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Distribution of Chlorinated Hydrocarbon Pesticides and PCBs in the ...

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TABLE OF CONTENTS<br />

2.9 Sediment Sampl<strong>in</strong>g<br />

2.10 Miscellaneous Sampl<strong>in</strong>g for<br />

<strong>Chlor<strong>in</strong>ated</strong> <strong>Hydrocarbon</strong>s<br />

2.11 Water Properties<br />

2.11.1 CTD Pr<strong>of</strong>iles<br />

2.11.2 Nutrients<br />

3.0 ANALYTICAL METHODS<br />

3.1 <strong>Chlor<strong>in</strong>ated</strong> <strong>Hydrocarbon</strong>s<br />

Materials<br />

Blanks <strong>and</strong> St<strong>and</strong>ardization<br />

In-Situ Sampler Columns Analysis<br />

Polyurethane Foam Plugs (Air Samples)<br />

Analysis<br />

Particulate Filters <strong>and</strong> Sediment<br />

Extractions<br />

Extraction <strong>of</strong> Biological Tissue<br />

Samples<br />

Sample Clean-up <strong>and</strong> Separation<br />

Instrumental Analysis<br />

Detection <strong>and</strong> Quantitation Limits<br />

3.2 Quality Control <strong>and</strong> ~uality Assurance <strong>in</strong><br />

Qrganochlor<strong>in</strong>e Analyses<br />

3.2.1 Instrument calibration<br />

3.2.2 Blanks<br />

3.2.3 Replicates<br />

3.2.4 Quality Assurance<br />

a) XAD Water Sampl<strong>in</strong>g Validation<br />

b) In-situ Particulate Sampl<strong>in</strong>g<br />

c) Air Sampl<strong>in</strong>g <strong>and</strong> Analyses<br />

d) Snow Samples<br />

e) Biota Samples<br />

f) Sediment Samples<br />

3 -3 POC/PON<br />

3.4 Lipids<br />

3.5 Reactive Nutrients<br />

3.6 Sediment Gra<strong>in</strong> Size<br />

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