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Bechtel Hanford, Inc. 3350 George Washington Way Richland, WA 99352 April 21, 1998 Attention: Joan Kessner SAF Number Date First Sample Received Date SDG Closed Number of Samples Sample Type SDG Number Data Deliverable CERTIFICATE OF ANALYSIS B98-061 March 9, 1998 March 16, 1998 15 Other-Cement W02275 21 Day Summary °ivanterra Emironmrnra7 sen'u es lc^ In ti I. Introduction Between March 9, and March 16, 1998, 15 21-day TAT other-cement samples were received by the Quanterra Environmental Se rvices Richland Laboratory (QESRL) for radiochemical and chemical analysis. Upon receipt, the samples were assigned the following laborato r y ID numbers to correspond with the Bechtel Hanford, Inc. (BHI) specific IDs: QESRL ID Ji BHI iD# YIATRI% DATE OF RECEIPT 80316101 BON680 Soil 3/9/98 80316102 BON681 Soil 3/9/98 80318401 BON682 Soil 3/10/98 80318402 BON683 Soil 3/10'98 80318403 BON684 Soil 3/10/98 80320601 BON685 Soil 3111198 803 2 0602 BON686 Soil 3i 11.'98 80320603 BON687 Soil 3x 11 "98 80322201 BON688 Soil 3/12x98 80312 1_02 BON689 Soil 3.12.'98 80324401 BON690 Soil 3J13^98 80324402 BON691 Soil 3; 1?x98 80327201 BON692 Soil 3.16,98 80327202 BON693 Soil 3, 16,98 80327203 BON694 Soil 3116,98 r1 G0I)..
Bechtel Hanford, Inc. April 21, 1998 Page 2 II. Analytical Results/Methodology iivanterra EnOronmenral Souk , The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information, analytical results and the appropriate associated statistical errors. The requested analyses were: Alpha Spectroscopy Americium-241 by method RICH-RC-5062 Plutonium-238, -239/40 by method RICH-RC-5062 Uranium-234, -235, -238 b_y method RICH-RC-5062 Gamma Spectroscopy Gamma Scan by method RICH-RC-5017 Gas Proportional Counting Total Strontium b y method RICH-RC-5006 Liquid Scintillation Counting Carbon-14 by method RICH-RC-5022 Nickel-63 by method RICH-RC-5069 Selenium-79 by method RD-3253 Technetium-99 by method RICH-RC-5029 Chemical Analyses Chromium Hex by EPA method RICH-RC-5005 III. Quality Control The analytical results for each analysis performed under SDG WO-2 -2 75 include a minimum of two Laboratory Control Samples (LCS) and one method (reagent) blank. Any exceptions have been noted in the "Comments" section_ Quality control sample results are reported in the same units as sample results. (JO U.;
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Quanterra Incorporated 13715 Rider
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Bechtel Hanford Incorporated April
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Ouanterra April 13, 1998 10:47 am A
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I Chain of Custody Record S I CDJa'
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Y Bechtel Hanford Inc. CHAIN OF CUS
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OateRme Received: FIVISM t SAMPLE C
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Environmental Contractor Contractor
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Quanterra 6W V S 014488 Effiroameat
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1 Bechtel Hanford Inc. CHAIN OF CUS
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C^ C-3 C) 1"J Cz Client Sample Scre
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K) 'ApItN CLIENT CODE ID MATRIXRECE
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Project Manager: N. Price Ouanterra
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Ilecldel Ilan ford Inc. CHAIN OF CU
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0 J d Î C)6-3 Ilechlel Ilanforll I
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Client Sample Screening Results 12-
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uuanterra March e3, Tenn ua:ul pm P
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Bechtel Hanford Inc. I 'olleclor Il
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Bechtel Hanford Inc. CHAIN OF CUSTO
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Bechtel HanforJ Inc. CHAIN OF CUSTO
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t e, CIO RFSH-SOW-93-0003 - rJRevis
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Project Manager: U. Price wuanterra
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Bechtel Hanford Inc. CHAIN Or CUSTO
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cc* Environmental Job Vo.22172 Rest
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C^ C-J CG L7 Client Sample Screenin
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Q'Auanterra 014501 Condition Upon R
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Dr a f tM W. Price Quanterra April
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Chain of Custody Record OIIA- Al 24
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CCN: 055088 Environmental Job No. 2
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A,, -i/I fIY6 —1 ` c,ir3 Beclael
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Qyrhianterra ;ter Sty orrecti Actio
Page 69 and 70: Category: PCB's Method: EPA 8080 Ma
Page 81 and 82: Duanterra-Richland 3350 George Wash
Page 87 and 88: 1D EPA SAMPLE NO. PCB ORGANICS ANAL
Page 89 and 90: Lab Name: OUANTERRA MO Contract: La
Page 91 and 92: Lab Name: QUANTERRA,MO Contract: La
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Page 97 and 98: Lab Name: QUANTERRA,MO Contract: 55
Page 99 and 100: Lab Name: QUANTERRA MO Contract: La
Page 101 and 102: Category: Mercury Method: EPA 7471
Page 103 and 104: Category: ICAP Metals Method: EPA 6
Page 105 and 106: U.S. EPA - --LP INORGANIC ANALYSES
Page 107 and 108: U.S. EPA CLP 1 EPA SAMPLE NO - INOR
Page 109 and 110: U.S. EPA --LP 1 EPA SAMPLE NO INORG
Page 111 and 112: U.S. EPA _LP i EPA SAMPLE NO. INORG
Page 113 and 114: U.S. EPA CLP 1 EPA SAMPLE NO INORGA
Page 115 and 116: Color Before: Color After: Comments
Page 117 and 118: U. E. EPA - CT 1 EPP_ SAMPLE NO. IN
Page 119: Color Before: Color After: Comments
Page 123 and 124: Bechtel Hanford, Inc. April 1-1, 19
Page 125 and 126: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 127 and 128: ISOTOPE TC-99 AM 241 U-234 U-235 U-
Page 137 and 138: ISOTOPE TC-99 AM-241 HEXCHROME U-23
Page 139 and 140: Quanterra Data Review C3eddist RADI
Page 141 and 142: First Lc. ei Second '_z% -I Form d
Page 143 and 144: Qaaatena Data Review Checklist RADI
Page 145 and 146: QUANTERRA LABORATORY NONCONFOR:N L-
Page 147 and 148: Quanterra Data Review Cbeddist RADI
Page 149 and 150: QuanaTm Data Review Chedd ist RADIO
Page 151 and 152: Quantem Data Review CSedtEu RADIOCH
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Page 155 and 156: Richland Laborato ry Quanterra Data
Page 157 and 158: Richland Laborato ry Qanter a Data
Page 159 and 160: Richland Laboratory Quanterra Data
Page 161 and 162: Richland Laborato ry Quarteim Data
Page 163 and 164: Richland Laboratory Quanterra Data
Page 165 and 166: Richland Laborato ry ^w° ` alters
Page 167 and 168: Richland Laboratory Quante"a Data R
Page 169 and 170: CHAIN OF CUSTODY FORMS
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C cc: li.- Bechtel Hanford Inc. CHA
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Environmental Restoration ERC Team
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Frlrr 1 SAMPLE CHECK-IN UST DateMme
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C l Bechtel Hanford Inc. CHAIN OF C
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Figure 1 SAMPLE CHECK-IN LIST DateT
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(7-- C) Client Sample Screening Res
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Environmental Restoration FJ^C Cont
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Oate/7me Received: Figure 1 SAMPLE
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Figure 1 Î Date/Time Received: `l
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Figu re 1 SAMPLE CHECK-IN LIST Date
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Figure 1 SAMPLE CCK-IN LIST Date/Tl
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L^ T J CLIENT CODE ID MATRIX RECEIV
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\^ ^c CHAIN-OF-CUSTODY BATCH ANALYS
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CHAIN-OF-CUSTODY BATCH ANALYSIS REC
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^ CHAIN- O=-CUST77-`'( B?TCI- ANAL'
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BATCH SUMMARY/CHAIN OF CUSTODY 4 0
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^CUSTOMER: CHAIN-DP-CUSTODY BATCH A
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CHAIN-OF-CUSTODY BATCH ANAL`SIS REC
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^CHAIN-OF-CUSTODY BATCH ANALYSIS RE
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(j..%"uanterra BATCH SUMMARY/CHAIN
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CLIENT: PROJECT ID: Cr+6 CHAIN OF C
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CLIENT: PROJECT ID: Ci+6 CHAIN OF C
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