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ISOTOPE RESULT TC-99 1 13E+02 AM-241 3 74E+03 U-234 7 12E+01 U-235 5 94E+00 U-238 2 27E+01 PU-238 4 97E+02 PU239/40 1 34E+04 AM-241 3 72E+03 CO-60 8.22E+03 CS-137DA 1.36E+06 EU-152 9 35E+03 E U-154 1 85E+03 E U-155 -1 56E+01 STRONTIUM 4 33E+05 C-14 6.59E+02 NI-63 2.76E+05 c1 ^ SE-79 7.68E+02 ~lumber of Results: '17 Comments: COUNTING TOTAL ERROR ERROR(2s) (2 s) 10E+03 3.2E+03 5.3E+02 7.7E+02 6.6E+01 6.8E+01 2.8E+01 2.8E+01 3 8E+01 3.9E+01 1.6E+02 1.7E+02 8.2E+02 1.9E+03 2.5E+03 2.5E+03 2.7E+02 8.6E+02 1.4E+05 1.4E+05 1 SE+03 1.7E+03 3.8E+02 4.2E+02 7.7E+02 7.7E+02 6.3E+03 1.6E+0S 5 9E+02 9.1 E+02 3.7E+03 3.5E+04 7.8E+02 2.9E+03 FORM Date: 4/16/1998 SAMPLE RESULTS LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 10:00:00 AM LAB SAMPLE ID: 80320602 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11:57:00 AM CLIENT ID: BON686 ORDER NBR: B98-061 MATRIX: OTHER MDA REPORT UNIT YIELD RST/MDA RST/CNTERR ANALYSIS DATE ALIQUOT SIZE ALQ UNIT DETECTOR ID 2.40E+03 pCi/sam 95.10% 005 0.11 4/2/98 0.000626 SA LSC 5.14E+01 pCi/sam 105.50% (72.8) (7.) 4/3/98 0.000836 SA ALPHA-SPEC 898E+01 pCi/sam 73.10% 0.79 (1.1) 4/4/98 0.000839 SA ALPHA-SPEC 8.35E+01 pCi/sam 73.10% 007 0.22 4/4/98 0.000839 SA ALPHA-SPEC 7 20E+01 pCi/sam 73.10% 0.31 0.59 4/4/98 0.000839 SA ALPHA-SPEC 5.00E+01 pCi/sam 6330% (9.9) (3.2) 3/31/98 0.000836 SA ALPHA-SPEC 3.36E+01 pCi/sam 63.30% (398.7) (16.4) 3/31/98 0.000836 SA ALPHA-SPEC N/A pCilsam N/A N/A (1.5) 3/26/98 0.4107 SA GAMMA N/A pCi/sam N/A N/A (30.9) 3/26/98 0.4107 SA GAMMA N/A pCi/sam N/A N/A (10.) 3/26/98 0.4107 SA GAMMA N/A pCi/sam N/A N/A (6.4) 3/26/98 04107 SA GAMMA N/A pCi/sam N/A N/A (4.9) 3/26/98 0.4107 SA GAMMA 1.25E+03 pCi/sam N/A -0.01 -0.02 3/26/98 0.4107 SA GAMMA 8.16E+02 pCi/sam 99.90% (530.) (68.5) 4/1/98 0-000837 SA AB 1.34E+03 pCi/sam 100.00% 0.49 (1 1) 4/9/98 0.001142 SA LSC 2.00E+03 pCi/sam 76.00% (138.3) (74.3) 4/3/98 0.000831 SA LSC 1.80E+03 pCi/sam 79.50% 043 0.99 4/1/98 0.00085 SA LSC METHOD NUMBER RICHRC5078 RICHRC5057 RICHRC5030 RICHRCS030 RICHRC5030 RICHRCS010 RICHRC5010 RICHRC5017 RICHRCS017 RICHRCS017 RICHRC5017 RICHRC5017 RICHRC5017 RICHRCSW6 RICHRC5022 RICHRC5069 RICHRC5043
FORM I Date: 4/16/1998 SAMPLE RESULTS LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/11/1998 1:05:00 PM LAB SAMPLE ID: 80320603 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11'.57.00 AM CLIENT ID: BON687 ORDER NBR: B98-061 MATRIX: OTHER ISOTOPE RESULT COUNTING ERROR(2s) TOTAL ERROR (2s) MDA REPORT UNIT YIELD RSTIMDA RST/CNTERR ANALYSIS DATE ALIQUOT SIZE ALO UNIT DETECTOR ID METHOD NUMBER TC-99 -9.47E+00 2.5E+01 7.9E+01 6.04E+01 pCi/sam 95.10% -0.16 -0.37 3/31/98 0.0245 SA LSC RICHRCS078 AM-241 3.43E+00 3.1E+00 3.1E+00 186E+00 pCi/sam 93.80% (1.8) (1.1) 4/4/98 0.0245 SA ALPHA-SPEC RICHRCS057 HEXCHROME 3.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A (1.5) N/A 3/12/98 1000 ML SPECPHOTO EPA7196 U-234 4.23E+01 1.1E+01 1.4E+01 282E+00 pCilsam 47.30% (16.1) (4.) 4/4/98 0.0272 SA ALPHA-SPEC RICHRCS030 U-235 6.00E-01 1.3E+00 1.3E+00 2.62E+00 pCi/sam 47.30% 0.23 0.46 4/4/98 00272 SA ALPHA-SPEC RICHRC5030 U-238 4.88E+01 1.1E+01 1.5E+01 2.98E+00 pCi/sam 47.30% (16.4) (4.3) 4/4/98 0.0272 SA ALPHA-SPEC RICHRC5030 PU-238 8.22E-01 1.3E+00 1.3E+00 2.04E+00 pCi/sam 58.70% 0.4 0.65 4/3198 0.0255 SA ALPHA-SPEC RICHRCS010 PU239/40 7.04E+00 3.6E+00 3.7E+00 2.23E+00 pCi/sam 58.70% (3.2) (2.) 4/3/98 0.0255 SA ALPHA-SPEC RICHRC5010 CO-60 6.12E+00 3.9E+01 3.9E+01 6.99E+01 pCilsam N/A 0.09 0.16 3/27/98 0.0517 SA GAMMA RICHRC5017 CS-137DA 1.48E+03 9.8E+01 1.8E+02 N/A pCilsam N/A N/A (151) 3/27/98 0.0517 SA GAMMA RICHRCS017 EU-152 403E+01 9.2E+01 9.2E+01 1.59E+02 pCi/sam N/A 0.25 0.44 3/27/98 0.0517 SA GAMMA RICHRC5017 EU-154 -4 46E+01 1.1E+02 1.1E+02 179E+02 pCi/sam N/A -0.25 -0.41 3/27/98 0.0517 SA GAMMA RICHRC5017 EU-155 -1.89E+01 7.4E+01 7.4E+01 1 15E+02 pCi/sam N/A -0.16 -0.26 3/27/98 0.0517 SA GAMMA RICHRC5017 K-40 1.91E+03 1.1E+03 1.1E+03 N/A pCi/sam N/A N/A (1.8) 3/27/98 0.0517 SA GAMMA RICHRC5017 STRONTIUM 6.79E+02 5.1E+01 2.5E+02 3.46E+01 pCi/sam 86.30% (19.6) (13.3) 4/2/98 0.0241 SA AB RICHRC5006 C-14 9.21E+01 3.0E+01 4.5E+01 6.40E+01 pCi/sam 100.00% (1.4) (3.1) 4098 00243 SA LSC RICHRC5022 NI-63 1.60E+02 2.6E+01 8.0E+01 5.20E+01 pCi/sam 93.70% (3.1) (6.1) 4/5/98 0.0255 SA LSC RICHRCS069 Fes+ SE-79 8.50E-01 2.7E+01 97E+01 6.33E+01 pCi/sam 74.30% 0.01 0.03 4/13/98 0.0257 SA LSC RICHRC5043 C.) Number of Results: 18 Comments:
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Quanterra Incorporated 13715 Rider
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Bechtel Hanford Incorporated April
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Ouanterra April 13, 1998 10:47 am A
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I Chain of Custody Record S I CDJa'
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Y Bechtel Hanford Inc. CHAIN OF CUS
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OateRme Received: FIVISM t SAMPLE C
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Environmental Contractor Contractor
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Quanterra 6W V S 014488 Effiroameat
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1 Bechtel Hanford Inc. CHAIN OF CUS
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C^ C-3 C) 1"J Cz Client Sample Scre
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K) 'ApItN CLIENT CODE ID MATRIXRECE
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Project Manager: N. Price Ouanterra
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Ilecldel Ilan ford Inc. CHAIN OF CU
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0 J d Î C)6-3 Ilechlel Ilanforll I
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Client Sample Screening Results 12-
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uuanterra March e3, Tenn ua:ul pm P
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Bechtel Hanford Inc. I 'olleclor Il
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Bechtel Hanford Inc. CHAIN OF CUSTO
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uuanterra march ca, ivvo uo:ur pm n
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Bechtel HanforJ Inc. CHAIN OF CUSTO
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t e, CIO RFSH-SOW-93-0003 - rJRevis
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Project Manager: U. Price wuanterra
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Bechtel Hanford Inc. CHAIN Or CUSTO
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cc* Environmental Job Vo.22172 Rest
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C^ C-J CG L7 Client Sample Screenin
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Q'Auanterra 014501 Condition Upon R
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Dr a f tM W. Price Quanterra April
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Chain of Custody Record OIIA- Al 24
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CCN: 055088 Environmental Job No. 2
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A,, -i/I fIY6 —1 ` c,ir3 Beclael
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Qyrhianterra ;ter Sty orrecti Actio
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Category: PCB's Method: EPA 8080 Ma
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Page 79 and 80: Category: PCB's Method: EPA 8080 Ma
Page 81 and 82: Duanterra-Richland 3350 George Wash
Page 87 and 88: 1D EPA SAMPLE NO. PCB ORGANICS ANAL
Page 89 and 90: Lab Name: OUANTERRA MO Contract: La
Page 91 and 92: Lab Name: QUANTERRA,MO Contract: La
Page 93 and 94: Lab Name: OUANTERRA,MO Contract Lab
Page 95 and 96: Lab Name: OUANTERRA,MO Contract: La
Page 97 and 98: Lab Name: QUANTERRA,MO Contract: 55
Page 99 and 100: Lab Name: QUANTERRA MO Contract: La
Page 101 and 102: Category: Mercury Method: EPA 7471
Page 103 and 104: Category: ICAP Metals Method: EPA 6
Page 105 and 106: U.S. EPA - --LP INORGANIC ANALYSES
Page 107 and 108: U.S. EPA CLP 1 EPA SAMPLE NO - INOR
Page 109 and 110: U.S. EPA --LP 1 EPA SAMPLE NO INORG
Page 111 and 112: U.S. EPA _LP i EPA SAMPLE NO. INORG
Page 113 and 114: U.S. EPA CLP 1 EPA SAMPLE NO INORGA
Page 115 and 116: Color Before: Color After: Comments
Page 117 and 118: U. E. EPA - CT 1 EPP_ SAMPLE NO. IN
Page 119 and 120: Color Before: Color After: Comments
Page 121 and 122: Bechtel Hanford, Inc. April 21, 199
Page 123 and 124: Bechtel Hanford, Inc. April 1-1, 19
Page 125 and 126: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 127 and 128: ISOTOPE TC-99 AM 241 U-234 U-235 U-
Page 129: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 137 and 138: ISOTOPE TC-99 AM-241 HEXCHROME U-23
Page 139 and 140: Quanterra Data Review C3eddist RADI
Page 141 and 142: First Lc. ei Second '_z% -I Form d
Page 143 and 144: Qaaatena Data Review Checklist RADI
Page 145 and 146: QUANTERRA LABORATORY NONCONFOR:N L-
Page 147 and 148: Quanterra Data Review Cbeddist RADI
Page 149 and 150: QuanaTm Data Review Chedd ist RADIO
Page 151 and 152: Quantem Data Review CSedtEu RADIOCH
Page 153 and 154: First Lz:,i Rv.ietc Second '_=^ e!
Page 155 and 156: Richland Laborato ry Quanterra Data
Page 157 and 158: Richland Laborato ry Qanter a Data
Page 159 and 160: Richland Laboratory Quanterra Data
Page 161 and 162: Richland Laborato ry Quarteim Data
Page 163 and 164: Richland Laboratory Quanterra Data
Page 165 and 166: Richland Laborato ry ^w° ` alters
Page 167 and 168: Richland Laboratory Quante"a Data R
Page 169 and 170: CHAIN OF CUSTODY FORMS
Page 171 and 172: C cc: li.- Bechtel Hanford Inc. CHA
Page 173 and 174: Environmental Restoration ERC Team
Page 175 and 176: Frlrr 1 SAMPLE CHECK-IN UST DateMme
Page 177 and 178: Bechtel Hanford Inc. CHAIN OF CUSTO
Page 179 and 180: C l Bechtel Hanford Inc. CHAIN OF C
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Figure 1 SAMPLE CHECK-IN LIST DateT
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(7-- C) Client Sample Screening Res
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Environmental Restoration FJ^C Cont
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Oate/7me Received: Figure 1 SAMPLE
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n Q 0 3 X05 Cy r,-) D 3-)6& - Zed C
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^J J J -T Bechtel Hanford Inc CHAIN
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Environmental Restoration ERC ream
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Figure 1 Î Date/Time Received: `l
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(7) ^ 96 . D3 1 C'-.n, 3 Client Sam
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c) H 1Q Bechtel Hanford Inc. CHAIN
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Figu re 1 SAMPLE CHECK-IN LIST Date
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Figure 1 SAMPLE CCK-IN LIST Date/Tl
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L^ T J CLIENT CODE ID MATRIX RECEIV
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\^ ^c CHAIN-OF-CUSTODY BATCH ANALYS
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CHAIN-OF-CUSTODY BATCH ANALYSIS REC
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I ) ° 1 . ^1 -,CIlO USTOMER: BHI M
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_ __ - . sA A.nK _ Sq Sb3184i6 ESJA
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_ ^'^ ^'^ -GC S I D3- - ------- ---
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^ Lk c^ U7^-ao j ESJA621 Pr,11/24/9
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C%ivanterra Emimnmlmd Senxu BATCH S
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v't_J ESJA616 ___Pcll/24/918%.11/24
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SISSî -SS^^-- -- ESJA620 Pt,11/24/
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Olb / 3 -Zs 'Y ESJA623 - -- Pr.1112
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I ^3^^^ CHAIN-OF-CUSTODY B4TC1-i AN
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0 /qg CUSTOMER: BHI MATRIX : OTHER
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^ CHAIN- O=-CUST77-`'( B?TCI- ANAL'
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_ S A-AuA-L _-_-__ESI27495 -- X31 y
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AN+_'.,1 PECCPD—filar-194(3 5 P,
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- _ ESI27502 0.0ZS1 Pr,12/13/97 Ba,
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BATCH SUMMARY/CHAIN OF CUSTODY 4 0
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^CUSTOMER: CHAIN-DP-CUSTODY BATCH A
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^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN
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uanflerra J o3I bt S riaa BATCH SUM
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Q^^- q' ^ CUSTOMER: BHI MATRIX : OT
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CHAIN-OF-CUSTODY B%T." ANAL'ii S RE
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^!s'aanf-errs F nimnn S nim BATCH S
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-5 - 2- 45 -4 lr vv\ --pu n 1 PC 'P
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--- —... — --VOL S- Lot Dw- - 4
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f^-1^ Ole I U^ ^ SA St3 RvFl^ or3s^
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-- - ---'^p3lfr4ti3-ESF14249 ,. - -
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_ I -- _ --- ESF14:-3 r{/d.oZ •+
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-- _ ESF14256 y S Y O. of 3'} bc. O
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Gluanterra .s w. BATCH SUMMARY/CHAI
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-$*t _-AL-SR c44 CHAIN-OF-CUSTODY B
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%uanterra .Sb.iCV BATCH SUMMARY/CHA
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CHAIN-OF-CUSTODY BATCH ANAL`SIS REC
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i..T":}1M1frt::l Sen+:rx BATCH SUMM
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! **^^ SE-79 *** CHAIN-OF-CUSTODY B
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^CHAIN-OF-CUSTODY BATCH ANALYSIS RE
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(j..%"uanterra BATCH SUMMARY/CHAIN
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n/ ^j\x CHAIN-OF-CUST011`r' BAICFi
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GvJ ^) ^ II VIA// CUSTOMER MATRIX B
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' l i uani'erra E _l,st8 S Tiv BATC
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_ SF^ Aa A^ Jll,! ''CUTS G^1C
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Get
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jS A- V-D 621=
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CLIENT: PROJECT ID: CS+6 CHAIN OF C
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CLIENT: PROJECT ID: BHI_45 SAF B98-
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CLIENT: PROJECT ID: Cr+6 CHAIN OF C
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CLIENT: PROJECT ID: Ci+6 CHAIN OF C
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