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Distribution of Chlorinated Hydrocarbon Pesticides and PCBs in the ...

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value is less than <strong>the</strong> procedural detection limit for that<br />

compound.<br />

3) if <strong>the</strong> blank corrected value was less than ten blank<br />

st<strong>and</strong>ard deviations, it was replaced by <strong>the</strong> value<br />

corespond<strong>in</strong>g to ten blank st<strong>and</strong>ard deviations <strong>and</strong> preceded<br />

with <strong>the</strong> letter Q denot<strong>in</strong>g that <strong>the</strong> compound was &<br />

detected but <strong>the</strong> determ<strong>in</strong>ed value was less than <strong>the</strong><br />

quantitation limit.<br />

-<br />

4) <strong>the</strong> result<strong>in</strong>g blank corrected quantities or <strong>the</strong> detection<br />

<strong>and</strong> quantitation limits were converted to concentrations<br />

<strong>and</strong> reported <strong>in</strong> <strong>the</strong> follow<strong>in</strong>g units;<br />

water - pg.~-' (pg = 10-12g)<br />

snow - pg.~-l <strong>in</strong> melt water<br />

ice - pg.~-l <strong>in</strong> melt water<br />

sediment - ng.g-', dry weight (ng =<br />

biota - ng.g-', dry weight (also reported as wet weight<br />

<strong>and</strong> lipid weight<br />

air - pg.m-3<br />

3.2 Quality Control <strong>and</strong> Quality Assurance <strong>in</strong><br />

Organochlor<strong>in</strong>e Analyses.<br />

Throughout <strong>the</strong> program, from sampl<strong>in</strong>g to GC analysis,<br />

steps were <strong>in</strong>cluded to monitor <strong>the</strong> quality <strong>of</strong> <strong>the</strong> data. The<br />

quality control <strong>in</strong>cluded scrut<strong>in</strong>y <strong>of</strong> <strong>in</strong>strument calibration,<br />

blanks <strong>and</strong> replicates. As part <strong>of</strong> <strong>the</strong> quality assurance program,<br />

various 'referencet materials such as, st<strong>and</strong>ard reference<br />

I

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