SPME Applications Guide - Labicom

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(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 854 Volatiles in Analysis of the volatile components in vanilla extracts and 85µm polyacrylate GC-MS vanilla extracts flavourings by SPME and gas chromatography J Ag Food Chem (2000) 48(12), 5802-5807 Sostaric, T.; Boyce, M. C.; Spickett, E. E. 40min @20°C 829 Volatiles of Analysis of headspace compounds of distillers grains using 75µm Carboxen/PDMS GC-MS distillers grains SPME in conjunction with GC/MS and TGA. 60min J Cereal Sci. (2001) 33(2), 223-229 Staff, C., Biswas, S. headspace 878 Essential oils in SPME of hop volatiles Potential use for determination and 100µm PDMS GC-MS hops verification of hop varieties 30min @ 70°C J. Chromatogr A 918 (2001) 159-167 Kovacevic, M., Kac, M. headspace 63 Essential oils in Determination of Essential Oils in Hops by Headspace SPME 100µm PDMS GC-FID hops J. Agric. Food. Chem, 44: 1768-1772 (1996) Field, J., Nickerson, G., James, D. Heider, C. 50°C, 4 hr 605 Essential oils Production of Yarrow (Achillea millefolium L.) in Norway: 100µm PDMS GC-MS in yarrow Essential Oil Content and Quality 40min @ 50°C J. Agric. Food Chem, (2000) 48 No,12, 6205-6209 Rohloff, J., Skagen, E., Steen, A., Iversen, T. headspace 221 Essential oils in A Comparison of Selected Analytical Approaches to the 100µm PDMS GC-MS Virginia cedar oil Analysis of an Essential Oil 10-120 sec Flavour and Fragrance Journal 12 (1): 1-8, (1997) Coleman, W., Lawrence, B. headspace 396 Essential oils in Automatic Injection SPME-Chiral-GC-MSD Analysis of 7µm PDMS GC-MS Virginia cedar oil Essential Oils 6 sec J.Chromatographic Sci., Vol. 36, Dec. 1998, 575-578 headspace Coleman, W., Perfetti, T., Lawrence, B. stirring 444 Volatiles in Identification of Volatile Compounds in Sunflower Oil 100µm PDMS GC-MS sunflower oil by Headspace SPME and Ion-Trap GC/MS J. High Resolut. Chromatgr. (1998), 46(7), 2744-2747 Keszler, A., Heberger, K., Gude M. 841 Volatiles in Mechanism of volatile compound production during storage 100µm PDMS GC-MS sunflower oil of sunflower oil 40 min @ 25°C J Ag Food Chem. (2000) 48(12), 5981-5985 Keszler, A., Kiska, T. Nemeth, A.. headspace 569 12 Aldehydes Influence of extraction parameters and medium on 100µm PDMS GC-MS in sunflower oil/water efficiency of SPME sampling in analysis of aliphatic aldehydes 30 min @ 40°C J-Chromatogram-A. 11 Jun 1999; 845(1-2): 337-347 Keszler,-A; Heberger,-K headspace 447 Xylene Determination of trace xylene in contaminated palm 100µm PDMS GC-FID in palm oil oil by SPME and capillary GC 1 min. 60°C Fenxi Huaxue (1999), 27(6), 676-678 headspace Chen, W., Guo, C., Hu, C. 803 Volatiles Volatile compounds of virgin olive oil evaluated by SPME in olive oil An application in the discrimination of virgin olive oils according to the cultivar and area Proceedings of the Phytochemical Society of Europe (2000) Vol. 46, 211-220 Servili, M; Montedoro, G; Selvaggini, R; Taticchi, A 577 Dimetyl disulfide & Volatile reduced sulfur compounds in butter by SPME 85µm polyacrylate GC-EID methanethiol J-Dairy-Res. Feb 1999; 66(1): 115-123 10 min. @ 30-35°C in butter Shooter,-D; Jayatissa,-N; Renner,-N Ambient temperature, unless otherwise indicated. 4
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 338 Benzene, toluene Determination of benzene & toluene in vegetable HPLC in vegetable oil oil by SPME/HPLC headspace J. Commod. Sci. (1999), 38(1), 3-14 Giuffrida, R., Clasadonte, M., Zerbo, A. 606 Volatiles Headspace SPME use for the Characterization of volatile Carboxen/DVB/PDMS GC-FID in vegetable oil compounds in vegetable oils of different sensory quality 20-60°C J. Agric Food Chem, (2000), 48(6), 2360-2367 headspace Jelen, H., Obuchowska, M., Zawirska-Wojtasiak, R. 885 Steroisomers Different stereoselectivity in the reduction of pulegone GC-MS Pulegone enantiomers by Mentha species Planta Medica (2001) 67(3) 260-262 Mosandl, A.; Beck, T.; Fuchs, S. 106 Flavors in Characterization of Beer Samples Using SPME-GC Analysis 100µm PDMS GC-FID beer Supelco Reporter Vol. 16, #4, pg. 7 Vas, G. 10 min 607 Sulfur compounds Determination of sulfur compounds in beer using headspace 65µm Carboxen/PDMS GC-FPD in beer SPME and GC analysis with pulsed FPD detector 32min @45°C J. Chromatogr. A. (2000), 872(1+2), 203-213 Hill, P., Smith, R. headspace 100 Flavors Characterization of Commercial Vodkas by SPME-GC/MS 100µm PDMS GC-MS in vodka J. Sci. Food Agric. 70: 380-388 (1996) Ng, L., Hupe, M., Harnois, J., Moccia, D. 1 hr 202 Methylcyclopendienyl Determination of Methylcyclopendienyl Manganese Tricarbonyl manganese in Beverages by SPME tricarbonyl Food Addit. Contam. 14 (3): 301-307 (1997) in beverages Forsyth, D., Dusseault, L. 395 Aroma volatiles Determination of Fresh Onion (Allium Cepa L) Volatiles 100µm PDMS GC-MS in onion by SPME Combined with GC/MS 1 min Z Lebedsm Unters Forsch A (1998) 207: 39-43 Jarvedpaa, E., Zhung, Z., Huopalahti, R., King, J. headspace 799 Aroma volatiles Possible advantage of various sample transfer techniques 100µm PDMS, GC-MS in onion for fast GC-MS analysis of true onion volatiles polyacrylate J. Chromatogr. A. (2000), 896(1+2), 117-124 2min, headspace Arnault, I.; Mondy, N.; Cadoux, F.; Auger, J. 954 Fatty acids, Analysis of free fatty acids in whey products by SPME 30µm PDMS GC-FID in whey products J Agric Food Chem, 2001, 49, 3993-3998 40 min @ 110°C Tomaino, R., Parker, J., Larick, D. headspace 816 Fatty acids, lactones Determination of free fatty acids and lactones in cheese in cheese by solid phase microextraction (SPME) Aust. J. Dairy Technol.,(1998), 53(2), 140 Wijesundera, C., Drury, L., Walsh, T. 101 Flavors SPME for Cheese Volatile Compound Analysis 100µm PDMS, GC, GC-MS in cheese J. Food Sci. 61: 1118-1129 (1996) polyacrylate Chin, H., Bernhard, R., Rosenberg, M. 60°C, 20 min 788 Volatilse Solid-Phase Microextraction-Mass Spectrometry: A New GC-MS in cheese Approach to the Rapid Characterization of Cheeses Anal. Chem (2001) 73(5), 1030-1036 Peres, Christophe; Viallon, Christine; Berdague, Jean-Louis 826 Volatiles in Use of preconcentration techniques applied to a Mass GC-MS Emmital cheese Spectrometer based "Electronic Nose". Analusis (2000) 28(8), 743-749 Bosset, J.; Escher, F.; Schaller, E.; Zenhausern, S.; Zesiger, T. Ambient temperature, unless otherwise indicated. 5
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