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2011-NMMU-Research-Report - Research Management - Nelson ...

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NRF <strong>Research</strong> Niche Areas<br />

The Institutional <strong>Research</strong> Development Programme (IRDP) of NRF<br />

seeks to assist higher education institutions in the development<br />

and enhancement of their research culture, environment, ethos<br />

and practice to become world-class African universities in order to<br />

deliver the skills required by the national system of innovation.<br />

The main objectives of the IRDP are to increase the quality of PhDs<br />

and other research outputs. Linked to this it seeks to promote staff<br />

development, increase the number of rated researchers and facilitate<br />

institutional partnerships.<br />

The <strong>NMMU</strong> had to identify and focus within the context of the<br />

IRDP its research activities into a limited number of <strong>Research</strong> Niche<br />

Areas (RNAs) where there were existing strengths and the potential<br />

for further development. The four RNAs eventually approved for<br />

<strong>NMMU</strong> by external peer reviewers were all pitched at the highest<br />

level, that of "developed RNAs".<br />

Innovative Batch Chemical<br />

Technology for Downstream<br />

Chemical Products and<br />

Processes<br />

Team Leader: Prof Ben Zeelie<br />

Mr Lubabalo Mafu at one of InnoVenton’s Small Production Platform rigs.<br />

23<br />

The research focus of this five-year programme was primarily on<br />

the development of alternative production methodologies for<br />

downstream chemicals and chemical products through the<br />

development of alternative technologies to traditional-batch<br />

and semi-batch production technologies. The development and<br />

evaluation of opportunities to grow and develop the South African<br />

downstream chemicals manufacturing sector was a particular focus<br />

of the programme.<br />

Effective chemical process development is an amalgam of synthetic<br />

methods, physiochemical properties, purification technologies,<br />

and chemical engineering (reactor and separation technologies)<br />

- orchestrated in a manner that will produce the desired chemical<br />

product safely, in high-quality, reproducible, and cost efficient. This<br />

type of integrated and applied research is not normally carried out at<br />

universities, which made the programme rather unique in the world.<br />

The following researchers formed part of the programme over<br />

the five-year period: Dr Shawn Gouws (Organic Electrochemical<br />

Synthesis); Dr Gary Dugmore (Small Production Platforms); Prof<br />

Ben Zeelie (Batch Chemical Process Development) and Dr Nigel<br />

Harmse (Natural and Renewal Raw Materials). The following<br />

students graduated with Masters and Doctoral degrees from<br />

the programme: I Asquith (Doctorate); S Buddoo (Doctorate);<br />

GR Gordon (Doctorate); MP Thomas (Doctorate); MC Schaefer<br />

(Doctorate); C Lombe (Masters); SE Qusheka (Masters); B Mpuhlu<br />

(Masters); L Brooks (Masters); N Rust (Doctorate); JR Indurkar<br />

(Doctorate); ND Satikge (Masters); PR Makgwane (Doctorate);<br />

LR Mafu (Masters); and B Mpuhlu (Doctorate). The programme<br />

also resulted in eight peer-reviewed publications, 14 conference<br />

presentations and five patents.<br />

Some highlights of the work carried out over the five-year period<br />

include the development of a continuous process for the production<br />

of p-menthane-3,8-diol, a valuable chemical that can be used in a<br />

variety of applications such as insect repellents, bactericides, and<br />

others. A small production platform was designed, constructed<br />

and optimised in our Kilo-Lab facility. The results of this work were<br />

then used for the specification and design of a commercial-scale<br />

production reactor capable of producing 120 ton product per<br />

year. A second example was the design, construction and use of<br />

a small production platform for the synthesis of a new candidate<br />

fuel additive from local South African raw materials. This synthesis,<br />

which usually involves reacting highly flammable materials under<br />

high pressure and temperature, was carried out in a continuousflow<br />

reactor over a solid catalyst safely and approximately 100 kg<br />

of the product was delivered for testing purposes.

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