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E. Other 1. Are all nonconformances included and noted? 2. Is the cormct date and time of analysis shown? Review Item ( Yes ( ^) 3. Did the analyst sign and date the frmt page of the analytical tmm? 4. Correct methodology used? 5. Transcrip tions chocked? No (V) N/A 20 Level Review (^) 6. Calculations checked at minimum frequenc y? 3 ^/ 7. Units checked? Comments on any "No" response: Analyst: Kw Lz e 7 ^ Ô n ^ Date: Second-Level Review: 12 Ie Date: 3/4/" Form No. CG-191. Rev. 2,1/97 page 2 of 2 Go b i
Richland Laborato ry Qanter a Data Review Check List METALS Work Order Numberts): 31ffzl S7 3)11 Lab Sample Num bers or SDG: u/ .^275 4J 0 Method/Test/Parameter. U+lo ur?L L Tl?-47f A. Initial Calibration 1. Performed at required frequency wih required number of levels? 2. Correlation coefficient within QC li mits? Yes No N/A 2"d Level Review Item Review (^) 3. Initial calibration ve rification (ICV) analyzed immediately after calibration and results within QC limits? L/ j 4. Initial calibration blank(ICB) analyzed immediately a fter ICV and J concentrations of all parameters < repor ti ng limit? B. Continuing Calibration L CC V analyzed at required frequency and all parameters within QC limits? 2. CCB analyzed at required frequency and all results < repot ting limit? C. Sample Analysis 1. Were any samples with concentrations above the linear range for any p arameter diluted and reanalyzed? v i' 2. Were all sample holding times met? D. QC Samples i 1. All results for the prepara ti on blank below limits? 2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable ^F 3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable? 4. Analy tical spikes within QC limits where applicable? 5. ICP only: One se rial dilu tion performed per SDG? 6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ? 7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the required frequencies and within limits? —I page 1 of 2 GUI U
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Quanterra Incorporated 13715 Rider
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Bechtel Hanford Incorporated April
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Ouanterra April 13, 1998 10:47 am A
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I Chain of Custody Record S I CDJa'
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Y Bechtel Hanford Inc. CHAIN OF CUS
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OateRme Received: FIVISM t SAMPLE C
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Environmental Contractor Contractor
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Quanterra 6W V S 014488 Effiroameat
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1 Bechtel Hanford Inc. CHAIN OF CUS
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C^ C-3 C) 1"J Cz Client Sample Scre
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K) 'ApItN CLIENT CODE ID MATRIXRECE
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Project Manager: N. Price Ouanterra
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Ilecldel Ilan ford Inc. CHAIN OF CU
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0 J d Î C)6-3 Ilechlel Ilanforll I
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Client Sample Screening Results 12-
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uuanterra March e3, Tenn ua:ul pm P
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Bechtel Hanford Inc. I 'olleclor Il
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Bechtel Hanford Inc. CHAIN OF CUSTO
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uuanterra march ca, ivvo uo:ur pm n
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Bechtel HanforJ Inc. CHAIN OF CUSTO
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t e, CIO RFSH-SOW-93-0003 - rJRevis
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Project Manager: U. Price wuanterra
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Bechtel Hanford Inc. CHAIN Or CUSTO
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cc* Environmental Job Vo.22172 Rest
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C^ C-J CG L7 Client Sample Screenin
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Q'Auanterra 014501 Condition Upon R
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Dr a f tM W. Price Quanterra April
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Chain of Custody Record OIIA- Al 24
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CCN: 055088 Environmental Job No. 2
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A,, -i/I fIY6 —1 ` c,ir3 Beclael
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Qyrhianterra ;ter Sty orrecti Actio
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Category: PCB's Method: EPA 8080 Ma
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Duanterra-Richland 3350 George Wash
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1D EPA SAMPLE NO. PCB ORGANICS ANAL
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Lab Name: OUANTERRA MO Contract: La
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Lab Name: QUANTERRA,MO Contract: La
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Lab Name: OUANTERRA,MO Contract Lab
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Lab Name: OUANTERRA,MO Contract: La
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Lab Name: QUANTERRA,MO Contract: 55
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Lab Name: QUANTERRA MO Contract: La
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Category: Mercury Method: EPA 7471
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Category: ICAP Metals Method: EPA 6
Page 105 and 106: U.S. EPA - --LP INORGANIC ANALYSES
Page 107 and 108: U.S. EPA CLP 1 EPA SAMPLE NO - INOR
Page 109 and 110: U.S. EPA --LP 1 EPA SAMPLE NO INORG
Page 111 and 112: U.S. EPA _LP i EPA SAMPLE NO. INORG
Page 113 and 114: U.S. EPA CLP 1 EPA SAMPLE NO INORGA
Page 115 and 116: Color Before: Color After: Comments
Page 117 and 118: U. E. EPA - CT 1 EPP_ SAMPLE NO. IN
Page 119 and 120: Color Before: Color After: Comments
Page 121 and 122: Bechtel Hanford, Inc. April 21, 199
Page 123 and 124: Bechtel Hanford, Inc. April 1-1, 19
Page 125 and 126: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 127 and 128: ISOTOPE TC-99 AM 241 U-234 U-235 U-
Page 137 and 138: ISOTOPE TC-99 AM-241 HEXCHROME U-23
Page 139 and 140: Quanterra Data Review C3eddist RADI
Page 141 and 142: First Lc. ei Second '_z% -I Form d
Page 143 and 144: Qaaatena Data Review Checklist RADI
Page 145 and 146: QUANTERRA LABORATORY NONCONFOR:N L-
Page 147 and 148: Quanterra Data Review Cbeddist RADI
Page 149 and 150: QuanaTm Data Review Chedd ist RADIO
Page 151 and 152: Quantem Data Review CSedtEu RADIOCH
Page 153 and 154: First Lz:,i Rv.ietc Second '_=^ e!
Page 155: Richland Laborato ry Quanterra Data
Page 159 and 160: Richland Laboratory Quanterra Data
Page 161 and 162: Richland Laborato ry Quarteim Data
Page 163 and 164: Richland Laboratory Quanterra Data
Page 165 and 166: Richland Laborato ry ^w° ` alters
Page 167 and 168: Richland Laboratory Quante"a Data R
Page 169 and 170: CHAIN OF CUSTODY FORMS
Page 171 and 172: C cc: li.- Bechtel Hanford Inc. CHA
Page 173 and 174: Environmental Restoration ERC Team
Page 175 and 176: Frlrr 1 SAMPLE CHECK-IN UST DateMme
Page 177 and 178: Bechtel Hanford Inc. CHAIN OF CUSTO
Page 179 and 180: C l Bechtel Hanford Inc. CHAIN OF C
Page 181 and 182: Figure 1 SAMPLE CHECK-IN LIST DateT
Page 183 and 184: (7-- C) Client Sample Screening Res
Page 187 and 188: Environmental Restoration FJ^C Cont
Page 189 and 190: Oate/7me Received: Figure 1 SAMPLE
Page 191 and 192: n Q 0 3 X05 Cy r,-) D 3-)6& - Zed C
Page 193 and 194: ^J J J -T Bechtel Hanford Inc CHAIN
Page 195 and 196: Environmental Restoration ERC ream
Page 197 and 198: Figure 1 Î Date/Time Received: `l
Page 199 and 200: (7) ^ 96 . D3 1 C'-.n, 3 Client Sam
Page 201 and 202: c) H 1Q Bechtel Hanford Inc. CHAIN
Page 203 and 204: Figu re 1 SAMPLE CHECK-IN LIST Date
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Figure 1 SAMPLE CCK-IN LIST Date/Tl
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L^ T J CLIENT CODE ID MATRIX RECEIV
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\^ ^c CHAIN-OF-CUSTODY BATCH ANALYS
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CHAIN-OF-CUSTODY BATCH ANALYSIS REC
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I ) ° 1 . ^1 -,CIlO USTOMER: BHI M
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_ __ - . sA A.nK _ Sq Sb3184i6 ESJA
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_ ^'^ ^'^ -GC S I D3- - ------- ---
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^ Lk c^ U7^-ao j ESJA621 Pr,11/24/9
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C%ivanterra Emimnmlmd Senxu BATCH S
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v't_J ESJA616 ___Pcll/24/918%.11/24
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SISSî -SS^^-- -- ESJA620 Pt,11/24/
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Olb / 3 -Zs 'Y ESJA623 - -- Pr.1112
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I ^3^^^ CHAIN-OF-CUSTODY B4TC1-i AN
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0 /qg CUSTOMER: BHI MATRIX : OTHER
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^ CHAIN- O=-CUST77-`'( B?TCI- ANAL'
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_ S A-AuA-L _-_-__ESI27495 -- X31 y
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AN+_'.,1 PECCPD—filar-194(3 5 P,
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- _ ESI27502 0.0ZS1 Pr,12/13/97 Ba,
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BATCH SUMMARY/CHAIN OF CUSTODY 4 0
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^CUSTOMER: CHAIN-DP-CUSTODY BATCH A
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^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN
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uanflerra J o3I bt S riaa BATCH SUM
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Q^^- q' ^ CUSTOMER: BHI MATRIX : OT
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CHAIN-OF-CUSTODY B%T." ANAL'ii S RE
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^!s'aanf-errs F nimnn S nim BATCH S
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Gluanterra .s w. BATCH SUMMARY/CHAI
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-$*t _-AL-SR c44 CHAIN-OF-CUSTODY B
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%uanterra .Sb.iCV BATCH SUMMARY/CHA
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CHAIN-OF-CUSTODY BATCH ANAL`SIS REC
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i..T":}1M1frt::l Sen+:rx BATCH SUMM
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! **^^ SE-79 *** CHAIN-OF-CUSTODY B
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^CHAIN-OF-CUSTODY BATCH ANALYSIS RE
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(j..%"uanterra BATCH SUMMARY/CHAIN
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n/ ^j\x CHAIN-OF-CUST011`r' BAICFi
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GvJ ^) ^ II VIA// CUSTOMER MATRIX B
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' l i uani'erra E _l,st8 S Tiv BATC
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_ SF^ Aa A^ Jll,! ''CUTS G^1C
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Get
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CLIENT: PROJECT ID: CS+6 CHAIN OF C
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CLIENT: PROJECT ID: BHI_45 SAF B98-
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CLIENT: PROJECT ID: Cr+6 CHAIN OF C
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CLIENT: PROJECT ID: Ci+6 CHAIN OF C
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