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NATIONAL INSTITUTE OF TECHNOLOGY KARNATAKA, SURATHAKAL ------------------------------------------------------------------------------------------------------------------ Department of Chemistry CY100 CHEMISTRY (3-1-0) 4 Electrochemical Cells - Nernst Equation, Energetics of cell reaction, Types of electrodes and their applications, Concentration cells, Primary and Secondary cells, Fuel cells. Electroplating � Theory, Polarization, Decomposition potential, Overvoltage, Electroplating and Electroless plating of copper � PCB preparation. Corrosion � Types, Theory and factors affecting corrosion, Corrosion control, Galvanic series, Measurements of corrosion rate. Water Technology � Hardness of water, Boiler troubles, Internal and external treatments, Desalination. Energy: Fuels, Classification, Calorific value and its Determination, Coal and its analysis, Petroleum, Catalytic cracking, Diesel and petrol knocking, Reforming of gasoline, Synthetic petrol, Power alcohol, Biodiesel, hydrogen as a source of energy. High Polymers: Addition, Condensation and Coordination polymerization, Copolymerisation, Molecular weights and their determinations, Methods of Polymerization, Tg & Tm and factors affecting them, Teflon, PMMA and UF: Elastomers � Compounding, SBR and silicone rubbers, Conducting, Biodegradable, Liquid crystal polymers. Instrumental methods of analysis: Colorimetry and spectrophotometry, Qualitative and quantitative analysis; Conductometry and Potentiometry. Semiconductor chemistry: Preparation of pure semiconductors, doping techniques. Chemistry of Nano � materials - Nanocarbons, ZnO and TiO2. Puri B.R. Sharma L.R. and Madan S Pathania, Principles of Physical Chemistry, Vishal Publishing Co., 41 st Edition 2004 Jain P.C. & Monika Jain, Engineering Chemistry, Dhanpat Rai & Sons, Delhi, Revised 14 th Edition 2004. Kuriacose, J.C and Rajaram, J, Engineering Chemistry, Volume I/II, Tata McGraw – Hill Publishing Co. Ltd. New Delhi, 2000 Gowariker et al., Polymer Science and Technology, Prentice Hall of India Pvt. Ltd., New Delhi, 2004. Chatwal. G. and Anand, S., Instrumental Methods of Chemical Analysis, S. D. Himalaya Publishing House, 2003. Mars G. Fontana, Corrosion Engineering, McGraw Hill Book Company, 1986. Rao, C. N.R. Chemistry of Nanomaterials, Volume I and II, Wiley Publication, 2004. Gandhi, S. K.,, VLSI Fabrication Principles, Wiley Interscience, 2 nd Edn. 1994 CY101 CHEMISTRY LABORATATORY (0-0-3) 2 Volumetric estimations involving metal-ion, redox, self and precipitation type indicators � analysis of water (hardness and chlorides), ores (haematite and pyrolusite); Instrumental methods of analysis � potentiometry, Colorimetry, conductometry, refractometry and viscometry; Analysis of polymers, metals, alloys and related Engineering materials. Engineering Chemistry Lab manual, Written by Faculty, Dept of Chemistry, NITK Surathkal. Furnis et al (ed)., Pearson., Vogel’s Text book of “ Quantitative Chemical Analysis” , ELBS, London CY201 PRINCIPLES OF ORGANIC SYNTHESIS (3–0–0) 3 Formation of C-C bonds: Organometallic reagents. Formation of aliphatic C-C bonds, base/acid catalyzed. Formation of aliphatic C-N bonds. Pericyclic reactions. Electrophilic aromatic substitution. Nucleophilic aromatic substitution reactions. Molecular rearrangements: Rearrangement to electrondeficient carbon, nitrogen and oxygen. Aromatic rearrangements. Photochemical reactions. Free radical reactions. Oxidation & reduction reactons. J. March, Advanced Organic Chemistry, 4 th edition, McGraw Hill, New York, 1994. R. O. C. Norman and J. M. Coxon, Principles of Organic Synthesis, Blackie Academic and Professional, Glasgow, NewYork, 1993. CY202 UNIT PROCESSES IN ORGANIC SYNTHESIS (3-0- 0) 3 Bond breaking, bond forming, synchronous bond breakage and formation, intramolecular migration, electron transfer, types of reactions. Electrophilic addition. Nucleophilic addition. Radical addition. Elimination. Substitution reactions. Intramolecular rearrangements and intermolecular rearrangements. Oxidation and reduction reactions. --------------------------------------------------------------------- NITK-Course Contents(UG)2010 Page 118 of 134
NATIONAL INSTITUTE OF TECHNOLOGY KARNATAKA, SURATHAKAL ------------------------------------------------------------------------------------------------------------------ P. H. Gorggins, Unit Processes in Organic Synthesis, 5 th edition, McGraw-Hill, 1958. J. March, Advanced Organic Chemistry, 3 rd edition, McGraw Hill, New York, 1985. CY205 ORGANIC CHEMISTRY (3-0- 0) 3 Strengths of organic acids and bases. Reagents of synthetic importance. Active methylene compounds. Named organic reactions. Stereochemistry: Optical activity, asymmetric carbon, enantiomers, diastereomers, configurations and conformations. Carbohydrate chemistry: Monosaccharides, disaccharides and polysaccharides. Benzene: Structure, aromaticity, Huckel�s rule, electrophilic substitution and orientation effect. Heterocyclic compounds � five and six membered. Dyes: Colour and constitution, applications, some important dyes of different types. I. L. Finar, Organic Chemistry, Volume 1: The Fundamental Principles, VI edition, ELBS, 1989. M. K. Jain and S. C. Sharma, Organic Chemistry, Shoban Lal Chand. & Co., 2000. CY206 INSTRUMENTAL ANALYSIS LAB. (0–0–4) 2 Potentiometry. Conductometry. Colorimetry. Refractometry. Gravimetric estimations. Demonstration of UV and IR spectrophotometer. A. I.Vogel, A Text Book of Quantitative Inorganic Analysis Including Elementary Instrumental Analysis, ELBS, Longman Group, UK, III Edition, 1962. J. Basset, R. C. Denny, CH Jaffery and J. Mendhan, Vogel’s Text Book of Quantitative Inorganic Analysis, including elementary analysis, ELBS, London, 5 th Edition, 1989. CY251 POLYMER SCIENCE AND TECHNOLOGY (3–0–0) 3 Basic concepts, configuration and conformation. Thermoplastic and thermosetting polymers. Condensation, addition, coordination, ring opening, metathesis polymerization. Copolymerization. Chemical reactions of polymers and polymer degradation. Analysis and testing of polymers. Rheology and mechanical properties: Kinetic theory of rubber elasticity, glassy state and glass transition, mechanical properties, crystalline melting point, property requirements and polymer utilization. Polymer processing: Molding, extrusion, calendaring, casting, coating, thermoforming, foaming. Multipolymer systems and composites. Additives and Compounding. Fibre and elastomer technology. F. W. Billmeyer, Textbook of Polymer Science, Wiley Interscience Publication, 1984. Joel R. Fried, Polymer Science and Technology, Prentice Hall, NJ, 1995. CY252 INDUSTRIAL CHEMISTRY (3–0–0) 3 Synthetic Organic Chemical Industries: Petrochemicals � Chemicals from C1, C2, C3, C4 compounds. Chemicals from aromatics. Phenols and alkyl phenols. Isomerization, Dehydrogenation. Oxidation of paraffins. Pesticides and Pharmaceutical Industries. Polymer Industries: PE, PVC, Teflon, SBR, NBR, Neoprene, Silicone rubber, Nylon, Dacron. Starch and cellulose derivatives. Natural product industries: Oils. Soaps. Detergents. Essential oils. Paints and Varnishes. Food industries. Fermentation industries. Explosives and propellants. E. Riegel, Industrial Chemistry, 6 th ed,, J. A. End, Reinhold Publishing Corp., 1962. R. N. Shreve, Chemical Process Industries, 3 rd ed., McGraw-Hill Book, 1967. CY300 INSTRUMENTAL METHODS OF ANALYSIS (3–0–0) 3 Electroanalytical methods: Conductometric and potentiometric titrations. Polarography - theory and applications. Amperometric titrations. Spectroanalytical methods: Molecular spectra. Beer-Lambert�s law and its deviations. IR, UV-visible spectroscopy � theory, instrumentation and applications. Atomic absorption spectroscopy: Thermal methods of analysis: TGA, DTA, DTG, instrumentation and applications. Solvent extraction: Principle, distribution coefficient, separation factor and efficiency, applications. Chromatography: Paper chromatography, TLC, GC, HPLC � theory, instrumentation, experimental techniques and applications. --------------------------------------------------------------------- NITK-Course Contents(UG)2010 Page 119 of 134
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