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Richland Laboratory
Quante"a Data Review Check List
METALS
Work Order Number(sl: X '.
lab Sample Numbers or SDG: U) L2275
Method/Test/Parameter: '
A. Ini tial Calibration
1. Performed at required frequency wih required num ber of levels?
2. Correlation coefficient within QC limits?
Yes No N/A 2°d Level
Review Item Review ( 3 )
3. Initial calibration ve rification (ICV) analyzed immediately after calibration
and results within QC limits?
4. Initial calibration blank(ICB) analyzed immediately after ICV and
concentrations of all parameters < reporting limit? 3
B. Continuing Calibration
1. CCV analyzed at required frequency and all parameters within QC limits?
2. CCB analyzed at required frequency and all results < repor ting limit?
C. Sample Analysis
I. Were any samples with concen tra ti
ons above the linear range for any parameter
diluted and reanalyzed?
t/ 3
2. Were all sample holding ti mes met? j
D. QC Samples lj
1. All results for the prepara ti
on blank below limits?
2. MS or MSQvISD recove ries within QC li
mits and °/dtPD (for MSD) acceptable?!! 1 F
3. LCS percent recovery within QC limits and °/gRPD (for LCSD) acceptable? I I —^
4. Analytical spikes within QC limits where applicable? 3
5. ICP only: One serial dilu tion performed per SDG? 3 j _
6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy?
7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the Lj
re uired fre uencies and within C limits?
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