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FORM Date: 4/16/1998 SAMPLE RESULTS LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/12/1998 9:15:00 AM LAB SAMPLE ID: 80322201 REPORT NBR: 4835 RECEIVED DATE: 3/12/1998 1:53:00 PM CLIENT ID: BON688 ORDER NBR: B98-061 MATRIX: OTHER ISOTOPE RESULT TC-99 -3.92E+00 AM-241 1 42E+00 HEXCHROME 2.00E-03 U-234 3.81E+01 U-235 1.44E+00 U-238 4.34E+01 PU-238 -5.63E-02 PU239/40 1.06E+00 CO-60 5.23E+01 CS-137UA 6.18E+02 EU-152 1 68E+01 EU-154 -1.14E+01 EU-155 2.57E+01 K-40 5.80E+03 STRONTIUM 2.08E+02 C-14 2.28E+01 c-) NI-63 7.60E+01 C SE-79 -1.37E+00 h-^ "Number of Resu lts: 118 Comments: COUNTING TOTAL ERROR ERROR(2s) (2 s) 2.5E+01 7.7E+01 2.1E+00 2.1 E+00 0.0E+00 0.0E+00 9.4E+00 1.2E+01 2.0E+00 2.0E+00 1 0E+01 1.3E+01 8.0E-02 8.0E-02 1.2E+00 1.2E+00 3.6E+01 3.6E+01 8.0E+01 1.0E+02 86E+01 86E+01 1.1E+02 1.1E+02 7.5E+01 7.5E+01 7.6E+02 9.6E+02 3.1 E+01 7 5E+01 2.6E+01 4.1E+01 2.3E+01 7.1 E+01 2 6E+01 9.4E+01 REPORT MDA UNIT YIELD 5.82E+01 pCi/sam 95.10% 2.97E+00 pCi/sam 86.60% 2.00E-03 mg/L N/A 3.39E+00 pCi/sam 5480% 3.39E+00 pCi/sam 54.80% 2.61E+00 pCi/sam 54.80% 1.61 E+00 pCi/sam 72.60% 9.52E-01 pCi/sam 72.60% 7.23E+01 pCi/sam N/A N/A pCi/sam N/A 1.43E+02 pCi/sam N/A 1.87E+02 pCi/sam N/A 1.20E+02 pCi/sam N/A 172E+03 pCi/sam N/A 3.47E+01 pCi/sam 73.80% 6.00E+01 pCi/sam 100.00% 5.05E+01 pCUsam 95.10% 6.14E+01 pCi/sam 76.70% RST/MDA RST/CNTERR -007 -016 048 0.68 1- N/A (11 2) (41) 0.42 0.72 (168) (4.3) -0.04 -0.71 (i.t) 087 072 (1 5) N/A (77) 0.12 02 -006 -01 0.21 034 (3.4) (7.6) (6.) (6-8) 0.38 087 (1.5) (33) -0.02 -005 ANALYSIS DATE 3131/98 4/4/98 3/13/98 4/4/98 4/4/98 4/4/98 4/3/98 4/3/98 3/27/98 3/27/98 3/27/98 3/27/98 3/27/98 3/27/98 4/2/98 4/2/98 4/5/98 4/13/98 ALIQUOT ALQ SIZE UNIT 00254 SA 00255 SA 100.0 ML 0.0264 SA 0.0264 SA 0.0264 SA 0.0255 SA 0.0255 SA 0.0507 SA 00507 SA 0.0507 SA 00507 SA 0.0507 SA 0.0507 SA 0.0254 SA 0.0257 SA 0.0259 SA 00257 SA DETECTOR ID LSC ALPHA-SPEC SPECPHOTO ALPHA-SPEC ALPHA-SPEC ALPHA-SPEC ALPHA-SPEC ALPHA-SPEC GAMMA GAMMA eIDLllr_1 CeL1S11ra GAMMA GAMMA AB LSC LSC LSC METHOD NUMBER RICHRCS078 RICHRCS057 EPA7196 RICHRCS030 RICHRCS030 RICHRC5030 RICHRCS010 RICHRCS010 RICHRCS017 RICHRCS017 RICHRC5017 RICHRC S017 RICHRC5017 RICHRCS017 RICHRC5006 RICHRC5022 RICHRC5069 RICHRCSO43
FORM I Date: 4/16/1998 SAMPLE RESULTS LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/12/1998 1:15:00 PM LAB SAMPLE ID: 80322202 REPORT NBR: 4835 RECEIVED DATE: 3/12/1998 1:53:00 PM CLIENT ID: BON689 ORDER NBR: B98-061 MATRIX: OTHER ISOTOPE RESULT COUNTING ERROR(2s) TOTAL ERROR (2 s) MDA REPORT UNIT YIELD RST/MDA RSTICNTERR ANALYSIS DATE ALIQUOT SIZE ALQ UNIT DETECTOR ID METHOD NUMBER TC-99 2.45E+02 9.7E+02 3.0E+03 2.22E+03 pCi/sam 95.10% 0.11 0.25 4/2/98 0.000677 SA LSC RICHRC5078 AM-241 313E-03 6.6E+02 8.4E+02 140E+02 pCi/sam 86.50% (22.4) (4.7) 4/4/98 0.000655 SA ALPHA-SPEC RICHRCS057 U-234 266E+01 43E+01 4.3E+01 755E+01 pCdsam 8150% 035 0.62 4/4198 0.000662 SA ALPHA-SPEC RICHRC5030 U-235 0.00E+00 0.0E+00 4.5E+01 4.10E+01 pCi/sam 81.50% 0. N/A 4/4/98 0.000662 SA ALPHA-SPEC RICHRC5030 U-238 5.81 E+01 6.1 E+01 6.1 E+01 6.92E+01 pCi/sam 81,50% 0.84 0.96 4/4/98 0.000662 SA ALPHA-SPEC RICHRCS030 PU-238 214E+02 1.1E+02 1.2E+02 6.59E+01 pCi/sam 70.80% (3.2) (1.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010 PU239/40 6.89E+03 6.3E+02 1.1E+03 7.19E+01 pCi/sam 70.80% (95.8) (10.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010 AM-241 2.75E+03 4.7E+02 5.4E+02 N/A pCi/sam N/A N/A (5.9) 3/26198 0.42 SA GAMMA RICHRC5017 CO-60 3.83E+03 1.8E+02 4.2E+02 N/A pCi/sam N/A N/A (21.7) 3/26/98 0.42 SA GAMMA RICHRC5017 CS-137DA 6.16E+05 1.9E+03 6.2E+04 N/A pCi/sam N/A N/A (320.5) 3/26198 0.42 SA GAMMA RICHRC5017 EU-152 6.96E+03 8.6E-02 1.1E+03 WA pCi/sam N/A N/A (8.1) 3/26198 042 SA GAMMA RICHRC5017 EU-154 1 74E+03 2.0E+02 2.7E+02 4.53E+02 pCUsam N/A (3.8) (8.7) 3/26/98 0.42 SA GAMMA RICHRC5017 EU-155 1.34E+02 3.3E+02 3.3E+02 5.05E+02 pCi/sam N/A 0.27 0.41 3/26/98 0.42 SA GAMMA RICHRC5017 STRONTIUM 4.06E+05 70E+03 1.5E+05 1.02E+03 pCi/sam 94.20% (3991) (58.2) 4/1/98 0.000661 SA AB RICHRC5006 0-14 3.75E+01 6.0E+02 9.3E+02 1 42E+03 pCi/sam 100.00% 0.03 0.06 4/9/98 0.001081 SA LSC RICHRC5022 c: NI-63 2.23E+05 3.7E+03 2.9E+04 2.42E+03 pCi/sam 77.30% (923) (60.) 413/98 0000675 SA LSC RICHRC5069 O I,_ SE-79 -6.38E+02 10E+03 38E+03 244E+03 pCi/sam 76.00% -026 -0.63 4/1/98 0000657 SA LSC RICHRC5043 G Number of Results: 17 Cov ents:
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Quanterra Incorporated 13715 Rider
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Bechtel Hanford Incorporated April
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Ouanterra April 13, 1998 10:47 am A
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I Chain of Custody Record S I CDJa'
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Y Bechtel Hanford Inc. CHAIN OF CUS
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OateRme Received: FIVISM t SAMPLE C
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Environmental Contractor Contractor
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Quanterra 6W V S 014488 Effiroameat
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1 Bechtel Hanford Inc. CHAIN OF CUS
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C^ C-3 C) 1"J Cz Client Sample Scre
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K) 'ApItN CLIENT CODE ID MATRIXRECE
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Project Manager: N. Price Ouanterra
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Ilecldel Ilan ford Inc. CHAIN OF CU
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0 J d Î C)6-3 Ilechlel Ilanforll I
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Client Sample Screening Results 12-
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uuanterra March e3, Tenn ua:ul pm P
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Bechtel Hanford Inc. I 'olleclor Il
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Bechtel Hanford Inc. CHAIN OF CUSTO
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uuanterra march ca, ivvo uo:ur pm n
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Bechtel HanforJ Inc. CHAIN OF CUSTO
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t e, CIO RFSH-SOW-93-0003 - rJRevis
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Project Manager: U. Price wuanterra
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Bechtel Hanford Inc. CHAIN Or CUSTO
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cc* Environmental Job Vo.22172 Rest
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C^ C-J CG L7 Client Sample Screenin
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Q'Auanterra 014501 Condition Upon R
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Dr a f tM W. Price Quanterra April
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Chain of Custody Record OIIA- Al 24
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CCN: 055088 Environmental Job No. 2
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A,, -i/I fIY6 —1 ` c,ir3 Beclael
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Qyrhianterra ;ter Sty orrecti Actio
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Category: PCB's Method: EPA 8080 Ma
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Page 81 and 82: Duanterra-Richland 3350 George Wash
Page 83 and 84: Category: PCB's Method: EPA 8080 Ma
Page 85 and 86: Category: PCB's Method: EPA 8080 Ma
Page 87 and 88: 1D EPA SAMPLE NO. PCB ORGANICS ANAL
Page 89 and 90: Lab Name: OUANTERRA MO Contract: La
Page 91 and 92: Lab Name: QUANTERRA,MO Contract: La
Page 93 and 94: Lab Name: OUANTERRA,MO Contract Lab
Page 95 and 96: Lab Name: OUANTERRA,MO Contract: La
Page 97 and 98: Lab Name: QUANTERRA,MO Contract: 55
Page 99 and 100: Lab Name: QUANTERRA MO Contract: La
Page 101 and 102: Category: Mercury Method: EPA 7471
Page 103 and 104: Category: ICAP Metals Method: EPA 6
Page 105 and 106: U.S. EPA - --LP INORGANIC ANALYSES
Page 107 and 108: U.S. EPA CLP 1 EPA SAMPLE NO - INOR
Page 109 and 110: U.S. EPA --LP 1 EPA SAMPLE NO INORG
Page 111 and 112: U.S. EPA _LP i EPA SAMPLE NO. INORG
Page 113 and 114: U.S. EPA CLP 1 EPA SAMPLE NO INORGA
Page 115 and 116: Color Before: Color After: Comments
Page 117 and 118: U. E. EPA - CT 1 EPP_ SAMPLE NO. IN
Page 119 and 120: Color Before: Color After: Comments
Page 121 and 122: Bechtel Hanford, Inc. April 21, 199
Page 123 and 124: Bechtel Hanford, Inc. April 1-1, 19
Page 125 and 126: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 127 and 128: ISOTOPE TC-99 AM 241 U-234 U-235 U-
Page 131: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 137 and 138: ISOTOPE TC-99 AM-241 HEXCHROME U-23
Page 139 and 140: Quanterra Data Review C3eddist RADI
Page 141 and 142: First Lc. ei Second '_z% -I Form d
Page 143 and 144: Qaaatena Data Review Checklist RADI
Page 145 and 146: QUANTERRA LABORATORY NONCONFOR:N L-
Page 147 and 148: Quanterra Data Review Cbeddist RADI
Page 149 and 150: QuanaTm Data Review Chedd ist RADIO
Page 151 and 152: Quantem Data Review CSedtEu RADIOCH
Page 153 and 154: First Lz:,i Rv.ietc Second '_=^ e!
Page 155 and 156: Richland Laborato ry Quanterra Data
Page 157 and 158: Richland Laborato ry Qanter a Data
Page 159 and 160: Richland Laboratory Quanterra Data
Page 161 and 162: Richland Laborato ry Quarteim Data
Page 163 and 164: Richland Laboratory Quanterra Data
Page 165 and 166: Richland Laborato ry ^w° ` alters
Page 167 and 168: Richland Laboratory Quante"a Data R
Page 169 and 170: CHAIN OF CUSTODY FORMS
Page 171 and 172: C cc: li.- Bechtel Hanford Inc. CHA
Page 173 and 174: Environmental Restoration ERC Team
Page 175 and 176: Frlrr 1 SAMPLE CHECK-IN UST DateMme
Page 177 and 178: Bechtel Hanford Inc. CHAIN OF CUSTO
Page 179 and 180: C l Bechtel Hanford Inc. CHAIN OF C
Page 181 and 182: Figure 1 SAMPLE CHECK-IN LIST DateT
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(7-- C) Client Sample Screening Res
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Environmental Restoration FJ^C Cont
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Oate/7me Received: Figure 1 SAMPLE
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n Q 0 3 X05 Cy r,-) D 3-)6& - Zed C
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^J J J -T Bechtel Hanford Inc CHAIN
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Environmental Restoration ERC ream
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Figure 1 Î Date/Time Received: `l
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(7) ^ 96 . D3 1 C'-.n, 3 Client Sam
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c) H 1Q Bechtel Hanford Inc. CHAIN
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Figu re 1 SAMPLE CHECK-IN LIST Date
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Figure 1 SAMPLE CCK-IN LIST Date/Tl
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L^ T J CLIENT CODE ID MATRIX RECEIV
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\^ ^c CHAIN-OF-CUSTODY BATCH ANALYS
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CHAIN-OF-CUSTODY BATCH ANALYSIS REC
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I ) ° 1 . ^1 -,CIlO USTOMER: BHI M
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_ __ - . sA A.nK _ Sq Sb3184i6 ESJA
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_ ^'^ ^'^ -GC S I D3- - ------- ---
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^ Lk c^ U7^-ao j ESJA621 Pr,11/24/9
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C%ivanterra Emimnmlmd Senxu BATCH S
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v't_J ESJA616 ___Pcll/24/918%.11/24
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SISSî -SS^^-- -- ESJA620 Pt,11/24/
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Olb / 3 -Zs 'Y ESJA623 - -- Pr.1112
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I ^3^^^ CHAIN-OF-CUSTODY B4TC1-i AN
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0 /qg CUSTOMER: BHI MATRIX : OTHER
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^ CHAIN- O=-CUST77-`'( B?TCI- ANAL'
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_ S A-AuA-L _-_-__ESI27495 -- X31 y
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AN+_'.,1 PECCPD—filar-194(3 5 P,
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- _ ESI27502 0.0ZS1 Pr,12/13/97 Ba,
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BATCH SUMMARY/CHAIN OF CUSTODY 4 0
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^CUSTOMER: CHAIN-DP-CUSTODY BATCH A
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^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN
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uanflerra J o3I bt S riaa BATCH SUM
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Q^^- q' ^ CUSTOMER: BHI MATRIX : OT
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CHAIN-OF-CUSTODY B%T." ANAL'ii S RE
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^!s'aanf-errs F nimnn S nim BATCH S
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-5 - 2- 45 -4 lr vv\ --pu n 1 PC 'P
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--- —... — --VOL S- Lot Dw- - 4
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f^-1^ Ole I U^ ^ SA St3 RvFl^ or3s^
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-- - ---'^p3lfr4ti3-ESF14249 ,. - -
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-- _ ESF14256 y S Y O. of 3'} bc. O
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Gluanterra .s w. BATCH SUMMARY/CHAI
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-$*t _-AL-SR c44 CHAIN-OF-CUSTODY B
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%uanterra .Sb.iCV BATCH SUMMARY/CHA
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CHAIN-OF-CUSTODY BATCH ANAL`SIS REC
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i..T":}1M1frt::l Sen+:rx BATCH SUMM
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! **^^ SE-79 *** CHAIN-OF-CUSTODY B
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^CHAIN-OF-CUSTODY BATCH ANALYSIS RE
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(j..%"uanterra BATCH SUMMARY/CHAIN
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n/ ^j\x CHAIN-OF-CUST011`r' BAICFi
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GvJ ^) ^ II VIA// CUSTOMER MATRIX B
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' l i uani'erra E _l,st8 S Tiv BATC
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_ SF^ Aa A^ Jll,! ''CUTS G^1C
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Get
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jS A- V-D 621=
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CLIENT: PROJECT ID: CS+6 CHAIN OF C
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CLIENT: PROJECT ID: BHI_45 SAF B98-
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CLIENT: PROJECT ID: Cr+6 CHAIN OF C
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CLIENT: PROJECT ID: Ci+6 CHAIN OF C
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