SPME Applications Guide - Labicom

More documents

Recommendations

Info

(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 364 Off-flavors Off Flavor and Malodors in Food: Mechanism of Formation various fibers GC in food and Analytical Techniques Book-Techniques for Analyzing Food Aroma, Marcel Decker ISBN: 0-8247-9788-4 Marsili, R. and conditions 376 Volatile metabolites Evaluation of SPME for Analysis of Volatile Metabolites 85µm polyacrylate GC-FID in water Produced by Staphylococci 80°C, 15 min J. Agric. Food Chem. 1998, 46, 228-234 Vergnais, L., Masson, F., Montel, M., Berdague, J., Talon, R. headspace, stirring 365 Volatiles Determination of Volatile Organic Compounds in Tea 100µm PDMS GC-MS in tea Industrie de la Bevande XXVI (1997) febbralo, 19-22 50°C, 15 min Guidotti, M. headspace 622 Polyphenols Comparative Study and Partial characterization of Azorean in green tea green Tea Polyphenols J. Food Compos. Anal. (1999), 12(4), 273-287 Baptista, J., da P Tavares, J., Carvalho, R. 319 Caffeine Quantitative Determination of Caffeine in Beverages, bare fiber GC-MS in tea, coffee Using a Combined SPME-GC-MS Method J. Chem. Educ. 74 (9): 1130-1132 (1997) Yang, M., Orton, M., Pawliszyn, J. 381 Aroma volatiles Characterization of Roasted Coffee and Coffee Beverages 100µm PDMS, GC-MS in coffee by SPME-GC and Principal Component Analysis 7µm PDMS J. Agric. Food Chem. 1997, 45: 4680-4686 60°C, 5 min Bicchi, C., Panero, O., Pellegrino, G., Vanni, A. headspace 302 Volatile aroma Obtention of a Brewed Coffee Aroma Extract by an 100µm PDMS GC-MS in brewed coffee Optimized Supercritical CO2-Based Process 60°C, 10 min J. Agric. Food Chem. 1998, 46, 4011-4016 Ramos, E., Valero, E., Ibanez, E., Reglero, G., Tabera, J. headspace 623 Aroma volatiles SPME Method Development for Headspace analysis of PDMS/DVB GC-MS in coffee volatile flavor compounds 60 min headspace J. Agri. Food Chem 2000, 48, (6) 2430-2437 Roberts, D., Pollien, P., Milo, C. pH 2 624 2-Acetyl-1-pyrroline Screening for 2-Acetyl-1-pyrroline in the Headspace of Rice 80µm Carboxen/DVB/PDMS GC-MS in rice using SPME/GC-MS 80°C, 15 min J. Agric. Food Chem 2001, 49, 245-249 headspace Grimm, C, Bergman, jC., Delgado, J., Bryant, R. .75gm in 100µl H20 464 2-MIB, geosmin Microwave mediated distillation with SPME 100µm PDMS GC-MS in water determination off-flavors, geosmin and 25 min methylisoborneol, in catfish tissue immersed J. Chromatogr. A (1999), 833(2), 223-230 salt added Zhu, M., Aviles, F., Conte, E., Miller, D., Perschbacher, P. 625 2-MIB, geosmin Microwave Distillation-SPME-GC Analysis of 80µm Carboxen/DVB/PDMS GC-IC-MS in water 2-methylisoboreneol and Geosmin in Catfish 60°C, 20 min Am-Lab Feb 2000: 32(3), 40-48 Lloyd, S., Grimm, C. heaspace 2-MIB, geosmin Analysis of 2-Methylisoboreneol and Geosmin in Catfish 100µm PDMS GC-MS in water by Microwave Distillation-SPME 40°C, 15 min J. Agri. Food Chem., 47, No. 1, pg. 164-169, 1999 saturated salt Lloyd, S., Grimm, C. stirring Ambient temperature, unless otherwise indicated. 16
(New references added to the 6th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 362 MIB & geosmin Determination of Geosmin and 2-Methylisoboreneol in Water Carboxen/DVB/PDMS GC-MS in water Using SPME and GC-Chemical Ionization/Electron Impact 60°C, 30 min Ionization Ion Trap MS headspace Analyst (Cambridge, U.K.) (1998), 123 (10), 2155-2160 stirring McCallum, R., Pendleton, P., Scumann, R., Trinh, M. salt added 465 C2-C10 acid, Evaluating Peats for their capacities to remove 85µm polyacrylate GC-MS aldehydes, phenols odorous compounds from liquid swine manure 20 min @ 72°C in swine manure using headspace SPME headspace, pH 2 J. Environ. Sci.Health, B34(4), 709-748 (1999) Rizzuti, A., Cohen, A., Hunt, P., Vanotti, M. 966 Esters in wine Analysis of esters in wines Various GC J.Chromatogr. A (2002) 963(1-2), 213-223 Rodriguez-Bencomo, J.J.; Conde, J.E.; Rodriguez-Delgado, M.A.; Garcia- Montelongo, F.; Perez-Trujillo, J.P. 967 Aroma in onions Flavor and odor differences between fresh and preserved onions Polyacrylate GC-MS J.Chromatogr. A (2002) 963(1-2), 89-93 Mondy, N.; Duplat, D.; Christides, J.P.; Arnault, L.; Auger, J. 968 Volatiles in olive oil Influence of crushing technique on composition of volatiles in olive oil. 65 um Carbowax/DVB GC-MS 969 970 992 996 997 999 European Journal of Lipid Science and Technology (2002) 104(8), 483-489 30 mins. Servili, M.; Piacquadio, P.; de Stefano, G.; Taticchi, A.; Sciancalepore, V. Volatiles in dry-cured ham Monitoring volatile compounds during the dry-cured ham ripening process J.Chromatogr. A (2002) 963(1-2), 83-88 Andres, A.I.; Cava, R.; Ruiz, J. Bisphenol in food packaging Odour compounds in food packaging materials Photooxidative quality changes of havarti cheese. Volatile compounds from scallops 1007 Insecticides in fruit Bisphenol type contaminants from food packaging materials in aqueous foods. HPLC J.Chromatogr. A (2002) 963(1-2), 375-380 Nerin, C.; Philo, M.R.; Salafranca, J.; Castle, L. Development of headspace SPME, GC-MS method for the identification of odour causing volatile compounds in packaging materials. 75 um carboxen/PDMS GC-MS J.Chromatogr. A (2002) 963(1-2), 381-392 Ezquerro, O.; Pons, B.; Tena, M.T. Response surface models used for prediction of photooxidative quality changes of havarti cheese. GC-MS European Food Research and Technology (2003) 216 (2), 93-98. Stapelfeldt, Henrik; Mortensen, Grith; Sorensen, John. Solid phase micro-extraction technique and its applications in medical analysis. Yaoxue Xuebao (2003) 38 (2), 153-158. Liu Zhen-ling; Wu Cai-ying. Volatile compounds recovered by solid-phase microextraction from fresh adductor muscle and total lipids from sea scallop ( Placopecten magellanicus ) from Georges Bank (Nova Scotia). PDMS/DVB GC-MS Journal of Food Science (2002) 67 (6), 2032-2037. 250 C, 2 minutes Linder, M.; Ackman, R. G. Headspace solid-phase microextraction in combination with gas chromatography-mass spectrometry for the rapid screening of organophosphorus insecticide residues in strawberries and cherries GC-MS J.Chromatogr. A (2003) 993(1-2), 197-203. Albanis, Triantafyllos A.; Lambropoulou, Dimitra A. Ambient temperature, unless otherwise indicated. 17
Page 1 and 2: SUPELCO Bulletin 925E SPME Applicat
Page 3 and 4: (New references added to the 6th ed
Page 15: (New references added to the 6th ed
Page 25 and 26: 1296 (New references added to the 6
Page 59 and 60: 1469 (New references added to the 6
Page 67 and 68:
(New references added to the 6th ed
Page 69 and 70:
Page 71 and 72:
Page 73 and 74:
Page 75 and 76:
Page 77 and 78:
Page 79 and 80:
Page 81 and 82:
Page 83 and 84:
Page 85 and 86:
Page 87 and 88:
Page 89 and 90:
Page 91 and 92:
Page 93 and 94:
Page 95 and 96:
Page 97 and 98:
1286 (New references added to the 6
Page 99 and 100:
Page 101 and 102:
Page 103 and 104:
Page 105 and 106:
Page 107 and 108:
Page 109 and 110:
Page 111 and 112:
Page 113 and 114:
Page 115 and 116:
Page 117 and 118:
Page 119 and 120:
Page 121 and 122:
Page 123 and 124:
Page 125 and 126:
Page 127 and 128:
Page 129 and 130:
Page 131 and 132:
Page 133 and 134:
Page 135 and 136:
Page 137 and 138:
Page 139 and 140:
Page 141 and 142:
Page 143 and 144:
Page 145 and 146:
1096 1113 (New references added to
Page 147 and 148:
Page 149 and 150:
Page 151 and 152:
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Page 161 and 162:
1334 1342 (New references added to
Page 163 and 164:
Page 165 and 166:
Page 167 and 168:
Page 169 and 170:
Page 171 and 172:
Page 173 and 174:
Page 175 and 176:
Page 177 and 178:
Page 179 and 180:
Page 181 and 182:
SPME Literature Literature No. Titl
show all

SPME Applications Guide - Labicom

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?