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Strona 2_redak - Instytut Agrofizyki im. Bohdana Dobrzańskiego ...

Strona 2_redak - Instytut Agrofizyki im. Bohdana Dobrzańskiego ...

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91<br />

13.1.1. Peschl rotational split level shear tester<br />

Peschl [131] presented a promising proposal of a rotational shear apparatus with<br />

associated method of determination of mechanical properties of powders [132], and a<br />

method of quality control of powders for industrial application [133]. The author<br />

analysed existing equipment and found that some apparatuses overest<strong>im</strong>ate the values<br />

of parameters as compared to values in a full-scale installation, while others underest<strong>im</strong>ate<br />

those values. Peschl, based on his examinations of industrial powders, stated<br />

that rotational split level (RSL) shear testers give values s<strong>im</strong>ilar to those encountered<br />

in practice. In the RSL apparatus, shearing of the samples takes place through the<br />

rotational movement of the lower part of the sample against the upper part of the<br />

sample. The horizontal cross-section area of the sample equals 30 cm 2 while its<br />

volume is 45 cm 3 . With rotational movement, no l<strong>im</strong>it on shear displacement exists,<br />

and the shear plane forms in the middle of sample height where the disturbances from<br />

horizontal borders of the sample are the least. The author recommends choosing such<br />

exper<strong>im</strong>ental procedure that would most closely reflect the conditions of real process<br />

for which the material parameters are determined. Peschl preferred not to suggest<br />

any standard procedure, but offered the possibility of programming of shear<br />

conditions with automatic control of the apparatus. Procedure of data analysis<br />

allows for linear or exponential approx<strong>im</strong>ation of yield condition. For majority of<br />

easy flowing or low-cohesion materials, linear approx<strong>im</strong>ation is a sufficient solution.<br />

In such a case material parameters have a clear interpretation.<br />

Some materials are characterized by strongly non-linear yield condition in<br />

a range of low normal pressures. For this group Peschl [132] suggested linear approx<strong>im</strong>ation<br />

in two intervals. Out of straight line est<strong>im</strong>ated for the range of higher pressure<br />

the higher principal stress 1 1 should be determined, while cohesion c and unconfined<br />

yield stress 1 c should be determined out of the course of a straight line est<strong>im</strong>ated for<br />

the lower range of normal pressure. If the mentioned above do not give satisfactory<br />

accuracy of description of the yield condition, a non-linear approx<strong>im</strong>ation using<br />

exponential function is necessary. The method of approx<strong>im</strong>ation cannot be settled at<br />

advance, but must be an outcome of consideration of particular case. Peschl cla<strong>im</strong>ed<br />

that his method gave the possibility of s<strong>im</strong>ulation of all conditions existing in practice,<br />

proper determination of parameters and, consequently, reliable operation of industrial<br />

installations. The author concluded that powder technology gained the level of<br />

engineering science and allowed for design of industrial installations without beforehand<br />

exper<strong>im</strong>enting on equipment and installation.<br />

Flowability is a material property of increasing <strong>im</strong>portance. With passage of<br />

t<strong>im</strong>e, this property is more extensively used as a measure of material quality.<br />

Consumers expect constant flowability of washing powder, milk powder or sugar.<br />

For mixing, dosing and packing, stable flowability is a crucial parameter for

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