SPME Applications Guide - Labicom

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(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1437 Polymer/additives 1518 1302 Residual styrene monomer 1209 Diethyl sulfide 1268 1434 Monocyclic aromatic compounds in heavy fuel oil. Methylcyclopentadienylmanganese tricarbonyl Direct solid sampling methods for gas chromatographic analysis of polymer/additive formulations GC-FTIR-MS Polymer Testing (2001) 20(7), 729-740. Bart, J.C.J. Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry. Journal of Separation Science (2002) 25(8), 539-542 Kusch, Peter; Knupp, Gerd Headspace solid-phase micro-extraction - gas chromatography - mass spectrometry applied to quality control in multilayer-packaging manufacture. Journal of Chromatography, A (2003) 1008 (1), 123-128. Ezquerro, O.; Pons, B.; Tena, M. T.* TiO/sub2/ reactivation in photocatalytic destruction of gaseous diethyl sulfide in a coil reactor Applied Catalysis B: Environmental (2003) 44 (1), 25-40. Lion, Claude; Savinov, Evgueni N.; Smirniotis, Panagiotis G.; Vorontsov, Alexandre V. A GC-MS method for analysis of volatile monocyclic aromatic compounds in heavy fuel oil using headspace-solid phase microextraction. Chromatographia (2003) 58 (1-2), 115-117. Mangani, G.; Berloni, A.; Maione, M. * Determination of methylcyclopentadienyl-manganese tricarbonyl by solid phase microextraction-direct thermal desorption-quartz furnace atomic absorption spectrometry Spectrochim Acta Part B At Spectrosc (2001) 56(2), 215-221. Alava-Moreno, Fausto; Bendicho, Carlos; Fragueiro, Maria Sandra; Lavilla, Isela 75um Carboxen PDMS, headspace 1760 Organo- Thermal stability analysis of organo-silicates, using headspace TGA, GC-MS silicates from solid phase microextraction techniques polyurethane Thermochim Acta, 429, #1, 13-18 Edwards, G.; Halley, P.; Kerven, G.; Martin, D. 1761 Volatiles Use of SPME to monitor gases resulting form headspace GC from polymer thermal plasma pyrolysis. pyrolysis Chromatographia, 60, #1-2, 85-88 Cubas, A.; Carasek, E; Debacher, N. ; de Souza, I. GC-MS GC-MS 1762 Volatiles Probing the microwave degradation mechanism of phenol- heaspace from 20° to GC-MS from phenolic containing polymeric compounds by sample pretreatment 80°C polymers and GC-MS analysis Analytica Chimica Acta, 526, #2, 121-129 Chang, Yu-Cheng; Chu, Tieh-Chi; Ko, Chu-Jung; Ko, Fu 1763 Thermal SPME to concentrate volatile products from thermal 100µm PDMS, GC-MS byproducts of degradation of polymers 75µm Carboxen polypropylene Polym Degradation Stab, 89, #1, 33-37 Bortoluzzi, J.; Carasek, E; Pinheiro, E.; Soldi, V 1764 Odours from Emission of possible odourous low molecular weight heaspace GC-MS polypropylene compounds in recycled biofibre/polypropylene composites composites monitored by head-space SPME-GC-MS Polym Degradation Stab, 90. #3, 555-562 De Las Heras, Luis A.; Espert, Ana; Karlsson, Sigbritt 1765 Odor Development and analytic of odor absorber headspace GC removal by Tenside Surfactants Deterg, 41, #6, 282-286 Zn ricinoleate Bohmer, Thomas; Muller, Felix; Peggau, Jorg Ambient temperature, unless otherwise indicated. 50
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1766 Volatiles from Headspace-SPME-GC-MS identification of volatile organic 75µm Carboxen GC-MS polystyrene compounrds released from expanded polystyrene headspace J. Polym. Environ., 12, #2, 83-87 Knupp, Gerd; Kusch, Peter 1767 2-cyclopentyl- Correlation between emitted and total amount of headspace GC-MS cyclo- 2-cyclopentyl- cyclopentanone in polamide 6.6 GC-RI pentanone in allows rapid assessment by Head Space and HS-SPME . polamide 6.6 under non-equilibrium conditions J. Chromatogr. A, 1052, #1-2, 151-159 Groning, Mikael; Hakkarainen, Minna 1768 2-cyclopentyl- Multiple headspace SPMEof 2-cyclopentyl- cyclopentanone headspace GC-MS cyclo- in polyamide 6.6: Possibilities and limitations in the headspace analysis of solid hydrogen-bonding matrices pentanone in J. Chromatogr. A, 1052, #1-2, 61-68 polamide 6.6 Groning, Mikael; Hakkarainen, Minna 1769 Hydrocarbons Determination of aromatic hydrocarbons in asphalt release headspace GC-MS from asphalt agents using headspace SPME-GC-MS J Chromatogra, A, 1069, #2, 235-244 Isacsson, Ulf; Tang, Bing Natural Products 401 Volatiles Analysis of Tobacco Volatiles with SPME 100µm PDMS GC-MS in tobacco Dr. W.D. Koller, Federal Research Centre for Nutrition, 10 min Institute of Process Engineering, Engesserstr. 20, 76131 Karlsruhe/Deutschland headspace 402 Pesticides in A Simple Screening for Pesticide Residues in Tobacco 100µm PDMS GC-MS water/MeOH extract Dr. W.D. Koller, Federal Research Centre for Nutrition, 10 min Institute of Process Engineering, Engesserstr. 20, 76131 Karlsruhe/Deutschland immersion 102 Flavor additives Qualitative and Quantitative Analysis of Flavor Additives 65µm Carbowax/DVB GC-FID in tobacco on Tobacco Products Using SPME-GC-MS 95°C, 15 min J. Agric. Food Chem. 45: 844-849 (1997) Clark, J., Bunch, J. KCl added 430 Alkaloids Determination of Tobacco Alkaloids Using SPME and GC-NPD 100µm PDMS GC-NPD in tobacco Chromatographia (1998), 47(7/8), 443-448 12 min, immersed Yang, S., Smetena, I. 1% NH3OH solution 627 Acetates Quantitative analysis of acetates in cigarette tobacco GC-MS in cigarette tobacco using SPME-GC-MS J. Chromatogr. Sci (2000), 38(4), 137-144 Watson, C., Ashley, D. headspace 137 Phenols in Quantitative Determination of Phenols in Mainstream Smoke 85µm polyacrylate GC-FID cigarette smoke with SPME-GC-Selected Ion Monitoring Mass Spectrometry 60 min J. Chromatogr. Sci. 34: 272-275 (1996) Clark, J., Bunch, J. stirring 628 Azo dyes Study on determination of prohibited azo dyes by SPME GC-MS in leather & textiles Fenxi Deshi Xuebao (2000), 19(1), 76-78 reduced to aromatic Xu, H., Tong, H. amines w/Na2SO4 Azo dyes Development of a SPME method for detection of the use of in leather & textiles banned Azo dyes in coloured tectiles and leather Rapid Commun.Mass Spectrom. 13, pp1833-1837 Cioni, G., Bartolucci, G., Pieraccini, G., Meloni, S., Moneti, G. Ambient temperature, unless otherwise indicated. 51
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SPME Applications Guide - Labicom

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