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Richland Laborato ry
Quanterra Data Review Check List
Work Order Number(sl: 9'U3
Lab Sample Numbers or SDG: ^Z / 7
Method/TestiParameter. e^f^
A. Initial Calibration
METALS
vyZ ^^
Review Item
1. Performed at required frequency wih required number of levels?
2. Correlation coefficient within QC limits?
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits? V
4. Initial calibration blank(ICB) analyzed immediately after ICV and
concentrations of all paramete rs < reporting limit?
B. Continuing Calibration
1. CC V analyzed at required frequency and all parameters within QC lirnits?
2. CCB analyzed at required frequen cy and all results < reporting limit?
C. Sample Analysis
1. Were any samples with concentrations above the linear range for any parameter
diluted and reanalyzed?
Yes
V)
No
(V)
N/A 2nd Level
Review ( 3 ^
2. Were all sample holding times met? i
D. QC Samples
1. All results for the preparation blank below limits?
2. MS or MS/NISI) recove ries within QC limits and n/aRPD (forMSD) acceptable ^C
3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable?
4. Analytical spikes within QC li
mits where applicable?
S. ICP only: One se rial dilution performed per SDG?
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ?
7. ICP only: Interference check samples GCSA, ICSAB) and FECAL analyzed at the
re uired fre uencies and within 9C limits?
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