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a study of the quality of a local herbal tea and volatiles of parinari ...

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4.3.2.1 Identity <strong>of</strong> volatile compounds extracted from S. cocculoides fruits<br />

using SPME <strong>and</strong> CFMD methods<br />

The volatile constituents <strong>of</strong> ripe <strong>and</strong> unripe S. cocculoides fruits extracted using SPME<br />

<strong>and</strong> CFMD methods are provided in Table 4.5 below. Six compounds were obtained in<br />

ripe S. cocculoides using SPME. In contrast, upon using <strong>the</strong> CFMD method, <strong>the</strong> same<br />

ripe S. cocculoides produced three compounds. Unripe S. cocculoides gave only 2-butoxy<br />

ethanol after CFMD.<br />

Table 4.5: Presence <strong>and</strong> identity <strong>of</strong> volatile compounds identified in ripe <strong>and</strong> unripe<br />

S. cocculoides fruits following SPME <strong>and</strong> CFMD extraction<br />

RI Compounds<br />

Ripe fruits Rip<br />

extracted<br />

using SPME<br />

Ripe fruits Unripe fruits<br />

extracted extracted using<br />

using CFMD CFMD<br />

1037 Isobutyl acetate Y X X<br />

1071 Ethyl 2 methyl butyrate Y Y X<br />

1141 2-Methyl-butyl-acetate Y X X<br />

1190 Butyl-2-methyl butyrate Y X X<br />

1758 Geranyl acetate Y X X<br />

Total number <strong>of</strong> esters 5 1 0<br />

1395 2-Butoxy ethanol X Y Y<br />

1915 2,6-Di-terbutyl-4-methyl-phenol Y X X<br />

Total number <strong>of</strong> alcohols 1 1 1<br />

1013 1-Oxiranylethanone* X Y X<br />

Total number <strong>of</strong> carbonyls X 1 Y<br />

Total number <strong>of</strong> compounds 6 3 1<br />

*tentative identification MS only<br />

Y-compound was extracted using this method<br />

X- compound was not extracted using this method<br />

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