Standard X-ray Diffraction Powder Patterns

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$Standard X-ray Diffraction Powder Patterns$

$Standard X-ray Diffraction$

Powder data cardsCardnumber3-0453Indexlines3. 302. 972. 35Cadmium Sulfate, CdSO4 (orthorhombic)SourceDow Chemical company.Additional published patterns. None.NBS sample. The sample of cadmium sulfatewas prepared at NBS from cadmium carbonatetreated with an excess of sulfuric acid and heatedto dry ness. Spectrographic analysis showed themajor impurities to be 0.001 to 0.01 percent eachof aluminum and silicon.20hkl001110101020111021200002121012201211031220131122202040212032041310013231301222141311113321240232302, 203142051, 150331133151Internal Standard,Tungsten, a ==3. 1648 ACu, 1.5405 i at 25 CdA4. 7013. 8263. 3293. 2772. 9612. 6882. 3582. 3522. 3362.2122. 10442. 00681. 98271. 91551. 82731. 77041. 66481. 63911. 61351, 60041. 54851. 52901. 52501. 51791. 49081. 48431. 47041. 45371. 44971. 35711. 34591. 32431. 30591. 29341. 26341. 23171. 22931. 220419611963/174110079686353237242618222117193121811387764971711694817115The sample was white. The indices of refraction could not be determined because the samplewas too fine.The d-values of the three strongest lines are:3.329, 3.277, and 2.961 A.Structural data. Kokkoros and Rentzeperis [1]in 1961 determined cadmium sulfate is orthorhombic with the most probable space group DJh-Pmmn (No. 59) with 2(CdSO4 ) per unit cell.Lattice constantsKokkoros andRentzeperis[1].National Bureauof Standardsat 25 °C.aA4 7094. 71746A6. 5626. 5590cA4. 6944. 7012The density of cadium sulfate calculated fromNBS lattice constants is 4.759 g/cm3 at 25 °C.kkl322223400014052114251420, 303024341313060421124204412161252342134224260333351, 153261440044432Internal Standard, 0Tungsten, a = 3. 1648 ACu, 1.5405 A at 25 CdA1, 21401. 21271. 17941. 15701, 14541. 12351. 11361. 11001. 10621. 10321. 09431. 09331. 07981. 07771. 05191. 04071. 03871. 03051. 02211. 01131. 00160. 9918. 9897. 9839. 9702. 9576. 9552. 949845Reference[1] P. A. Kokkoros and P. J. Rentzeperis, X-ray investigation of the anhydrous cadmium and mercuricsulphates, Acta Cryst. 14, 329-330 (1961).I64335333546522476323335433
Cadmium Telluride, CdTe (cubic)Powder data cardsCardNumber10-207IndexLines3. 742. 291. 95Vaughan [1].SourceAdditional published patterns. None.NBS sample. The sample of cadmium telluridewas obtained from Semi-Elements Inc., Saxonburg,Pa. Spectrographic analysis showed thefollowing impurities: 0.01 to 0.1 percent siliconand 0.0001 to 0.001 percent each of barium, iron,and lead.The sample was a black opaque powder.The d-values of the 0three strongest lines are:3.741, 2.290, and 1.954 A.Structural data. Zachariasen [2] in 1926 determined that cadmium telluride has the zinc sulfidestructure, the space group Td-F43m (No. 216),and 4(CdTe) per unit cell. The lattice constantsof Zachariasen and Goldschmidt have been converted from kX to angstrom units for comparisonwith the NBS value.192619261963Lattice constantZachariasen [2]_ _ _ _Goldschmidt [3]_ ....... ___ _National Bureau of Standardsat 25 °CL_ _....._._.__....£6. 4776. 4536. 481The density of cadium telluride calculated fromthe NBS lattice constant is 5.856 g/cm3 at 25 °C.hkl111220311400331422511440531620533444711642731dA3. 7422. 2901. 9541. 6191. 4881. 3231. 2471. 1461.0951. 0250. 9884.9356. 9076. 8661. 8438Internal Standard,Tungsten, a = 3.1648 ACu, 1.5405 A at 25 °CAverage value of last five lines _References/1006228591042442
Page 1 and 2: c ^r.
Page 3 and 4: UNITED STATES DEPARTMENT OF COMMERC
Page 5 and 6: Introduction.. _ __________________
Page 7 and 8: STANDARD X-RAY DIFFRACTION POWDER P
Page 9 and 10: D. E. Appleman, and D. Handworker.
Page 11 and 12: Ammonium Fluoberyllate, (NH4) 2BeF4
Page 13 and 14: Ammonium Fluoborate, NH4BF4 (orthor
Page 15 and 16: Arsenic Trioxide, claudetite, As2O3
Page 17 and 18: Powder data cardsBarium Stannate, B
Page 19 and 20: Bismuth Orthophosphate, BiPO4 (trig
Page 21 and 22: Bismuth Orthovanadate (high form),
Page 23 and 24: Bismuth Telluride (tellurobismuthit
Page 25: Cadmium Perchlorate Hexahydrate, Cd
Page 29 and 30: Calcium Fluoride Phosphate (fluorap
Page 31 and 32: Cesium Chromate, Cs>CrO 4 (orthorho
Page 33 and 34: Cobalt Fluosilkate Hexahydrate, CoS
Page 35 and 36: Copper Sulfate (chalcocyanite), CuS
Page 37 and 38: Erbium Arsenate, ErAsO4 (tetragonal
Page 39 and 40: Gallium Arsenide, GaAs (cubic)Powde
Page 41 and 42: Indium Arsenide, InAs (cubic)Powder
Page 43 and 44: Lanthanum Niobium Titanium Oxide, L
Page 45 and 46: Lithium Phosphate, high form, Li3PO
Page 47 and 48: Magnesium Ammonium Phosphate Hexahy
Page 49 and 50: Potossium Chlorate, KCIO3 (monoclin
Page 51 and 52: Potassium Zinc Decavanadate 16 Hydr
Page 53 and 54: Silver Antimony Telluride, AgSbTe2
Page 55 and 56: Sodium Trimetaphosphate, Na3P3O9 (o
Page 57 and 58: Sodium Trimetaphosphate Monohydrate
Page 59 and 60: Strontium 1:1 Berate, SrO-B2O3 (ort
Page 61 and 62: Thallium Chromate, Tl2CrO4 (orthorh
Page 63 and 64: Titanium Dioxide, brookite, TiO2 (o
Page 65 and 66: CUMULATIVE INDEX TO CIRCULAR 539, V

Standard X-ray Diffraction Powder Patterns

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