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Richland Laborato ry
Quarteim Data Review Check List
METALS
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Work Order Num ber(sl: ZbL gp
Lab Sample Numbers or SDG: ^^ W O
Method/Test/Parameter:
A. Initial Calibration
1. Performed at required frequency wih requited number of levels?
2. Correlation coefficient within QC limits?
Yes No N/A 2°a Level
Review Item (`) Review (v)
3. Initial calibration ve ri fication (ICV) analyzed immediately after calibration
and results within QC limits?
4. Initial calibration blank( ICB) analyzed immediately after ICV and
concentrations of all parameters < reporting limit?
B. Continuing Calibration
1. CCV analyzed at required frequen cy and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < repor ting limit?
C. Sample Analysis
L Were any samples with con centrations above the linear range for any p arameter
diluted and reanalyzed? v
2. Were all sample holding ti
mes met?
D. QC Samples
L All results for the prepara tion blank below limits?
2. MS or MS/MSD recove ries within QC limits and °/d2PD (for MSD) acceptable? py
3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable?
4. Analytical spikes within QC limits where applicable?
5. ICP only: One se rial dilu tion performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency ?
7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the
re aired fre uencies and within C limits? `/
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