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Extraction Technologies For Medicinal And Aromatic Plants - Unido

Extraction Technologies For Medicinal And Aromatic Plants - Unido

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1 AN OVERVIEW OF EXTRACTION TECHNIQUES FOR MEDICINAL AND AROMATIC PLANTS<br />

1.3 <strong>Aromatic</strong> Plant Extracts<br />

The types of volatile isolates that are obtained commercially<br />

from aromatic plants are essential oils, concretes, absolutes, pomades<br />

and resinoids. Essential oils are isolated from plant material by distillation<br />

whereas other volatile isolates are obtained by solvent extraction.<br />

1.3.1 Concrete<br />

This is an extract of fresh fl owers, herbs, leaves and the fl owering<br />

tops of plants obtained by the use of a hydrocarbon solvent such as butane,<br />

pentane, hexane and petroleum ether. Concrete is rich in hydrocarbonsoluble<br />

material and devoid of water-soluble components. It is generally a<br />

waxy, semisolid, dark-colored material free from the original solvent.<br />

In practice, concretes are produced in static extractors. These<br />

extractors are fi tted with numerous perforated trays so that the fl owers do<br />

not get compressed by their own weight. Each perforated tray has a spacer<br />

so the number and distance between them are predetermined.<br />

The set of perforated trays can be within a removable cylindrical<br />

basket. In the centre of the lower tray, there is a rod on which the spacers<br />

and the perforated trays are fi tted while at the top there is a ring or a<br />

hook so that the entire contents of the extractor can be readily removed by<br />

a chain pulley block.<br />

While stacking the fl owers on these trays, care should be taken<br />

to minimize bruising and damage of the fl owers, because such damage can<br />

result in the release of enzymes in the fl ower juice which deteriorates the<br />

quality of concrete. The basket stacked with fl owers is inserted into the<br />

extractor and the solvent of choice is introduced from the bottom into the extractor<br />

until the material on the perforated disc assembly is completely immersed.<br />

Four to fi ve such washes are given until the material is exhausted.<br />

The enriched solvent from the extractor is pumped into an<br />

evaporator for solvent recovery and the solvent content is reduced to about<br />

one-tenth the original volume. The recovered solvent is pumped to the solvent<br />

tanks to be used again. The concentrated material from the evaporator<br />

is pumped into a vacuum evaporator where the solvent is removed more<br />

carefully under high vacuum and the recovered solvent is returned to the<br />

solvent tanks for repeated use. The resultant concrete has an odor similar<br />

to but stronger than the material from which it was extracted.<br />

In concrete manufacturing, it is a normal practice to circulate<br />

fresh solvent through a battery of extractors. At each cycle, the solvent becomes<br />

more enriched with the fl ower volatiles until extraction is complete.<br />

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