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Bechtel <strong>Hanford</strong> Incorporated April 21, 1998 Project Number: 550.260 SDG: W02275 Page 2 imbanterra Emironmental Services The liquid phase of the samples were placed in containers and put on hold for the following sample IDs: St. LouisID BHI ID Richland ID Matrix Date of Receipt 17199-003 BON681 FILTRATE 80316002 Liquid 09-MAR-98 17221-003 BON690 FILTRATE 80324301 Liquid 13-MAR-98 17221-004 BON691 FILTRATE 80324302 Liquid 13-MAR-98 17224-005 BON693 FILTRATE 80327102 Liquid 16-MAR-98 17224-006 BON694 FILTRATE 80327103 Liquid 16-MAR-98 1I. Analytical Results/ Methodology The analytical results for this report are presented by analytical test. Each set of data includes sample identification information, analytical results and the appropriate detection limits. Analyses requested PCBs (Aroelor-1254) by EPA 8080. ICP-Trace Metals (Lead) by EPA Method 6010. Mercury by EPA Method 7471. III. Quality Control A Laboratory Control Sample and Method Blank were analyzed with each preparation batch MatrixSpike and Matrix Spike Duplicate analyses were performed per the protocol for each analyte in this SDG. IV. Definitions The following codes were used to denote laboratory quality control samples and can he found in the data summary secti-)n of this report: QCBLK- Quality Control Blank, Method Blank QCLCS- Quality Control Laborator y Control Sample. Blank Spike V. Comments 0 000 63
Bechtel <strong>Hanford</strong> Incorporated April 21. 1998 Project Number: 550.260 SDG: W02275 Page 3 f,mbanterra Environmental Som, e, Shipping and Receiving There are no comments or nonconformances associated with the shipping and receivin g of these samples. Wet Chemistry Percent Moisture analyses for the solid phase samples were requested after the priority results were reported. A Percent Moisture report was transmitted by facsimile on April 13, 1998. PCBs There are no comments or nonconformances associated with this analysis. Metals Percent solids was not determined for the samples in SDG W02275. Due to software configuration, the CLP forms list solid sample result units as " dry weight" and `7 solids as " 100 ". The results on the forms are actually mg/Kg as is and are not corrected for percent solids. The figure of 100 was used as percent solids for calculation purposes only and does not represent measured solids content of the samples. The percent difference for the Lead serial dilution (12.9) was greater than 10. therefore all associated data was flagged with a "E". I certify that this data package is in compliance %vith the SOW. hoth technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee. as verified by the following signature. Reviewed and approved: Robert E. White Project Manager 000-00y
Page 1: Quanterra Incorporated 13715 Rider
Page 5 and 6: Ouanterra April 13, 1998 10:47 am A
Page 7 and 8: I Chain of Custody Record S I CDJa'
Page 9 and 10: Y Bechtel Hanford Inc. CHAIN OF CUS
Page 11 and 12: OateRme Received: FIVISM t SAMPLE C
Page 13 and 14: Environmental Contractor Contractor
Page 15 and 16: Quanterra 6W V S 014488 Effiroameat
Page 17 and 18: 1 Bechtel Hanford Inc. CHAIN OF CUS
Page 19 and 20: C^ C-3 C) 1"J Cz Client Sample Scre
Page 21 and 22: K) 'ApItN CLIENT CODE ID MATRIXRECE
Page 23 and 24: Project Manager: N. Price Ouanterra
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Page 29 and 30: Client Sample Screening Results 12-
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Page 45 and 46: Project Manager: U. Price wuanterra
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Q'Auanterra 014501 Condition Upon R
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Dr a f tM W. Price Quanterra April
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Chain of Custody Record OIIA- Al 24
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Bechtel Hanford Inc. CHAIN OF CUSTO
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CCN: 055088 Environmental Job No. 2
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Client Sample Screening Results 17-
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A,, -i/I fIY6 —1 ` c,ir3 Beclael
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Qyrhianterra ;ter Sty orrecti Actio
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Category: PCB's Method: EPA 8080 Ma
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Duanterra-Richland 3350 George Wash
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1D EPA SAMPLE NO. PCB ORGANICS ANAL
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Lab Name: OUANTERRA MO Contract: La
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Lab Name: QUANTERRA,MO Contract: La
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Lab Name: OUANTERRA,MO Contract Lab
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Lab Name: OUANTERRA,MO Contract: La
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Lab Name: QUANTERRA,MO Contract: 55
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Lab Name: QUANTERRA MO Contract: La
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Category: Mercury Method: EPA 7471
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Category: ICAP Metals Method: EPA 6
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U.S. EPA - --LP INORGANIC ANALYSES
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U.S. EPA CLP 1 EPA SAMPLE NO - INOR
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U.S. EPA --LP 1 EPA SAMPLE NO INORG
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U.S. EPA _LP i EPA SAMPLE NO. INORG
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U.S. EPA CLP 1 EPA SAMPLE NO INORGA
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Color Before: Color After: Comments
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U. E. EPA - CT 1 EPP_ SAMPLE NO. IN
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Color Before: Color After: Comments
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Bechtel Hanford, Inc. April 21, 199
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Bechtel Hanford, Inc. April 1-1, 19
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FORM I Date: 4/16/1998 SAMPLE RESUL
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ISOTOPE TC-99 AM 241 U-234 U-235 U-
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ISOTOPE TC-99 AM-241 HEXCHROME U-23
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Quanterra Data Review C3eddist RADI
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First Lc. ei Second '_z% -I Form d
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Qaaatena Data Review Checklist RADI
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QUANTERRA LABORATORY NONCONFOR:N L-
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Quanterra Data Review Cbeddist RADI
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QuanaTm Data Review Chedd ist RADIO
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Quantem Data Review CSedtEu RADIOCH
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First Lz:,i Rv.ietc Second '_=^ e!
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Richland Laborato ry Quanterra Data
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Richland Laborato ry Qanter a Data
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Richland Laboratory Quanterra Data
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Richland Laborato ry Quarteim Data
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Richland Laboratory Quanterra Data
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Richland Laborato ry ^w° ` alters
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Richland Laboratory Quante"a Data R
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CHAIN OF CUSTODY FORMS
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C cc: li.- Bechtel Hanford Inc. CHA
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Environmental Restoration ERC Team
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Frlrr 1 SAMPLE CHECK-IN UST DateMme
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C l Bechtel Hanford Inc. CHAIN OF C
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Figure 1 SAMPLE CHECK-IN LIST DateT
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(7-- C) Client Sample Screening Res
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Environmental Restoration FJ^C Cont
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Oate/7me Received: Figure 1 SAMPLE
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Figure 1 Î Date/Time Received: `l
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c) H 1Q Bechtel Hanford Inc. CHAIN
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Figu re 1 SAMPLE CHECK-IN LIST Date
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Figure 1 SAMPLE CCK-IN LIST Date/Tl
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L^ T J CLIENT CODE ID MATRIX RECEIV
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\^ ^c CHAIN-OF-CUSTODY BATCH ANALYS
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CHAIN-OF-CUSTODY BATCH ANALYSIS REC
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I ^3^^^ CHAIN-OF-CUSTODY B4TC1-i AN
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0 /qg CUSTOMER: BHI MATRIX : OTHER
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^ CHAIN- O=-CUST77-`'( B?TCI- ANAL'
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BATCH SUMMARY/CHAIN OF CUSTODY 4 0
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^CUSTOMER: CHAIN-DP-CUSTODY BATCH A
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uanflerra J o3I bt S riaa BATCH SUM
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CHAIN-OF-CUSTODY B%T." ANAL'ii S RE
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CLIENT: PROJECT ID: Cr+6 CHAIN OF C
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CLIENT: PROJECT ID: Ci+6 CHAIN OF C
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