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E. Other 1. Are a ll nonconformances included and noted? 2. Is the correct date and time of analysis shown? 3. Did the analyst sign and date the from page of the analy tical run? 4. Correct methodology used? 5. Transc riptions chocked? Rem Item Yes No N/A 224 Level Review (V) 6. Calculations checked at minimum 5squmcy? 7. Units checked? j Comments on any "No" m6ponse: Analyst: ^Q7^P ` 41 d 3 Second-Level Review: âl^f p Form No. CG-191. Rev. 2, 1/97 Date: 3 z/ fzpz Date: 31145 page 2 of 2 6 0 7 3 I
Richland Laborato ry Quarteim Data Review Check List METALS _^b!_31 i srLf ^_ Work Order Num ber(sl: ZbL gp Lab Sample Numbers or SDG: ^^ W O Method/Test/Parameter: A. Initial Calibration 1. Performed at required frequency wih requited number of levels? 2. Correlation coefficient within QC limits? Yes No N/A 2°a Level Review Item (`) Review (v) 3. Initial calibration ve ri fication (ICV) analyzed immediately after calibration and results within QC limits? 4. Initial calibration blank( ICB) analyzed immediately after ICV and concentrations of all parameters < reporting limit? B. Continuing Calibration 1. CCV analyzed at required frequen cy and all parameters within QC limits? 2. CCB analyzed at required frequency and all results < repor ting limit? C. Sample Analysis L Were any samples with con centrations above the linear range for any p arameter diluted and reanalyzed? v 2. Were all sample holding ti mes met? D. QC Samples L All results for the prepara tion blank below limits? 2. MS or MS/MSD recove ries within QC limits and °/d2PD (for MSD) acceptable? py 3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable? 4. Analytical spikes within QC limits where applicable? 5. ICP only: One se rial dilu tion performed per SDG? 6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency ? 7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the re aired fre uencies and within C limits? `/ I 3 i ^^ page 1 of 2 60! 4 —i _r P,
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Quanterra Incorporated 13715 Rider
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Bechtel Hanford Incorporated April
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Ouanterra April 13, 1998 10:47 am A
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I Chain of Custody Record S I CDJa'
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Y Bechtel Hanford Inc. CHAIN OF CUS
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OateRme Received: FIVISM t SAMPLE C
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Environmental Contractor Contractor
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Quanterra 6W V S 014488 Effiroameat
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1 Bechtel Hanford Inc. CHAIN OF CUS
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C^ C-3 C) 1"J Cz Client Sample Scre
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K) 'ApItN CLIENT CODE ID MATRIXRECE
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Project Manager: N. Price Ouanterra
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Ilecldel Ilan ford Inc. CHAIN OF CU
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0 J d Î C)6-3 Ilechlel Ilanforll I
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Client Sample Screening Results 12-
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uuanterra March e3, Tenn ua:ul pm P
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Bechtel Hanford Inc. I 'olleclor Il
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Bechtel Hanford Inc. CHAIN OF CUSTO
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uuanterra march ca, ivvo uo:ur pm n
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Bechtel HanforJ Inc. CHAIN OF CUSTO
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t e, CIO RFSH-SOW-93-0003 - rJRevis
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Project Manager: U. Price wuanterra
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Bechtel Hanford Inc. CHAIN Or CUSTO
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cc* Environmental Job Vo.22172 Rest
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C^ C-J CG L7 Client Sample Screenin
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Q'Auanterra 014501 Condition Upon R
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Dr a f tM W. Price Quanterra April
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Chain of Custody Record OIIA- Al 24
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Bechtel Hanford Inc. CHAIN OF CUSTO
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CCN: 055088 Environmental Job No. 2
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A,, -i/I fIY6 —1 ` c,ir3 Beclael
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Qyrhianterra ;ter Sty orrecti Actio
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Category: PCB's Method: EPA 8080 Ma
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Duanterra-Richland 3350 George Wash
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1D EPA SAMPLE NO. PCB ORGANICS ANAL
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Lab Name: OUANTERRA MO Contract: La
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Lab Name: QUANTERRA,MO Contract: La
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Lab Name: OUANTERRA,MO Contract Lab
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Lab Name: OUANTERRA,MO Contract: La
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Lab Name: QUANTERRA,MO Contract: 55
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Lab Name: QUANTERRA MO Contract: La
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Category: Mercury Method: EPA 7471
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Category: ICAP Metals Method: EPA 6
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U.S. EPA - --LP INORGANIC ANALYSES
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U.S. EPA CLP 1 EPA SAMPLE NO - INOR
Page 109 and 110: U.S. EPA --LP 1 EPA SAMPLE NO INORG
Page 111 and 112: U.S. EPA _LP i EPA SAMPLE NO. INORG
Page 113 and 114: U.S. EPA CLP 1 EPA SAMPLE NO INORGA
Page 115 and 116: Color Before: Color After: Comments
Page 117 and 118: U. E. EPA - CT 1 EPP_ SAMPLE NO. IN
Page 119 and 120: Color Before: Color After: Comments
Page 121 and 122: Bechtel Hanford, Inc. April 21, 199
Page 123 and 124: Bechtel Hanford, Inc. April 1-1, 19
Page 125 and 126: FORM I Date: 4/16/1998 SAMPLE RESUL
Page 127 and 128: ISOTOPE TC-99 AM 241 U-234 U-235 U-
Page 137 and 138: ISOTOPE TC-99 AM-241 HEXCHROME U-23
Page 139 and 140: Quanterra Data Review C3eddist RADI
Page 141 and 142: First Lc. ei Second '_z% -I Form d
Page 143 and 144: Qaaatena Data Review Checklist RADI
Page 145 and 146: QUANTERRA LABORATORY NONCONFOR:N L-
Page 147 and 148: Quanterra Data Review Cbeddist RADI
Page 149 and 150: QuanaTm Data Review Chedd ist RADIO
Page 151 and 152: Quantem Data Review CSedtEu RADIOCH
Page 153 and 154: First Lz:,i Rv.ietc Second '_=^ e!
Page 155 and 156: Richland Laborato ry Quanterra Data
Page 157 and 158: Richland Laborato ry Qanter a Data
Page 159: Richland Laboratory Quanterra Data
Page 163 and 164: Richland Laboratory Quanterra Data
Page 165 and 166: Richland Laborato ry ^w° ` alters
Page 167 and 168: Richland Laboratory Quante"a Data R
Page 169 and 170: CHAIN OF CUSTODY FORMS
Page 171 and 172: C cc: li.- Bechtel Hanford Inc. CHA
Page 173 and 174: Environmental Restoration ERC Team
Page 175 and 176: Frlrr 1 SAMPLE CHECK-IN UST DateMme
Page 177 and 178: Bechtel Hanford Inc. CHAIN OF CUSTO
Page 179 and 180: C l Bechtel Hanford Inc. CHAIN OF C
Page 181 and 182: Figure 1 SAMPLE CHECK-IN LIST DateT
Page 183 and 184: (7-- C) Client Sample Screening Res
Page 187 and 188: Environmental Restoration FJ^C Cont
Page 189 and 190: Oate/7me Received: Figure 1 SAMPLE
Page 191 and 192: n Q 0 3 X05 Cy r,-) D 3-)6& - Zed C
Page 193 and 194: ^J J J -T Bechtel Hanford Inc CHAIN
Page 195 and 196: Environmental Restoration ERC ream
Page 197 and 198: Figure 1 Î Date/Time Received: `l
Page 199 and 200: (7) ^ 96 . D3 1 C'-.n, 3 Client Sam
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Page 203 and 204: Figu re 1 SAMPLE CHECK-IN LIST Date
Page 209 and 210: Figure 1 SAMPLE CCK-IN LIST Date/Tl
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L^ T J CLIENT CODE ID MATRIX RECEIV
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\^ ^c CHAIN-OF-CUSTODY BATCH ANALYS
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CHAIN-OF-CUSTODY BATCH ANALYSIS REC
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I ) ° 1 . ^1 -,CIlO USTOMER: BHI M
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^ Lk c^ U7^-ao j ESJA621 Pr,11/24/9
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C%ivanterra Emimnmlmd Senxu BATCH S
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v't_J ESJA616 ___Pcll/24/918%.11/24
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SISSî -SS^^-- -- ESJA620 Pt,11/24/
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Olb / 3 -Zs 'Y ESJA623 - -- Pr.1112
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I ^3^^^ CHAIN-OF-CUSTODY B4TC1-i AN
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0 /qg CUSTOMER: BHI MATRIX : OTHER
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^ CHAIN- O=-CUST77-`'( B?TCI- ANAL'
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AN+_'.,1 PECCPD—filar-194(3 5 P,
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- _ ESI27502 0.0ZS1 Pr,12/13/97 Ba,
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BATCH SUMMARY/CHAIN OF CUSTODY 4 0
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^CUSTOMER: CHAIN-DP-CUSTODY BATCH A
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^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN
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uanflerra J o3I bt S riaa BATCH SUM
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Q^^- q' ^ CUSTOMER: BHI MATRIX : OT
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CHAIN-OF-CUSTODY B%T." ANAL'ii S RE
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^!s'aanf-errs F nimnn S nim BATCH S
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Gluanterra .s w. BATCH SUMMARY/CHAI
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-$*t _-AL-SR c44 CHAIN-OF-CUSTODY B
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%uanterra .Sb.iCV BATCH SUMMARY/CHA
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CHAIN-OF-CUSTODY BATCH ANAL`SIS REC
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i..T":}1M1frt::l Sen+:rx BATCH SUMM
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! **^^ SE-79 *** CHAIN-OF-CUSTODY B
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^CHAIN-OF-CUSTODY BATCH ANALYSIS RE
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(j..%"uanterra BATCH SUMMARY/CHAIN
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n/ ^j\x CHAIN-OF-CUST011`r' BAICFi
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GvJ ^) ^ II VIA// CUSTOMER MATRIX B
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CLIENT: PROJECT ID: CS+6 CHAIN OF C
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CLIENT: PROJECT ID: BHI_45 SAF B98-
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CLIENT: PROJECT ID: Cr+6 CHAIN OF C
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CLIENT: PROJECT ID: Ci+6 CHAIN OF C
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