Thermo Miran Sapphire XL Manual 2005 - IE Monitoring Instruments

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6. Change Gas................................................................................................................. 6-1 7. Configuration and Setup ........................................................................................... 7-1 Calibration................................................................................................................... 7-3 Preferences .................................................................................................................. 7-3 Gas Unit....................................................................................................................... 7-5 Clock ...........................................................................................................................7-6 Analysis ....................................................................................................................... 7-7 Analysis Setup page 1 ................................................................................................. 7-8 Analysis Setup Page 2 ............................................................................................... 7-17 Analysis Setup Page 3 ............................................................................................... 7-19 Analysis Setup Page 4 ............................................................................................... 7-21 Application View and Edit........................................................................................ 7-25 8. Site Info....................................................................................................................... 8-1 Sites ............................................................................................................................. 8-1 Locations ..................................................................................................................... 8-2 Sites and Locations Summary ..................................................................................... 8-5 9. Report/Data Transfer ................................................................................................ 9-1 Select Site.................................................................................................................... 9-1 Print Menu................................................................................................................... 9-2 Data Transfer............................................................................................................... 9-3 Memory Clear.............................................................................................................. 9-5 Hyperterminal.............................................................................................................. 9-5 10. Maintenance and Service ...................................................................................... 10-1 Zero Gas Filter........................................................................................................... 10-1 Particulate Filter ........................................................................................................ 10-1 Battery Pack .............................................................................................................. 10-1 Care of Optics............................................................................................................ 10-2 Service Locations ...................................................................................................... 10-3 11. Firmware Update................................................................................................... 11-1 Introduction ............................................................................................................... 11-1 Procedure................................................................................................................... 11-2 iv
12. User Performance Verification............................................................................. 12-1 Introduction ............................................................................................................... 12-1 Procedure................................................................................................................... 12-1 13. Infrared Spectroscopy Tutorial............................................................................ 13-1 Overview ................................................................................................................... 13-1 Electromagnetic Energy ............................................................................................ 13-1 Basic Properties of Waves......................................................................................... 13-3 Atoms and Molecules in Motion............................................................................... 13-4 Qualitative Analysis: Identifying Compounds.......................................................... 13-7 Quantitative Analysis: Measuring Absorption Levels ............................................ 13-15 The Beer-Lambert Law ........................................................................................... 13-16 Infrared Spectroscopy Summary............................................................................. 13-18 How the SapphIRe Analyzer Works ....................................................................... 13-19 14. Custom Report Formatting................................................................................... 14-1 General ...................................................................................................................... 14-1 Obtaining a Custom Report....................................................................................... 14-1 Header ....................................................................................................................... 14-2 Gas Data .................................................................................................................... 14-3 Footer......................................................................................................................... 14-4 Report-Entry Fields ................................................................................................... 14-4 Coding Guide ............................................................................................................ 14-5 Appendix A - Warranty................................................................................................ A-1 Appendix B – Intrinsic Safety.......................................................................................B-1 Appendix C – Scan/Calibration Procedure ................................................................ C-1 Introduction .................................................................................................................C-1 A. Create a Logging Site .............................................................................................C-2 B. Perform a Peak Pick or Full Spectrum Scan...........................................................C-3 C. Download Data From the Analyzer to a PC ...........................................................C-5 D. – Analyze the Spectrum..........................................................................................C-6 E. – Create a New Single Gas or Multi-Gas Library Application...............................C-6 F. – Calibration..........................................................................................................C-10 G. – Generate the P-Matrix .......................................................................................C-11 H. – Enter P-MTRIX into the Analyzer and Verify Calibration Accuracy...............C-13 v
Page 1 and 2: MIRAN ® 205B Series SapphIRe PORTA
Page 3: CONTENTS 1. Introduction...........
Page 7 and 8: Chapter1 INTRODUCTION GENERAL DESCR
Page 9 and 10: Chapter 2 SPECIFICATIONS Thermo Env
Page 11: 2-3 Chapter 2 Specifications Table
Page 14 and 15: Chapter 3 Instrument Preparation Po
Page 16 and 17: Chapter 3 Instrument Preparation WA
Page 18 and 19: Chapter 3 Instrument Preparation No
Page 20 and 21: Chapter 3 Instrument Preparation Ca
Page 23 and 24: Chapter 4 OPERATION CONTROLS AND DI
Page 25 and 26: ENTERING ALPHANUMERIC CHARACTERS 4-
Page 27 and 28: ┌──────────
Page 29 and 30: 4-7 Chapter 4 Operation To establis
Page 31 and 32: 4-9 Chapter 4 Operation If the inst
Page 33 and 34: USING THE SEARCH FEATURE 4-11 Chapt
Page 35 and 36: ERROR SCREENS 4-13 Chapter 4 Operat
Page 37 and 38: Built-in clock's date/time is wrong
Page 39: ANALOG OUTPUT 4-17 Chapter 4 Operat
Page 42 and 43: Chapter 5 Analysis To re-zero the a
Page 44 and 45: Chapter 5 Analysis Caution: If ENTE
Page 46 and 47: Chapter 5 Analysis To review the Lo
Page 48 and 49: Chapter 5 Analysis Flag Screens In
Page 50 and 51: Chapter 6 Change Application ┌─
Page 52 and 53: Chapter 6 Change Application SPECTR
Page 55 and 56:
Chapter 7 CONFIGURATION and SETUP S
Page 57 and 58:
CALIBRATION 7-3 Chapter 7 Configura
Page 59 and 60:
7-5 Chapter 7 Configuration and Set
Page 61 and 62:
ANALYSIS 7-7 Chapter 7 Configuratio
Page 63 and 64:
Log Mode 7-9 Chapter 7 Configuratio
Page 65 and 66:
Other Parameters 7-11 Chapter 7 Con
Page 67 and 68:
Compensation 7-13 Chapter 7 Configu
Page 69 and 70:
7-15 Chapter 7 Configuration and Se
Page 71 and 72:
ANALYSIS SETUP PAGE 2 7-17 Chapter
Page 73 and 74:
ANALYSIS SETUP PAGE 3 7-19 Chapter
Page 75 and 76:
Page 77 and 78:
Unit 7-23 Chapter 7 Configuration a
Page 79 and 80:
APPLICATION VIEW AND EDIT ┌──
Page 81 and 82:
Group TWA 7-27 Chapter 7 Configurat
Page 83 and 84:
Gas STEL Time Interval 7-29 Chapter
Page 85 and 86:
Humidity to Absorbance Correction 7
Page 87 and 88:
Reference Compensation Summary 7-33
Page 89 and 90:
Page 91 and 92:
Pathlength 7-37 Chapter 7 Configura
Page 93 and 94:
┌──────────
Page 95:
Page 98 and 99:
Chapter 8 Site Info General Comment
Page 100 and 101:
Chapter 8 Site Info How to Use Loca
Page 103 and 104:
Chapter 9 Report/Data Transfer Warn
Page 105 and 106:
9-3 Chapter 9 Report/Data While pri
Page 107:
MEMORY CLEAR 9-5 Chapter 9 Report/D
Page 110 and 111:
Long Term Storage NiCd batteries di
Page 113 and 114:
Chapter 11 Firmware Update INTRODUC
Page 115 and 116:
┌──────────
Page 117:
Uploading Setup Information 11-5 Ch
Page 120 and 121:
Chapter 12 User Performance Verific
Page 122 and 123:
Chapter 13 Infrared Spectroscopy Tu
Page 124 and 125:
Page 126 and 127:
Page 128 and 129:
Page 130 and 131:
Page 132 and 133:
Page 134 and 135:
Page 136 and 137:
Page 138 and 139:
Page 140 and 141:
Page 143 and 144:
Chapter 14 Custom Report Formatting
Page 145 and 146:
GAS DATA 14-3 Chapter 14 Custom Rep
Page 147 and 148:
Example: REPORT-ENTRY FIELDS 14-5 C
Page 149 and 150:
Special Characters Certain characte
Page 151 and 152:
31: Current Time-Minutes Descriptio
Page 153 and 154:
14-11 Chapter 14 Custom Report Form
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Page 161 and 162:
Page 163 and 164:
Page 165 and 166:
Field Designator S (Measurement Sta
Page 167 and 168:
26 to 29: Reserved Description: Res
Page 169:
Page 173 and 174:
Appendix B Intrinsic Safety The Sap
Page 175 and 176:
Appendix C Scan/Calibration Procedu
Page 177 and 178:
B. PERFORM A PEAK PICK OR FULL SPEC
Page 179 and 180:
C-5 Appendix C Scan/Calibration Pro
Page 181 and 182:
Page 183 and 184:
Page 185 and 186:
C-11 Appendix C Scan/Calibration Pr
Page 187 and 188:
C-13 Appendix C Scan/Calibration Pr
Page 189 and 190:
Appendix D HUMIDITY COMPENSATION TA
Page 191 and 192:
Appendix E MIRAN ® SapphIRe Field
Page 193 and 194:
MIRAN SapphIRE Field Performance Ve
Page 195:
MIRAN SapphIRE Field Performance Ve
Page 198 and 199:
Appendix F Parts and Accessories Pa
Page 200 and 201:
Appendix F Parts and Accessories Ac
Page 203 and 204:
Appendix G USING HYPERTERMINAL with
Page 205 and 206:
Appendix H STANDARD LIBRARIES Compo
Page 207 and 208:
Compound Name Acronym Detection Det
Page 209:
Compound Name Acronym Detection Det
Page 212 and 213:
Index Display .....................
Page 214:
Index Site Info....................
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