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Richland Laborato ry
Qanter a Data Review Check List
METALS
Work Order Numberts): 31ffzl S7 3)11
Lab Sample Num bers or SDG: u/ .^275 4J 0
Method/Test/Parameter. U+lo ur?L L Tl?-47f
A. Initial Calibration
1. Performed at required frequency wih required number of levels?
2. Correlation coefficient within QC li
mits?
Yes No N/A 2"d Level
Review Item Review (^)
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits? L/ j
4. Initial calibration blank(ICB) analyzed immediately a fter ICV and J
concentrations of all parameters < repor ti ng limit?
B. Continuing Calibration
L CC V analyzed at required frequency and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < repot ting limit?
C. Sample Analysis
1. Were any samples with concentrations above the linear range for any p arameter
diluted and reanalyzed? v i'
2. Were all sample holding times met?
D. QC Samples i
1. All results for the prepara ti on blank below limits?
2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable ^F
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?
4. Analy tical spikes within QC limits where applicable?
5. ICP only: One se rial dilu tion performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ?
7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the
required frequencies and within limits?
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