/PDMS GC-FID in milk & water spring water using SPME-GC for quantification 45°C, 15 min J.Agric.FoodChem 2001, 49(3), 1377-1381 headspace vanAardt, M., Duncan, S., Bourne, D., Marcy, J., Long, T., Hackney, C., Heisey, C., salt added Ambient temperature, unless otherwise indicated. 15
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