SPME Applications Guide - Labicom

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(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1348 Fungicides in wine 1356 Volatiles in wines 1362 1367 1368 Cyclopiazonic acid in cheese. Off flavours in orange juice. Flavour compounds in wine. Solid-phase microextraction-gas chromatographic-mass spectrometric method for the determination of the fungicides cyprodinil and fludioxonil in white wines. Journal of Chromatography A (2002) 942(1-2), 41-52 Simal Gandara, J.; Cancho Grande, B.; Rial Otero, R.; Yague Ruiz, C. Classification of Nebbiolo-based wines from Piedmont (Italy) by means of solid-phase microextraction-gas chromatography-mass spectrometry of volatile compounds. Journal of Chromatography A (2002) 943(1), 123-137 Aceto, Maurizio; Marengo, Emilio; Maurino, Valter 50/30um DVB/Carboxen PDMS GC-MS GC-MS Determination of cyclopiazonic acid in cheese samples using solid-phase microextraction with high performance liquid chromatography. Food Chemistry (2001) 75(2), 249-254. Zambonin, C. G.; Monaci, L.; Aresta, A. * Carbowax/TPR HPLC 2-Methyl-3-furanthiol and methional are possible off-flavours in stored orange juice: aroma-similarity, NIF/SNIF GC-Olfactometry, and GC analyses. GC-O Journal of Agricultural and Food Chemistry (2001) 49(11), 5425-5432. Bezman, Y.; Rouseff, R. L.; Naim, M. * Headspace solid phase microextraction ( SPME ) analysis of flavour compounds in wines. Effect of the matrix volatile composition in the relative response factors in a wine model. GC Journal of Agricultural and Food Chemistry (2001) 49(11), 5142-5151. Rocha, S.; Ramalheira, V.; Barros, A.; Delgadillo, I.; Coimbra, M. A. 1370 Volatiles in solid foods. New device for direct extraction of volatiles in solid samples using SPME GC-MS 1372 Coffee aroma Journal of Agricultural and Food Chemistry (2001) 49(11), 5115-5121. Ruiz, J.; Ventanas, J.; Cava, R. The use of an electronic aroma-sensing device to assess coffee differentiation. Comparison with SPME gas chromatography-mass spectrometry aroma patterns. 100 um PDMS GC-MS Journal of Food Composition and Analysis (2001) 14(5), 513-522. Costa Freitas, A. M.; Parreira, C.; Vilas-Boas, L. 1377 PAH in rice. Dynamics analysis for the distribution of PAH in rice. Journal of Health Science (2001) 47(5), 446-451. Liu, X. X.; Korenaga, T. GC-MS 1378 Fatty acids in milk. 1382 1387 Volatile flavour compounds. Cucumber flavour compounds Quantitative determination of short-chain free fatty acids in milk using solidphase microextraction and gas chromatography. Polyacrylate GC Journal of Agricultural and Food Chemistry (2001) 49(10), 4603-4608. Gonzalez-Cordova, A. F.; Vallejo-Cordoba, B. * Comparison of simultaneous distillation extraction and solid-phase microextraction for the determination of volatile flavour components. GC-MS Journal of Chromatography, A (2001) 930(1-2), 1-7. Cai, J. B.; Liu, B. Z.; Su, Q. D.* Solid-phase microextraction ( SPME ) technique for measurement of generation of fresh cucumber flavour compounds. Journal of Agricultural and Food Chemistry (2001) 49(9), 4203-4207. Palma-Harris, C.; McFeeters, R. F.*; Fleming, H. P. PDMS GC Ambient temperature, unless otherwise indicated. 26
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1389 Scotch whiskies 1390 Volatiles in potato tubers 1399 PCBs in food. 1401 Aroma from wine must. 1402 Headspace congeners of blended scotch whiskies of different product categories from SPME analysis. Journal of the Institute of Brewing (2001) 107(5), 315-332. Lee, K. -Y. M.; Paterson, A. *; Birkmyre, L.; Piggott, J. R PDMS, polyacrylate GC-FID Volatile fingerprinting (SPME-GC-FID) to detect and discriminate diseases of potato tubers. Plant Disease (2002) 86(2), 131-137 Kushalappa, A. C.; Chen, C. R.; Lee, B.; Lui, L. H. Fast extraction, clean-up and detection methods for the rapid analysis and screening of seven indicator PCBs in food matrices. Trends in Analytical Chemistry (2002) 21(1), 39-52 Anklam, E.; von Holst, Christoph; Bjorklund, E. Optimization of solid phase microextraction analysis of aroma compounds in a Portuguese muscatel wine must. 85 um polyacrylate Journal of Microcolumn Separations (2001) 13(6), 236-242. Relva, A. M.; Freire, Luis M. T. Vaz; Freitas, A. M. Costa GC-FID Lipid degeneration products in oils Monitoring of lipid degradation products by solid-phase microextraction 100 um PDMS GC-FID Journal of Microcolumn Separations (2001) 13(6), 215-220. 1403 Volatiles in bananas 1414 Volatiles from fruit. 1415 Off-flavors from milk 1418 1420 1421 1422 Volatiles in soybean and corn oils Volatile compounds in wine. Pesticides in strawberries. Volatile compounds from oranges. Doleschall, Fruzsina; Kemeny, Zsolt; Kovari, Katalin; Recseg, Katalin Optimization of solid-phase microextraction analysis for studying change of headspace flavor compounds of banana during ripening. Journal of Agricultural and Food Chemistry (2002) 50(4), 653-657 Liu, Tai-Ti; Yang, Tsung-Shi Solid phase microextraction and gas chromatography-olfactometry analysis of internal volatiles from intact citrus fruits and their aroma activity GC-O Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD142. Rouseff, Russell L.; Lin, Jianming SPME GC-MS-based testing for monitoring off-flavor development in processed milk. Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD27. Marsili, Ray T. Solid phase microextraction of volatile soybean oil and corn oil compounds. Journal of Food Science (2002) 67(1), 71-76 Min, D. B.; Lee, J. H.; Steenson, D. F. Various fibers compared GC-MS Polydimethylsiloxane solid-phase microextraction-gas chromatography method for the analysis of volatile compounds in wines. Its application to the characterization of varietal wines. PDMS GC Journal of Chromatography A (2001) 922(1-2), 267-275. Polo, M. C.; Martin-Alvarez, P. J.; Pozo-Bayon, M. A.; Pueyo, E. Determination of organochlorine pesticides and chlorobenzenes in strawberries by using accelerated solvent extraction combined with sorptive enrichment and gas chromatography/mass spectrometry. Journal of AOAC International (2001) 84(4), 1194-1201. Wennrich, Luise; Breuste, Juergen; Koeller, Gabor; Popp, Peter Analysis of volatile compounds released from embryogenic cultures and somatic embryos of sweet oranges by head space SPME GC-MS Plant Cell Tissue and Organ Culture (2001) 66(1), 31-34. Del Bosco, S. Fatta; Alonzo, G.; Saiano, F.; Tusa, N. Ambient temperature, unless otherwise indicated. 27
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SPME Applications Guide - Labicom

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