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SPME Applications Guide - Labicom

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1423<br />

1424<br />

1426<br />

(New references added to the 6th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference Conditions Instrument<br />

Volatiles from turkey<br />

breast.<br />

Volatiles of gourd<br />

flowers.<br />

The effects of temperature and pressure on the performance of<br />

Carboxen/PDMS fibres during solid phase microextraction ( <strong>SPME</strong> ) of<br />

headspace volatiles from cooked and raw turkey breast. Carboxen/PDMS<br />

Flavour and Fragrance Journal (2001) 16(4), 294-302.<br />

Cronin, D. A.; Brunton, N. P.; Monahan, F. J.<br />

Headspace-<strong>SPME</strong> analysis of volatiles of the ridge gourd (Luffa acutangula)<br />

and bitter gourd (Momordica charantia) flowers. GC-MS<br />

Flavour and Fragrance Journal (2001) 16(4), 289-293.<br />

Grun, I. U.; Fernando, L. N.<br />

Aroma of strawberry<br />

drink. Changes in the aroma of a strawberry drink during storage.<br />

Journal of Agricultural and Food Chemistry (2001) 49(7), 3244-3252.<br />

Siegmund, Barbara; Derler, Karin; Pfannhauser, Werner<br />

1440 Truffle aroma Truffle aroma characterization by headspace solid-phase microextraction<br />

Journal of Chromatography A (2003) 1017(1-2), 207-214<br />

Diaz, P.; Ibanez, E.; Reglero, G.; Senorans, F.J<br />

1441 Propionic acid in feed<br />

1442<br />

1448<br />

Volatiles in Italian<br />

Vinegars<br />

Garlic flavor<br />

components<br />

1451 Volatiles in Olive Oil<br />

1452 Volatiles in Olive Oil<br />

1453<br />

Free fatty acids in ewe<br />

cheese<br />

1454 Aroma volatiles in beef<br />

Analysis of total propionic acid in feed using headspace solid-phase<br />

microextraction and gas chromatography<br />

Journal of Chromatography A (2003) 1017(1-2), 161-166<br />

Ibanez, Carlos<br />

Quantitative analysis of 2-furfural and 5-methylfurfural in different Italian<br />

vinegars by headspace solid-phase microextraction coupled to gas<br />

chromatography-mass spectrometry using isotope dilution<br />

Journal of Chromatography A (2003) 1017(1-2), 141-149<br />

Calabrese, Roberto; Davoli, Enrico; Giordano, Lucia; Rotilio, Domenic<br />

Comparative study of extraction techniques for determination of garlic<br />

flavour components by gas chromatography-mass spectrometry.<br />

Analytical and Bioanalytical Chemistry (2003) 377(4), 749-756<br />

Lee, S. N.; Kim, N. S.; Lee, D. S.<br />

Solid-phase microextraction in the analysis of virgin olive oil volatile fraction:<br />

Characterization of virgin olive oils from two distinct geographical areas of<br />

northern Italy.<br />

Journal of Agricultural and Food Chemistry (2003) 51(22), 6572-6577<br />

Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale,<br />

Lorena; Vichi, Stefania<br />

Solid-phase microextraction in the analysis of virgin olive oil volatile fraction:<br />

Modifications induced by oxidation and suitable markers of oxidative status.<br />

Journal of Agricultural and Food Chemistry (2003) 51(22), 6564-6571<br />

Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale,<br />

Lorena; Vichi, Stefania<br />

Quantification of short-chain free fatty acids in "Terrincho" ewe cheese:<br />

Intravarietal comparison.<br />

Journal of Dairy Science (2003) 86(10), 3102-3109<br />

Ferreira, I. M. P. L. V. O.; Ferreira, M. A.; Pinho, O.<br />

Evaluation of two commercial solid-phase microextraction fibres for the<br />

analysis of target aroma compounds in cooked beef meat<br />

Talanta (2003) 61(4), 529-537<br />

Istasse, Louis; Machiels, David<br />

Ambient temperature, unless otherwise indicated. 28<br />

50/30um DVB/Carboxen PDMS<br />

headspace 13.6 mins.<br />

GC-MS<br />

85um Polyacrylate headspace GC-FID, GC-MS<br />

50/30um DVB/Carboxen PDMS<br />

headspace<br />

50/30um DVB/Carboxen PDMS,<br />

headspace<br />

85um Polyacrylate 65 degrees<br />

C, 45 mins. Headspace<br />

50/30um DVB/Carboxen PDMS,<br />

Carboxen PDMS, headspace<br />

GC-MS<br />

GC-MS<br />

GC-FID, GC-MS<br />

GC-FID, GC-MS<br />

GC-FID<br />

GC-MS

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