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guide to thin section microscopy - Mineralogical Society of America

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Guide <strong>to</strong> Thin Section Microscopy<br />

Extinction<br />

Optical character <strong>of</strong> the extinction directions<br />

If a birefringent crystal <strong>section</strong> is in extinction position, the vibration directions Z' and X‘ are<br />

parallel <strong>to</strong> the N-S and E-W directions <strong>of</strong> the crosshairs (cf. Fig. 4-23). For a variety <strong>of</strong><br />

applications it may be important <strong>to</strong> know which direction corresponds <strong>to</strong> the higher,<br />

respectively lower, refractive index:<br />

• Determination <strong>of</strong> mineral colour in a specific vibration direction (cf. Ch. 4.2.1).<br />

• Determination <strong>of</strong> optical sign <strong>of</strong> optically uniaxial minerals which are elongate in c<br />

direction or platy having the basal plane ({001}, {0001}) as the dominant crystal face.<br />

• Determination <strong>of</strong> sign <strong>of</strong> elongation (l) <strong>of</strong> acicular <strong>to</strong> columnar, platy or flaky minerals in<br />

elongate crystal <strong>section</strong>s.<br />

For a distinction between vibration directions Z' and X‘, compensa<strong>to</strong>r plates are used. These<br />

are anisotropic crystal plates <strong>of</strong> constant or variable retardation with known orientation <strong>of</strong> the<br />

X and Z wave vibration directions (α = n x and γ = n z ). The vibration direction <strong>of</strong> the Z wave<br />

(γ = n z ) is engraved in the metal casing <strong>of</strong> the compensa<strong>to</strong>rs. Commonly used compensa<strong>to</strong>rs<br />

(Fig. 4-42):<br />

The first-order red plate (lambda plate, λ plate, sensitive tint plate) consists <strong>of</strong> a quartz or<br />

gypsum plate that is cut parallel <strong>to</strong> the optic axis, about 62 µm thick, which shows a firs<strong>to</strong>rder<br />

red interference colour in diagonal position (Γ = 551 nm).<br />

The lambda/4 (lambda quarter) plate consists <strong>of</strong> a <strong>thin</strong> quartz or mica plate which shows a<br />

grey interference colour in diagonal position (Γ = 130-150 nm, depending on manufacturer).<br />

The quartz wedge consists <strong>of</strong> a wedge-shaped quartz plate with the long axis parallel <strong>to</strong> the<br />

optic axis. In diagonal position, this quartz wedge shows interference colours ranging across<br />

four orders (Γ = 0 <strong>to</strong> 2200 nm).<br />

Most commonly, the compensa<strong>to</strong>rs are inserted diagonally in<strong>to</strong> the microscope tube below the<br />

analyzer. The wave corresponding <strong>to</strong> n z (γ or Z’) vibrates in NE-SW direction, the wave<br />

corresponding <strong>to</strong> n x (α or X’) in NW-SE direction.<br />

Raith, Raase & Reinhardt – February 2012<br />

Figure 4-42. Compensa<strong>to</strong>rs– first-order red plate (λ plate), lambda/4 plate and quartz wedge<br />

104

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