SPME Applications Guide - Labicom

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(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1500 Volatiles in orange juice Variables affecting SPME headspace analysis of orange juice volatiles 1516 Voltiles in pineapple 1517 Aroma compounds in wine 1520 Volatiles in smoked fish 1521 1525 1526 Aroma volatiles in cantaloupe Fatty acid ethyl ethers in rum Volatiles in alcoholic fermentation of grapes 1534 Butyltin in wines 1535 Ethylphenol in wine Abstracts of Papers American Chemical Society (2002) 224(1-2), AGFD 49 Goodrich, Renee M.; Bryan, Charles R.; Braddock, Robert J. Volatile compounds in hydrolyzed pineapple (Ananas comosus L. Merryl) perola variety and clarified pasteurized juices obtained by solid-phase microextraction Alimentaria (2002) 39(333), 129-132 de Carvalho, Lucia Maria Jaeger; da Silva, Carlos Alberto Bento; de Oliveira Godoy, Ronoel Luiz; Abadio, Fernanda Dias Bartolomeu; Figueira, Jose Americo A. Headspace solid-phase microextraction gas chromatography/mass spectrometry in the analysis of the aroma constituents of 'Cannonau of Jerzu' wine. Rapid Communications in Mass Spectrometry (2002) 16(11), 1086-1091 Podda, Gianni; Begala, Michela; Corda, Luciana; Fedrigo, Maria Anna; Traldi, Pietro Volatile components of raw and smoked black bream (Brama raii) and rainbow trout (Oncorhynchus mykiss) studied by means of solid phase microextraction and gas chromatography/mass spectrometry. Journal of the Science of Food and Agriculture (2002) 82(9), 945-952 Guillen, Maria D.; Errecalde, Maria C. Effect of storage on some volatile aroma compounds in fresh-cut cantaloupe melon. Journal of Agricultural and Food Chemistry (2002) 50(14), 4043-4047 Lamikanra, Olusola; Richard, Olga A. Headspace solid-phase microextraction of higher fatty acid ethyl esters in white rum aroma. Journal of Chromatography A (2002) 954(1-2), 51-57 Guasch, J.; Busto, O.; Marti, M. P.; Mestres, M.; Perez, J.; Pino, J. Investigation of volatiles evolution during the alcoholic fermentation of grape must using free and immobilized cells with the help of solid phase microextraction ( SPME ) headspace sampling. Journal of Agricultural and Food Chemistry (2002) 50(13), 3840-3848 Komaitis, Michael; Kanellaki, Maria; Koutinas, Athanasios; Mallouchos, Athanasios Journal of Agricultural and Food Chemistry (2002) 50(13), 3810-3817 Ducruet, Violette; Feigenbaum, Alexandre; Gratadoux, Jean Jacques; Jouquand, Celine; Lecanu, Laurent Headspace solid-phase micro-extraction gas chromatography-mass detection method for the determination of butyltin compounds in wines. Analytica Chimica Acta (2002) 458(1), 231-239 Azenha, Manuel; Vasconcelos, Maria Teresa Determination of ethylphenol compounds in wine by headspace solid-phase microextraction in conjunction with gas chromatography and flame ionization detection. Analytica Chimica Acta (2002) 458(1), 111-117 Nepveu, Francoise; Gastine, Valerie; Monje, Marie-Carmen; Privat, Christelle Ambient temperature, unless otherwise indicated. 30 65um PDMS DVB GC-MS GC-MS headspace GC-MS headspace GC-MS 85um Polyacrylate, NaCl added, 40mins. GC-FID
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1537 Ethyl carbamate in wine 1539 1541 1542 1546 1555 3-alkyl-2methoxypyrazines in wine Butyltin in Portuguese wines Volatiles in Spanish honey Short-chain fatty acids in cane and beet sugars Sulfur compounds in wines Determination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometry. American Journal of Enology and Viticulture (2002) 53(1), 60-63 Zoecklein, B. W.; Whiton, R. S. Headspace solid-phase microextraction analysis of 3-alkyl-2methoxypyrazines in wines. Journal of Chromatography A (2002) 953(1-2), 1-6 Guasch, J.; Busto, O.; Marti, M. P.; Mestres, M.; Sala, C. 65um Carbowax DVB, 30mins, headspace GC-MS Butyltin compounds in Portuguese wines. GC-MS Journal of Agricultural and Food Chemistry (2002) 50(9), 2713-2716 Azenha, Manuel; Vasconcelos, Maria Teresa Analysis of volatiles from Spanish honeys by solid-phase microextraction and gas chromatography-mass spectrometry. Journal of Agricultural and Food Chemistry (2002) 50(9), 2633-2637 Tadeo, Jose L.; Calvo, Rosa M.; Perez, Rosa A.; Sanchez-Brunete, Consuelo Semiquantitative determination of short-chain fatty acids in cane and beet sugars. Journal of Chromatographic Science (2002) 40(3), 127-132 Grimm, Casey C.; Batista, Rebecca B.; Godshall, Mary An Application of headspace solid-phase microextraction to the determination of sulphur compounds with low volatility in wines. Journal of Chromatography A (2002) 945(1-2), 211-219 Mestres, M.; Busto, O.; Guasch, J. 75um Carboxen PDMS, 70 degrees C, 30mins. GC-MS 50/30um DVB/Carboxen PDMS GC-MS 1196 Analysis of chemical constituents of capsicol by GC-MS. Fenxi Ceshi Xuebao (2003) 22 (1), 67-70. Zhu, X. L.; Liu, B. Z.; Zong, R. W.; Yun, G. O. GC-MS 1211 1243 Nicotine in cigarettes 1274 1314 Identification of 2-bromo-3,4,5,6-tetrachloroaniline and its quantification in the color additives D&C Red Nos. 27 and 28 (phloxine B) using solid-phase microextraction and gas chromatography-mass spectrometry GC-MS Journal of Chromatography A (2003) 1005 (1-2), 143-153. Andrzejewski, Denis; Weisz, Adrian Determination of nicotine and other minor alkaloids in international cigarettes by solid-phase microextraction and gas chromatography/mass spectrometry. GC-MS Analytical Chemistry (2003) 74 (19), 4878-4884. Wu, W. J.; Ashley, D. L.; Watson, C. H.* Determination of the volatile constituents of Chinese Coriandrum sativum L. by gas chromatography-mass spectrometry with solid-phase microextraction. 100 um PDMS, 250 C, 3 minutes GC-MS Chromatographia (2003) 57 (5-6), 357-361. Deng, C. H.; Song, G. X.; Hu, Y. M.*; Zhang, X. M. Aroma dilution method using GC injector split ratio for volatile compounds extracted by headspace solid phase microextraction. GC-O Food Chemistry (2003) 83 (1), 151-158. Lee, Hyong Joo; Kim, Kyoung Heon; Kim, Tae Hwan; Kim, Young-Suk; Lee, Sang Mi; Oh, Sangsuk Ambient temperature, unless otherwise indicated. 31
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